• Title/Summary/Keyword: synthetic temperature

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A Study on the Manufacture of the Cu Powder from Electrochemical Recovery of Waste Rinse Water at the Cu Electroplating Process (동 도금 수세 폐수로부터 구리 분말 제조에 관한 연구)

  • 김영석;한성호
    • Journal of the Korean institute of surface engineering
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    • v.36 no.2
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    • pp.194-199
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    • 2003
  • Polarization measurements were peformed to investigate the electrochemical behavior of copper ions and limiting current density in waste rinse water from copper electroplating processes. A newly designed cyclone type electrolyzer was tested to recover the copper powder. Synthetic solutions were prepared using analytical grade $CuSO_4$ to the desired waste water concentration and pH was adjusted with $H_2$$SO_4$. Electrowinning was peformed at room temperature and the solution was cycled with a pump. Results showed that more than 99 percent of Cu was recovered and the size of the recovered Cu powder ranges from 0.1 - $0.5\mu\textrm{m}$. The chemical composition of the Cu powder mainly consists of $Cu_2$O and Cu and can be easily reduced to pure Cu powder.

Controlled synthesis of reactive polymeric architectures for stimuli-responsive materials

  • Theato, Patrick;Nilles, Katja;Metz, Nadine
    • Proceedings of the Polymer Society of Korea Conference
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    • 2006.10a
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    • pp.329-329
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    • 2006
  • Various new active ester monomers based on (meth)acrylates and 4-vinylbenzoic acid have been prepared. Investigation of the controlled radical polymerization behavior of the respective monomers resulted in excellent polymerization control, thus, opening synthetic routes to reactive block copolymers. Polymer analogous reactions with amines yielded functional polymers. In the case of the copolymer poly(N-isopropylacrylamide-co-acetone oxime acrylate) a lower critical solution temperature could be measured at $52^{\circ}C$. Thus, the reactive copolymer features two characters: reactive AND stimuliresponsive behavior.

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Lubrication and Cooling Characteristics of Warm Forging Lubricants (온간단조 윤활제의 윤활 및 냉각특성)

  • Kang, J. H.;Ko, B. H.;Jae, J. S.;Kang, S. S.
    • Transactions of Materials Processing
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    • v.14 no.7 s.79
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    • pp.619-623
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    • 2005
  • Lubrication and cooling characteristics are the most important factors of elevated temperature forging lubricants. Usually adopted lubricants in warm forging processes are graphite, synthetic and emulsion lubricants. Most widely and effectively applied lubricants are graphite lubricants, but these have a lot of problems like tool corrosion and dusty environment. In this research, boronite lubricant is considered, because it is able to substitute for graphite. Hot ring compression test, cooling test and mass production test are performed to check the validity of new lubrication pigment.

Studies on the Cation Exchangers from Coals (炭質陽이온交煥體 製造에 關한 硏究)

  • Lee, Bum-Soon;Yoo, In-Sang
    • Journal of the Korean Chemical Society
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    • v.4 no.1
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    • pp.62-66
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    • 1957
  • With the intention of preparing cation exchangers from the domestic coals, and using these for softening hard water and some other purposes, seven kinds of raw coal were tested and the results are as follows. 1) The following conditions of preparation were given the good results. Reaction time 5 hours Reaction temperature $95^{\circ}$ Concentration of sulfuric acid 98% Amount of sulfuric acid 10 times to the sample (as weight) 2) The raw coals which is rich in fixed carbon and have the fuel ratio 0.8 to 1.0 were suitable, and Kampo lignite has shown the best results. 3) The cation exchangers from coals were able to exchange the cation, both hydrogen and sodium type dynamically and statically, like the synthetic ion exchange resin. The exchange capacities were as follows. Total capacity 1.60 meq/g. Breakthrough capacity 1.30 meq/g. Usable breakthrough capacity 1.20 meq/g National Central Research laboratory

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Ag Nanowires Prepared by a Modified Polyol Method with 1,4-Benzoquinone Additives

  • Kang, Miseon;Chung, Eunseon;Kim, Sang-Ho;Rhee, Seog Woo
    • Bulletin of the Korean Chemical Society
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    • v.35 no.11
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    • pp.3209-3212
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    • 2014
  • This paper describes a selective synthetic method of fabricating Ag nanowires by using a modified polyol process. To synthesize the Ag nanowire, an ethylene glycolic solution of silver nitrate and an ethylene glycolic solution of polyvinylpyrrolidone solution containing a small amount of organic oxidant, 1,4-benzoquinone, were slowly added to a hot ethylene glycol medium at $160^{\circ}C$ for 8 min using a syringe pump. The reaction mixtures were heated for an additional 45 min and cooled to room temperature. Finally, the silver nanomaterials were isolated from the mixture by centrifugation. The crystal structure of the nanomaterials was investigated by powder X-ray diffraction analyses, and their morphology was investigated by scanning electron microscopy. A small amount of organic oxidant, 1,4-benzoquinone, played a significant role in controlling the morphology during crystal growth. Consequently, Ag nanowires rather than Ag nanoparticles were selectively obtained.

Calibration of Stellar Isochrones for G- and K-type Dwarfs based on High-Resolution Spectra

  • Lim, Yeseul;An, Deokkeun
    • The Bulletin of The Korean Astronomical Society
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    • v.41 no.2
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    • pp.56.3-57
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    • 2016
  • We present a recent progress on calibration of stellar isochrones based on a set of high-resolution spectra for 170 G- and K-type dwarfs in the solar neighborhood. We compare observed magnitudes of these stars in a number of broad passbands [UB(B_T)V(V_T)RIJHK] with model magnitudes generated using ATLAS9 synthetic library at the previously derived set of spectroscopic parameters. We find systematic offsets in colors from these passbands, which are mainly revealed as a function of effective temperature of stars. In order to remove these systematic color mismatches, we derive correction functions and apply them to the model spectra.

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Combinatorial Synthesis and Screening of the Tb-activated Phosphors in the System $CaO-Y_{2}O_3-Al_{2}O_{3}$

  • Yoon, Ho-Shin;Kim, Chang-Hae;Park, Hee-Dong;Ryu, Seung-Kon
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.836-839
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    • 2003
  • We have synthesized some phosphors in the system $CaO-Y_{2}O_3-Al_{2}O_{3}$ by combinatorial polymerized-complex method. Composition and synthetic temperature of phosphors in the liblary was screened from the emission intensities of individual samples under VUV excitation. In $Tb^{3+}$-activated $CaO-Y_{2}O_3-Al_{2}O_{3}$, green phosphors showing good intensity were found to be $CaYAl_{3}O_{7}$, $CaYalO_{4}$, $YAlO_{3}$, $Y_{3}Al_{5}O_{12}$, $Y_{4}Al_{2}O_{9}$, $Ca_{3}Al_{2}O6$.

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Scientific Visualization of Oceanic Data (GIS정보를 이용한 해양자료의 과학적 가시화)

  • Im, Hyo-Hyuc;Kim, Hyeon-Seong;Han, Sang-Cheon;Seong, Ha-Keun;Kim, Kye-Yeong
    • Proceedings of the Korean Society of Marine Engineers Conference
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    • 2006.06a
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    • pp.195-196
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    • 2006
  • Recently, there are increasing need to make a synthetic assessment about oceanic data which is collected over the various scientific field, in addition to just gathering oceanic data. In this study, we made a basic map using satellite image, aerial photo, multi-beam data, geological stratum data etc. And as well we are producing comprehensive SVT(Scientific Visualization Toolkit) which can visualize various kinds of oceanic data. These oceanic data include both survey data such as tidal height, tide, current, wave, water temperature, salinity, oceanic weather data and numeric modelling results such as ocean hydrodynamic model, wave model, erosion/sediment model, thermal discharged coastal water model, ocean water quality model. In this process, we introduce GIS(Geographic Information System) concepts to reflect time and spatial characteristics of oceanic data.

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Analysis of Electrocoagulation Process using Faraday's Law (Faraday's Law에 의한 전기응집공정의 분석)

  • Kim, Hye-Sook;Yun, Young-Im;Cho, Eun-Jeong;Choi, Yun-Hee;Oh, Mi-Young;Kim, Yeong-Kwan
    • Journal of Industrial Technology
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    • v.21 no.A
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    • pp.351-355
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    • 2001
  • This research was carried out to find out the possibility of using Faraday's law in analyzing the electrocoagulation system. Bench-scale reactor equipped with aluminum electrode plates was operated using synthetic wastewater which received sodium chloride for conductivity adjustment. Phosphate was added to the wastewater to induce the precipitation with Al. The amount of aluminum dissolved from the electrodes could be predicted by Faraday's law with a difference less than 5%. This difference was greater at a higher electric current, probably due to the increased solution temperature. However, effect of pH on the dissolution of the aluminum was negligible. The result of this study suggested that the operating condition of electrocoagulation system could be developed using the Faraday's law when the pollutant concentration is given.

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Synthesis of spherical phosphors (Y,Gd)$BO_3$:Eu from Precursors in Polymeric Form by Aerosol Pyrolysis

  • Jeoung, Byung-Woo;Yoo, Won-Tae;Hong, Gun-Young;Yoo, Jae-Soo
    • 한국정보디스플레이학회:학술대회논문집
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    • 2002.08a
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    • pp.788-791
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    • 2002
  • The phosphors of high luminous efficiency for PDP application must have high purity, single phase, and dense surface. In this work, the polymeric reaction was applied to preparation of spherical phosphor by aerosol pyrolysis in order to enhance mechanical and optical characteristics. The red phosphor of (Y,Gd)$BO_3$:Eu was prepared from polymeric precursor, in which citric acid and ethylene glycol were used as ion carriers, i.e monomers. For enhancing the luminescence intensity and mechanical characteristics. optimum synthesizing condition were investigated through concentration of monomers, synthetic temperature. doped activator concentrations, and annealing process. The phosphors synthesized with monomers showed quite different morphology from those without monomers. It was observed that polymeric precursor made an effect on particle formation mechanism and status of particles surface. The resultant spherical phosphors show the comparable luminescent properties to the commercial product (product by Nichia co.). Also, they were observed to have the rigid surface.

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