• 제목/요약/키워드: tem-8

검색결과 559건 처리시간 0.024초

TEM sample preparation using micro-manipulator for in-situ MEMS experiment

  • Hyunjong Lee;Odongo Francis Ngome Okello;Gi-Yeop Kim;Kyung Song;Si-Young Choi
    • Applied Microscopy
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    • 제51권
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    • pp.8.1-8.7
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    • 2021
  • Growing demands for comprehending complicated nano-scale phenomena in atomic resolution has attracted in-situ transmission electron microscopy (TEM) techniques for understanding their dynamics. However, simple to safe TEM sample preparation for in-situ observation has been limited. Here, we suggested the optical microscopy based micro-manipulating system for transferring TEM samples. By adopting our manipulator system, several types of samples from nano-wires to plate-like thin samples were transferred on micro-electro mechanical systems (MEMS) chip in a single step. Furthermore, the control of electrostatic force between the sample and the probe tip is found to be a key role in transferring process.

휴대폰 전자파의 혈액 조사를 위한 SAR별 TEM 셀의 입력 전력 산출 (Input Power Determination of TEM Cell Due to SAR for Mobile Phone Wave Blood Exposure)

  • 윤지훈;손태호
    • 한국전자파학회논문지
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    • 제16권8호
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    • pp.810-814
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    • 2005
  • TEM 셀 내에 있는 혈액에 대한 삽입 손실과 반사율을 측정하여, 원하는 혈액 흡수 SAR(Specific Absorption Rate) 선택에 따른 TEM셀 입력 전력을 구하였다. 혈액 세포는 피부 세포와 함께 전자파 영향을 연구하기 위한 기준 세포이다. 따라서 SAR에 따른 혈액 세포에 인가할 전력 산출은 정확해야 함은 물론 타당성이 있어야 한다. 이 연구에서는 g당 혈액 세포가 받는 전력을 산출하기 위해 50 g의 혈액을 이용하여 전달 전력 감소를 측정하였다. 측정된 데이터로부터 휴대폰 전자파 생체 흡수율 SAR 0.8, 1.6, 3, 4 mW/g에 해당하는 TEM셀 입력 전력을 계산하였다. 이 연구 결과는 배양 세포의 전자파 방사 장치에 응용함을 목적으로 하고 있다.

집속 이온빔을 이용한 투과 전자 현미경 시편의 표면 영향에 관한 연구 (Study on Surface Damage of Specimen for Transmission Electron Microscopy(TEM) Using Focused Ion Beam(FIB))

  • 김동식
    • 전자공학회논문지 IE
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    • 제47권2호
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    • pp.8-12
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    • 2010
  • TEM(Transmission Electrion microsopy) 투과전자현미경은 재료의 기초 구조 분석과 반도체 또는 생물시편의 미세 구조분석에 널리 사용되는 장비이다. TEM 분석은 필수적으로 목적에 부합되는 적절한 시편제작이 수반되어야 한다. 다양한 전자 현미경 시편 제작 방법 중 본 논문에서는 FIB(Focus Ion Beam)를 이용한 시편 제작법 중 시편에 입사되는 에너지와 이온 Gun과 시편과의 상호 각도, 이온 밀링 깊이 조절 등의 실험을 통하여 표면 손상 최소화를 벌크 웨이퍼와 패턴화된 시편에서 실험하였다. 최소화된 표면 영향성(약 5nm)을 패턴화된 시편에 구현하였다.

Microstructure and Third Order Optical Nonlinearities of Ion-Implanted and Thermally Annealed $Cu-SiO_2$ Thin Films

  • 채이;이민영;김현경;문대원
    • Bulletin of the Korean Chemical Society
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    • 제18권8호
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    • pp.886-889
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    • 1997
  • The crystal structure and optical properties of copper nanoparticles, prepared in fused silica by ion-implantation and subsequent heat-treatment, were characterized by X-ray, TEM, linear absorption, and degenerate four-wave mixing (DFWM) technique. The X-ray data show fcc lattice structure of the nanocrystals and their size was measured as 8-20 nanometer by high resolution TEM. Using DFWM, the third-order nonlinear optical coefficient of the Cu-SiO2 thin films was measured as 0.4-1.1×10-8 esu in the surface plasmon resonance absorption region (540-570 nm).

Development of TEM Coil for Animal Experiments at 3T MRI System

  • Chu, Myung-Ja;Choe, Bo-Young;Kim, Kyung-Nam;Chung, Sung-Taek;Oh, Chang-Hyun;Lee, Hyoung-Koo;Suh, Tae-Suk
    • 한국의학물리학회:학술대회논문집
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    • 한국의학물리학회 2002년도 Proceedings
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    • pp.365-366
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    • 2002
  • A novel TEM resonator coil was developed for the imaging of small animals. The functional elements of the TEM resonator were 8 inner conductors, distributed in a cylindrical pattern and connected at the ends with capacitors to the cylindrical outer shield. The TEM resonator coil with cavity elements was robust to the surrounding influences due to the self-shielding structure. The TEM resonator coil with high Q factor could provide high quality MR images at 3.0T MRI system. Also, the TEM resonator coil has an advantage for a fine tune with length adjustment of each cavity elements. Thus, The TEM resonator coil at 3.0T, even higher field could be used in the research studies.

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부산시내 종합병원의 임상 검체에서 분리된 Extended -Spectrum $\beta$-Lactamase 생성 Klebsiella pneumoniae의 형별 분류 (Extended-Spectrum $\beta$-Lactamase (ESBL) Typing of Klebsiella pneumoniae Isolated from Clinical Specimen in Pusan)

  • 김윤태;이훈구
    • 미생물학회지
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    • 제36권3호
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    • pp.221-227
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    • 2000
  • 본 연구는 등전점과 PCR 생성물을 통하여 광범위 $\beta$-Lactamase(ESBL) 를 생성하는 Klebsiella pneumoniae의 ESBL 유형을 결정하였다. 부산시내 소재 3개 종합병원의 임상검체로부터 20균주의 ESBL 을생성하는 Klebsiella pneumoniae를 분리하였다. 제 3세대 cephalosporin인 cefotaime, cef-tazidime, ceftriaxone으로 double disk synergy test를 시행하여 ESBL 생성균주를 확인하였다. 등전점 및 PCR결과 TEM 형 (pI 5.2~6.0, 1080 bp), TEM+SHV 혼합형(pI 5.2~6.0 및 pI 7.0~7.4 로 1080 bp, 599bp), SHV형 (pI 7.0~ 7.4, 599 bp) , 그리고 PCR결과는 SHV형으로 나타났으나 등전점을 나타내지 않는 것과 등전점 및 PCR 결과 어느 쪽에도 속하지 않는 non TEM non SHV 형 등 5개군으로 나뉘어 졌다.

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대구지역 폐수처리장에서 분리한 cefotaxime-resistant Escherichia coli의 특성 (Characterization of cefotaxime-resistant Escherichia coli isolated from wastewater treatment plant in Daegu)

  • 김환득;박대현;이미리;김은정;조재근
    • 한국동물위생학회지
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    • 제37권4호
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    • pp.225-231
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    • 2014
  • In this study, 185 cefotaxime-resistant Escherichia coli were isolated from different stages of a wastewater treatment plant (WWTP) in Daegu in Korea. Among them, 99.5% (184 isolates) originated from raw sewage and 0.5% (1 isolates) from the final effluent. Cefotaxime-resistant E. coli were high resistant to ampicillin, piperacillin, cefazolin, cephalothin, cefachlor and cefamandole (99.5~100%). About 93% of the cefotaxime-resistant E. coli were extended-spectrum ${\beta}$-lactamases (ESBL)-producing E. coli. The $bla_{TEM+CTX}$ gene was the most predominant of the ESBL genes (72.5%), followed by $bla_{CTX-M}$ (16.2%), $bla_{TEM}$ (8.7%), $bla_{TEM+CTX+SHV}$ (1.1%), $bla_{TEM+SHV}$, $bla_{TEM+OXA}$, and $bla_{TEM+CTX+SHV}$ (respectvely 0.5%). Class 1 and 2 integron were found in 49.7% and class 3 integron was not found. All of integron positive isolates were multiresistant (i.e. resistant to four or more antibiotics). Our findings showed WWTP is contaminated with antibiotic resistant bacteria with resistance genes.

Modified TEM Horn for Enhanced Radiation Characteristics at Low Frequency

  • Kim, Jae Sik;Park, Hyeong Soon;Yoon, Young Joong;Ryu, Jiheon;Choi, Jin Soo
    • Journal of electromagnetic engineering and science
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    • 제14권2호
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    • pp.74-78
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    • 2014
  • This paper presents a modified TEM horn that improves radiation characteristics at a low frequency region. The proposed antenna consists of an asymmetric TEM (ATEM) horn and a loop structure with an elliptical shape. The bandwidth and gain at low frequency region can be enhanced by using the ATEM horn configuration and adding a loop structure with an elliptical shape to the ATEM horn. The bandwidth of the proposed antenna is from 2.14 to over 20 GHz, whereas that of the conventional TEM horn is from 2.7 to over 20 GHz, where the dimensions of both antennas are the same except for the thickness of the loop structure. The physical and electrical dimensions of the proposed antenna are $60mm{\times}62.5mm{\times}64mm$ ($width{\times}height{\times}length$) and $0.428{\lambda}_L{\times}0.445{\lambda}_L{\times}0.456{\lambda}_L$, where ${\lambda}_L$ corresponds to the lowest frequency of the bandwidth. The realized gain of the proposed antenna is improved by 0.802 dB on average at the low frequency region (2 to 8 GHz), where the maximum gain increase is 2.932 dB when compared to a conventional TEM horn.

엔진 배기 폐열회수로 인한 배기 특성 변화 (Change in Engine Exhaust Characteristics Due to Automotive Waste Heat Recovery)

  • 김기범
    • 한국산학기술학회논문지
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    • 제15권8호
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    • pp.4723-4728
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    • 2014
  • 본 연구에서는 1-D 해석 프로그램인 AMESim을 활용하여 열전소자와 디젤엔진을 모델링하여 이를 New European Driving Cycle (NEDC) 운전모드에서 구동시킨 자동차에서 나오는 폐열을 이용해 열전소자로 발전을 하고 이에 따른 결과를 분석해보는 연구를 수행하였다. 열전소자 모델링 시 배기폐열 회수율 및 전기 에너지 변환률 뿐만 아니라 재료적 특성을 고려하여 열전달부분에 초점을 맞추었다. 또한, 디젤 산화 촉매(DOC)를 설계하여 열전소자로 인한 폐열회수가 디젤 산화촉매 활성화에 미치는 영향과, 그 결과 배기가스의 성분별 증감을 조사하였다. 열전소자를 이용한 폐열회수는 자동차 연비개선에 도움이 되지만, 배기가스의 온도를 떨어뜨려 촉매 활성화에 영향을 미치게 되면, CO와 HC 배출이 최대 14% 증가하는 것을 관찰하였다. 따라서, 열전소자를 이용한 배기 폐열 회수 시스템 개발 시에 배기에 미치는 영향을 고려해야 한다.

Tripod polishing을 이용한 IBAD/RABiTS 기판의 TEM 분석 (TEM analysis of IBAD/RABiTS substrates prepared by Tripod polishing)

  • 최순미;정준기;유상임;박찬;오상수;김철진
    • 한국초전도ㆍ저온공학회논문지
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    • 제8권1호
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    • pp.9-14
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    • 2006
  • Sample preparation plays a critical role in microstructure analysis using TEM. Although TEM specimen has been usually prepared by jet-polishing or Ar-ion beam milling technique. these methods could not be applied to YBCO CC which is composed of IBAD or RABiTS substrates, several buffet layers, and YBCO superconducting layer because of big difference in mechanical strengths between the metallic phase and oxide phases. To obtain useful cross-sectional information such as interface between the phases or second phases in YBCO CC, it is prerequisite to secure the large area of thin section in the cross-sectional direction. The superconducting layer or the buffer layers are relatively weak and fragile compared to the metallic substrate such as Ni-5wt%W RABiTS of Hastelloy-based IBAD, and preferential removal of weak ceramic phases during polishing steps makes specimen preparation almost impossible. Tripod polisher and small jig were home-made and employed to sample preparation. The polishing angle was maintained <$1^{\circ}$ throughout the polishing steps using 2 micrometers attached to the tripod plate. TEM specimens with large and thin area could be secured and used for RABiTS/IBAD substrate analyses. In some cases, additional Ar-beam ion milling with low beam current and impinging angle was used for less than 30 sec. to remove debris or polishing media attacked to the specimens.