• Title/Summary/Keyword: system separation method

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Simultaneous analysis method of 89Sr and 90Sr in liquid sample using automated separation system (자동핵종분리장치를 이용한 액체시료 중 89Sr, 90Sr 동시분석법 연구)

  • Kim, Heewon;Lee, Yong-Jin;Kim, Sun-Ha;Lee, Jin-Hong;Lim, Jong-Myoung;Kim, Hyuncheol
    • Analytical Science and Technology
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    • v.33 no.6
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    • pp.274-284
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    • 2020
  • This study described the analytical method for simultaneous determination of 89Sr and 90Sr in liquid sample using automated separation system. Radiostrontium in 0.5 kg of liquid sample was concentrated as SrCO3 to reduce the volume of sample, and purified from the sample using Sr-resin 2 mL (BV, Bed volume). The behavior of Sr and interferences such as Ba, Ca and Y were estimated with various flow rate ranging from 1 to 4 mL min-1. The detailed procedure for the purification of Sr on Sr-resin was presented. The purified radiostronitum was measured in Cerenkov mode and then measured in Scintillation mode by mixing scintillation cocktail. The measured value in both modes were used to calculate the activity of 89Sr and 90Sr. The performance tests were carried out the lab-control-sample having various activity ratio of between 89Sr and 90Sr. The recovery of Sr was ranged from 68 to 94 %. The relative bias of 89Sr activity was ranged from -5 to 20 %, and it was ranged from -10 to 10 % for 90Sr.

Ln-resin and HIBA Method for La-Ce and Sm-Nd Isotope Measurement (La-Ce 및 Sm-Nd 동위원소계 측정을 위한 란탄-레진법과 HIBA(Hydroxy Isobutyric Acid)분리법의 상호비교)

  • Lee, Seung-Gu;Lee, Hyomin;Asahara, Yoshihiro;Lee, Mi-Jeong;Choo, MiKyeong;Lee, SeungRyeol
    • The Journal of the Petrological Society of Korea
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    • v.21 no.4
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    • pp.431-439
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    • 2012
  • A column chemistry is the most useful tools for isolating the elements of interest in isotope geochemistry. Here we introduce the chemical experimental procedure for Sm, Nd, La and Ce separation such as Teflon powder or Ln-resin method using HDEHP of KIGAM, KBSI, KOPRI and ${\alpha}$-HIBA(${\alpha}$-Hydroxy Isobutyric acid) method of Nagoya University, Japan. This technical report will provide an useful information in selecting the experiment method for rare earth element isotope system study such as Sm-Nd and La-Ce isotope system.

A full-color anaglyph three-dimensional display system using active color filter glasses

  • Kim, Jong-Hyun;Kim, Young-Hoon;Hong, Ji-Soo;Park, Gil-Bae;Hong, Kee-Hoon;Min, Sung-Wook;Lee, Byoung-Ho
    • Journal of Information Display
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    • v.12 no.1
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    • pp.37-41
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    • 2011
  • Presented herein is a novel stereoscopic three-dimensional (3D) display system with active color filter glasses. This system provides full-color 3D images by applying the time-multiplexing technique on the original anaglyph method. By switching between the opposite anaglyph statuses, a full-color anaglyph is presented. A liquid crystal panel from a 3D monitor serves as an active color filter operating at 120 Hz. A display panel and a color filter are connected to one graphic card as a dual-link system, for synchronization. To test the quality of this system, a left/right-eye image separation test and an experiment with stereoscopic images were carried out. Although there was some crosstalk and blur, the system, as expected, provided full-color 3D display. This system overcomes a monochromatic 3D image, which is the major weakness of the original anaglyph system.

A method for predicting the aerodynamic performance of low-speed airfoils (저속익형의 공기역학적 성능예측의 한 방법)

  • Yu, Neung-Su
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.22 no.2
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    • pp.240-252
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    • 1998
  • The purpose of this study is to develop a method for predicting the aerodynamic performance of the low speed airfoils in the 2-dimensional, steady and viscous flow. For this study, the airfoil geometry is specified by adopting the longest chord line system and by considering local surface curvature. In case of the inviscid incompressible flow, the analysis is accomplished by the linearly varying strength vortex panel method and the Karman-Tsien correction law is applied for the inviscid compressible flow analysis. The Goradia integral method is adopted for the boundary layer analysis of the laminar and turbulent flows. Viscous and inviscid solutions are converged by the Lockheed iterative calculating method using the equivalent airfoil geometry. The analysis of the separated flow is performed using the Dvorak and Maskew's method as the basic method. The wake effect is also considered by expressing its geometry using the formula of Summey and Smith when no separation occurs. The computational efficiency is verified by comparing the computational results with experimental data and by the shorter execution time.

Preparation of High Purity Chondroitin Sulfate (고순도 콘드로이틴 황산의 제조)

  • Kim, Young-Jun;Cho, Suk-Hyung
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.10 no.4
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    • pp.865-871
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    • 2009
  • Chondroitin sulfate was extracted by alkali method and enzyme method from shark cartilage. In extract system, various processing parameters such as concentration of alkali and alcarase, temperature etc, have been investigated for optimization condition. The pure chondroitin sulfate was obtained by UF membrane separation. The characteristics was also investigated with gel permeation chromatograpy(GPC). The molecular weight of chondroitin sulfate was $2.7\times10^4$ Da.

Development of a high-performance liquid chromatographic method for the determintion of levosulpiride in plasma

  • Ban, Eun-Mi;Jang, Dong-Jin;Kim, Adele;Park, Jeong-Sook;Kim, Chong-Kook
    • Proceedings of the PSK Conference
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    • 2002.10a
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    • pp.400.3-401
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    • 2002
  • Levosulpiride is the levo-enantiomer from of racemic sulpride. abenzamide derivative selectively inhibition doparninergic D2 receptos at the trigger zone both in the central nervous system and in the gastrointestinal tract. We report a rapid and sensitive HPLC method using reverse phase C 18 column with fluorescence detection for separation and quantitation of levosulpiride in plasma. Tiapride was used as an internal standard. After adding an internal standard. levosulpiride in 800 ${\mu}l$ of plasma was extracted under basic conditions with ethyl acetate and methylene chloride. (omitted)

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Implementation and Experimental Evaluation of Bandwidth Allocation Scheme on PROFIBUS (PROFIBUS에서 대역폭 할당 기법 구현 및 실험적 평가)

  • Hong, Seung-Ho;Kim, Yu-Chul;Kim, Ji-Yong
    • Journal of Institute of Control, Robotics and Systems
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    • v.6 no.11
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    • pp.943-954
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    • 2000
  • Fieldbus is the lowest level industrial network in the communication hierarchy of factory automation and distributed process control systems. Data generated from field devices are largely divided into three categories : time-critical, periodic and time-available data. Because these data share one fieldbus medium, it needs a method that allocates these data to the bandwidth-limited fieldbus medium. This paper introduces an implementation method of bandwidth allocation scheme on PROFIBUS. In order to implement bandwidth allocation scheme on PROFIBUS, the following functions need to be supplemented on the FDL(Fieldbus Datalink Layer) protocol: (i) separation of medium bandwidth into periodic and non-periodic intervals, (ii) synchronization of node timers over a local link. In order to examine the validity of bandwidth allocation scheme on PROFIBUS, this paper develops an experimental model of a network system. The results obtained from the experimental model show that the bandwidth allocation scheme satisfies the performance requirement of time-critical, periodic and time-available data.

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Mechanical Pretreatment of Municipal Waste Incineration Ash for Recovering Heavy Metals by the Horizontal Gyration Method

  • Park, Joonchul;Kaoru Masuda;Yamaguchi Hiroshi;Shigehisa Endoh
    • Proceedings of the IEEK Conference
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    • 2001.10a
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    • pp.664-667
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    • 2001
  • Segregation of binary particle systems in a horizontally gyrated bed has been experimentally studied to recover the heavy metals from municipal waste incineration (MWI) ash. Differences in density and size had less effect on segregation. Effective segregation took place under the centrifugal effect of 1 or less for any particle size ratio. Zn, Cu and Pb were concentrated in the upper side of bed by the horizontal vibration. However, there was less change in concentration for other metals such as Mg, Al and Fe etc. The separation system with the horizontal gyrating separator proved to be an effective method for the pretreatment of recovering Zn, Cu and Pb from incineration residues.

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Studies on the Differential Determination of cis-, and trans-Neopynamin and Fenitrothion by High Pressure Liguid Chromatography (고속 액체 크로마토그라피에 의한 cis- 및 trans-Neopynamin과 Fenitrothion의 분리 정량에 관한 연구)

  • 이왕규;정해수
    • YAKHAK HOEJI
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    • v.24 no.2
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    • pp.117-122
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    • 1980
  • A new application of high pressure liquid chromatography for the determination of fenitrothion and cis- and trans-neopynamin in insecticidal preparations was investigated. Optimum conditions for a good separation and determination were determined; solvent system: dichloromethane + n-hexane = 17 + 83; Bow rate: 0.5ml/min; column: u-porasil ($4mm{\times}3Ocm$); absorbance wavelength: 254nm; 0.05 AUFS and sample size: 30 ul. Recovery of fenicrothion, cis- and trans-neopynamin from mixed artificial preparations was 99.6%, 99.7% and 99.8% respectively. Also reproducibility tests showed that the coefficient of variation was 0.89% for fenitrothion, 0.74% cis-neopynamin and 1.1% for trans-neopynamin. There was no interference with insecticidal preparation containing DDVP, allethrin, S-421 and kerosene. HPLC method was rapid, accurate and it gave better reproducibility and higher sensitivity than any other analytical method. It was considered that HPLC could be greatly applied to the analysis of fenitrothion and neopynamin in insecticidal preparations.

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Multi-Time Scale Separations and Optimal Control Problems of Multi-Parameter Singular Perturbation Systems (여러 매개상수 특이접동계에서의 여러 시간스케일 분리와 최적제어 문제)

  • Kim, Sam-Soo;Hong, Jae-Keun;Kim, Soo-Joong
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.24 no.1
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    • pp.20-27
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    • 1987
  • The hierarchical approach method is proposed to sperate each different time scale sub-systems from linear time invariant multi-parameter singular perturbation systems. By means of this proposal, the original multi-parameter singular perturbation systems is completely separated into independent subsystems with each different time scale. It is also investigated that the controllability of the system is invariant. And this paper applies singular perturbation methods to the minimum control effort problem for linear time invariant systems with constrained controls. Also near-optimum control theory, which is based on dividing the total time interval with the time scales respectively, is proposed. As a result, the time scale separation method is show to be particularly useful in a near optimum design which can be otained through a decentralized control structure.

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