• Title/Summary/Keyword: system separation method

Search Result 742, Processing Time 0.031 seconds

Simultaneous HPLC Analysis of Three Flavonoids in the Extracts of Artocarpus heterophyllus Heartwoods

  • Septama, Abdi Wira;Panichayupakaranant, Pharkphoom
    • Natural Product Sciences
    • /
    • v.22 no.2
    • /
    • pp.77-81
    • /
    • 2016
  • A reversed-phase high-performance liquid chromatographic method is described for the simultaneous determination of three antibacterial flavonoids, artocarpanone, artocarpin, and cycloartocarpin in ethyl acetate extracts from Artocarpus heterophyllus heartwoods. Separation was achieved using a TSK-gel ODS-80Tm column ($5{\mu}m$, $4.6{\times}150mm$) at $25^{\circ}C$ with a gradient elution system of methanol and water as follows: 0-8 min, 60:40; 8-27 min, 80:20; 27-35 min, 60:40, v/v, at a flow rate of 1 mL/min, and a quantitative UV detection at 285 nm. The method was validated by measuring the key parameters, including specificity, linearity, sensitivity, accuracy, repeatability and reproducibility. A high degree of specificity and sensitivity was achieved. The calibration curves for all three flavonoids showed good linearity with a coefficient of determinations ($R^2$) of ${\geq}0.9995$. The recoveries of the method were from 98-104%, with good reproducibility and repeatability (RSD values of less than 2%) were also achieved. Ethyl acetate was the best solvent for extraction of these three flavonoids using the heat reflux conditions for 1 h. This optimized sample preparation and HPLC method can be practically used for a routine standardization process of the extracts from the A. heterophyllus heartwoods.

Delimitation of Jurisdiction of Commercial, Civil and Administrative Courts: IT Challenges

  • Baranenko, Dmytro;Stepanova, Tetiana;Pillai, Aneesh V.;Kostruba, Anatolii;Akimenko, Yuliia
    • International Journal of Computer Science & Network Security
    • /
    • v.22 no.7
    • /
    • pp.85-90
    • /
    • 2022
  • In modern conditions of the development of public relations, there is a continuous development of technologies. This not only reflects the convenience of service users, and new technology but also contributes to the emergence of new disputes to protect the rights of stakeholders. Therefore, it is urgent to study the distinctions between the jurisdiction of commercial, civil and administrative courts in resolving IT disputes. The work aims to study the peculiarities of delimitation of the jurisdiction of commercial, civil, and administrative courts through the prism of IT measurement. The research methodology consists of such methods as a historical, comparative-legal, formal-logical, empirical, method of analogy, method of synthesis, method of analysis, and systematic method. Examining the specifics of delimiting the jurisdiction of commercial, civil, and administrative courts through the IT dimension, it was concluded that there is a problem in determining the jurisdiction of the court. In addition, the judicial practice on this issue is quite variable, which negatively affects the predictability of technology in resolving potential disputes. In this regard, the criterion models for distinguishing between commercial, administrative, and civil proceedings according to the legal classification of the parties, as well as the nature of the claim are identified. This separation will contribute to a more accurate application of legal norms and methods of application of administrative norms and reduce the number of cases of improper proceedings.

Free vibration analysis of combined system with variable cross section in tall buildings

  • Jahanshahia, Mohammad Reza;Rahgozar, Reza
    • Structural Engineering and Mechanics
    • /
    • v.42 no.5
    • /
    • pp.715-728
    • /
    • 2012
  • This paper deals with determining the fundamental frequency of tall buildings that consist of framed tube, shear core, belt truss and outrigger systems in which the framed tube and shear core vary in size along the height of the structure. The effect of belt truss and outrigger system is modeled as a concentrated rotational linear spring at the belt truss and outrigger system location. Many cantilevered tall structures can be treated as cantilevered beams with variable cross-section in free vibration analysis. In this paper, the continuous approach, in which a tall building is replaced by an idealized cantilever continuum representing the structural characteristics, is employed and by using energy method and Hamilton's variational principle, the governing equation for free vibration of tall building with variable distributed mass and stiffness is obtained. The general solution of governing equation is obtained by making appropriate selection for mass and stiffness distribution functions. By applying the separation of variables method for time and space, the governing partial differential equation of motion is reduced to an ordinary differential equation with variable coefficients with the assumption that the transverse displacement is harmonic. A power-series solution representing the mode shape function of tall building is used. Applying boundary conditions yields the boundary value problem; the frequency equation is established and solved through a numerical process to determine the natural frequencies. Computer program has been developed in Matlab (R2009b, Version 7.9.0.529, Mathworks Inc., California, USA). A numerical example has been solved to demonstrate the reliability of this method. The results of the proposed mathematical model give a good understanding of the structure's dynamic characteristics; it is easy to use, yet reasonably accurate and suitable for quick evaluations during the preliminary design stages.

A Study on the Realization of Wireless Home Network System Using High-performance Speech Recognition in Variable Position (가변위치 고음성인식 기술을 이용한 무선 홈 네트워크 시스템 구현에 관한 연구)

  • Yoon, Jun-Chul;Choi, Sang-Bang;Park, Chan-Sub;Kim, Se-Yong;Kim, Ki-Man;Kang, Suk-Youb
    • Journal of the Korea Institute of Information and Communication Engineering
    • /
    • v.14 no.4
    • /
    • pp.991-998
    • /
    • 2010
  • In realization of wireless home network system using speech recognition in indoor voice recognition environment, background noise and reverberation are two main causes of digression in voice recognition system. In this study, the home network system resistant to reverberation and background noise using voice section detection method based on spectral entropy in indoor recognition environment is to be realized. Spectral subtraction can reduce the effect of reverberation and remove noise independent from voice signal by eliminating signal distorted by reverberation in spectrum. For effective spectral subtraction, the correct separation of voice section and silent section should be accompanied and for this, improvement of performance needs to be done, applying to voice section detection method based on entropy. In this study, experimental and indoor environment testing is carried out to figure out command recognition rate in indoor recognition environment. The test result shows that command recognition rate improved in static environment and reverberant room condition, using voice section detection method based on spectral entropy.

Protection Distance Calculation Between Inductive Systems and Radiocommunication Services Using Frequency Below 30 MHz (30 MHz 이하에서 무선 서비스와 유도성 시스템 간의 보호 거리 산출)

  • Shim, Yong-Sup;Lee, Il-Kyoo;Park, Seung-Keun
    • The Journal of Korean Institute of Communications and Information Sciences
    • /
    • v.37C no.12
    • /
    • pp.1211-1221
    • /
    • 2012
  • This paper describes separation distance to protect radiocommunication services from the interference of inductive systems using frequencies below 30 MHz for the co-existence between radiocommunication services and inductive systems. For the analysis, the interference scenario model is proposed between inductive system and radiocommunication services. Then the calculation method of protection distance is suggested by comparing the radiation power of inductive system with the allowable interference level of victim services, radiocommunication services, according to the applied propagation model. Also, the protection distance for protecting radiocommunication services in the 30 MHz below is calculated through the interference analysis from RFID(Radio Frequency IDentification) and PDP(Plasma Display Panel) TV based on the suggested method. The proposed calculation method was adopted as ITU-R recommendation in related with resolution 63 at ITU-R SG(Study Group) 1 meeting in June, 2012. It will be available to use for the protection of radiocommunication services from the interference of wireless power transfer system and power line telecommunication system.

Cladding of Cu and Bronze/Al Alloy by $CO_2$ Laser (고출력 $CO_2$레이저빔에 의한 구리, 청동/알루미늄 합금 클래딩)

  • 강영주;김재도
    • Journal of Welding and Joining
    • /
    • v.15 no.4
    • /
    • pp.109-115
    • /
    • 1997
  • Laser cladding is a technique for modification of metal surface. In this laser cladding experiment a metal powder feeding system was developed for more efficient laser cladding. This system can reduce processing time and be used simpler than the conventional method. The feeding of metal powder has given a rise to the process for sequential buildup of bulk rapidly solidified materials in the form of fine powder stream to the laser cladding process. The parameters of laser cladding have been investigated using this experimental equipment. Bronze on aluminum alloy and copper on aluminum alloy were experimented by using defocused beam, powder feeding system, and gas shielding. Good cladding was achieved in the range of beam travel speed of 2.25m/min. In the case of copper/aluminum and bronze/aluminum substrate, the absorption of laser beam was too high to produce low diluted clad. In the case of copper/1050 aluminum, the optimal laser cladding condition was of laser power of 2.8kW, powder feed rate of 0.31g/s and beam travel speed of 2.25m/min. In the case of bronze/aluminum the optimal condition is of laser power of 2.5kW, powder feed rate of 0.31g/s, and beam travel speed of 2.36m/min.

  • PDF

Horizontal hydrodynamic coupling between shuttle tanker and FPSO arranged side-by-side

  • Wang, Hong-Chao;Wang, Lei
    • Ocean Systems Engineering
    • /
    • v.3 no.4
    • /
    • pp.275-294
    • /
    • 2013
  • Side-by-side offloading operations are widely utilized in engineering practice. The hydrodynamic interactions between two vessels play a crucial role in safe operation. This study focuses on the coupled effects between two floating bodies positioned side-by-side as a shuttle tanker-FPSO (floating production, storage and offloading) system. Several wave directions with different side-by-side distances are studied in order to obtain the variation tendency of the horizontal hydrodynamic coefficients, motion responses and mean drift forces. It is obtained that the coupled hydrodynamics between two vessels is evidently distinguished from the single body case with shielding and exaggerating effects, especially for sway and yaw directions. The resonance frequency and the peak amplitude are closely related with side-by-side separation distance. In addition, the horizontal hydrodynamics of the shuttle tanker is more susceptible to coupled effects in beam waves. It is suggested to expand the gap distance reasonably in order to reduce the coupled drift forces effectively. Attention should also be paid to the second peaks caused by hydrodynamic coupling. Since the horizontal mean drift forces are the most mainly concerned forces to be counteracted in dynamic positioning (DP) system and mooring system, prudent prediction is beneficial in saving consumed power of DP system and reducing tension of mooring lines.

A Study on the Measurement of Contact Force of Pantograph on High Speed Train

  • Seo, Sung-Il;Cho, Yong-Hyun;Mok, Jin-Yong;Park, Choon-Soo;Kim, Ki-Hwan
    • 제어로봇시스템학회:학술대회논문집
    • /
    • 2005.06a
    • /
    • pp.1374-1378
    • /
    • 2005
  • Appropriate upward force is crucial for the pantograph on high speed train to collect current from the catenery system without separation. However, at high speed, large aerodynamic lifting force is generated by the contact plate and the arms of pantograph, which may cause wear of the contact wire. In this study, to confirm the interface performance of the pantograph on Korea High Speed Train, a method to measure the contact force of the pantograph was proposed and the related measurement system was developed. The forces acting on the pantograph were clarified and a procedure to calculate the aerodynamic lifting force was proposed. A special device was invented and applied to measure the lifting force. Measured contact forces were displayed by the developed system and evaluated according to the criteria. Countermeasures were also taken to reduce the contact force based on the results.

  • PDF

Influence of Oxygen Supply Method on the Performance of IGCC Plants (IGCC 플랜트에서 산소공급방식이 성능에 미치는 영향)

  • Ahn, Ji-Ho;Kim, Tong-Seop
    • Journal of Hydrogen and New Energy
    • /
    • v.23 no.3
    • /
    • pp.264-273
    • /
    • 2012
  • In this paper, two types of integrated gasification combined cycle (IGCC) plants using either an air separation unit (ASU) or an ion transport membrane (ITM), which provide the oxygen required in the gasification process, were simulated and their thermodynamic performance was compared. Also, the influence of adopting a pre-combustion $CO_2$ capture in the downstream of the gasification process on the performance of the two systems was examined. The system using the ITM exhibits greater net power output than the system using the ASU. However, its net plant efficiency is slightly lower because of the additional fuel consumption required to operate the ITM at an appropriate operating temperature. This efficiency comparison is based on the assumption of a moderately high purity (95%) of the oxygen generated from the ASU. However, if the oxygen purity of the ASU is to be comparable to that of the ITM, which is over 99%, the ASU based IGCC system would exhibit a lower net efficiency than the ITM based system.

Development of a Composite Rotor for Flywheel Energy Storage System (플라이휠 에너지 저장 장치용 복합재 로터 개발)

  • Kim, Myung-Hun;Han, Hun-Hee;Kim, Jae-Hyuk;Kim, Seong-Jong;Ha, Seong-Gyu
    • Proceedings of the Korean Society For Composite Materials Conference
    • /
    • 2005.11a
    • /
    • pp.169-172
    • /
    • 2005
  • A flywheel system is an electromechanical energy storage device that stores energy by rotating a rotor. The rotating part, supported by magnetic bearings, consists of the metallic shaft, composite rims of fiber-reinforced materials, and a hub that connects the rotor to the shaft. The delamination in the fiber wound composite rotor often lowered the performance of the flywheel energy storage system. In this work, an advanced hybrid composite rotor with a split hub was designed to both overcome the delamination problem in composite rim and prevent separation between composite rim and metallic shaft within all range of rotational speed. It was analyzed using a three-dimensional finite clement method. In order to demonstrate the predominant perfom1ance of the hybrid composite rotor with a split hub, a high spin test was performed up to 40,000 rpm. Four radial strains and another four circumferential strains were measured using a wireless telemetry system. These measured strains were in excellent agreement with the FE analysis. Most importantly, the radial strains were reduced using the hybrid composite rotor with a split hub, and all of them were compressive. As a conclusion, a compressive pressure on the inner surface of the proposed flywheel rotor was achieved, and it can lower the radial stresses within the composite rotor, enhancing the performance of the flywheel rotor.

  • PDF