• 제목/요약/키워드: synthetic specimen

검색결과 49건 처리시간 0.025초

Study on Corrosion Characteristics and Stress Corrosion Cracking of the Weldment for HT-60 Steel in Synthetic Seawater

  • Na, Eui-Gyun;Koh, Seung-Ki;Oh, Seok-Hyung
    • Journal of Mechanical Science and Technology
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    • 제14권2호
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    • pp.152-158
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    • 2000
  • The contents of this paper include the evaluation of corrosion characteristics and the behaviour of stress corrosion cracking (SCC) for the weldment and post weld heat treatment (PWHT) specimen and parent of HT -60 steel using a slow strain rate test (SSRT) in synthetic seawater. Corrosion characteristics were obtained from the polarization curves by potentiostat, and SCC phenomena were evaluated through the parameters such as reduction of area and time to failure by comparing the experimental results in corrosive environment with those obtained in air. Corrosion rate of the weldment was the fastest, followed by parent and PWHT specimen. SCC phenomena between the weldment of HT-60 steel and synthetic seawater were shown. Besides, SCC was dependent upon the pulling speed greatly. Maximum severity of SCC was obtained at a speed of $10^{-6}mm/min$, whereas SCC could not be seen almost at $10^{-4}mm/min$. The resistance to SCC for PWHT specimen was improved considerably compared that of the weldment at $10^{-6}mm/min$. In case of SCC failure, it was verified from SEM examination that brittle mode and lots of pits could be seen at the fractured region near the surface of the specimen.

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합성절연유의 전기적 특성에 미치는 BTA의 영향 (The Influence of the BTA on Electrical Properties of Synthetic Fluids)

  • 신종열;신현택;홍진웅
    • 한국전기전자재료학회논문지
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    • 제11권2호
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    • pp.162-166
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    • 1998
  • Synthetic fluid, class 7 group 2, as an insulating and cooling material is selected as. specimen, arid it is studied for the physical and electrical properties. Also, Benzotriazole(following as BT A) known as a suppressant of streaming electrification is added to it, and the change of physical and electrical properties by addition of BT A is investigated. From the spectrum of FT-IR, it is confirmed that the absorption peak in wavenumbers $3400{\sim}3450[cm^{-1}]$ is small or disappears when BTA is added. AC breakdown strength and volume resistivity of each specimen are investigated. It is considered that the effective content of BTA is about 10[ppm] for the suppression of electrification in this experiment.

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합성절연유의 절연파괴 특성에 미치는 유동대전 억제제의 영향 (The Effect of Antistatic Agent for Streaming Electrification on the Breakdown Characteristics of Synthetic Fluids)

  • 송병기;이수원;신종열;신현택;홍진웅
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1997년도 하계학술대회 논문집 C
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    • pp.1414-1416
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    • 1997
  • The electrical breakdown characteristics of the synthetic fluids No.2 of KS class VII used for insulating and cooling the materials for the ignition coil are studied. Also, Benzotriazole(BTA) as the streaming electrification suppressant additive is added to the oil, and the change of electrical properties due to different BTA concentration is investigated. To investigate the electrical characteristics, the breakdown strength of each specimen by an experiment for AC breakdown are analyzed. The breakdown strength of specimen by adding BTA is higher than virgin specimen in low e region, but lower than that in high region because of melting BTA. It is considered that the effective content of BTA as charge suppressant additive is about 10[ppm] from the results of AC breakdown.

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수열합성반응에 의한 경량콘크리트 블록 개발에 관한 기초적 연구 (The Fundamental Study on the Development of Light Weight Concrete Block by the Hydro-Thermal Synthetic Reaction)

  • 강철;강기웅;정지용;곽은구;권기주;김진만
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2005년도 봄학술 발표회 논문집(II)
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    • pp.461-464
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    • 2005
  • As the research on the development of the lightweight concrete block by the hydro-thermal synthetic reaction mixed with the calcareous material and bottom ash that is used less among siliceous material, we studied on the physical and chemical characteristics in the changes of hydro-thermal synthetic reaction of lightweight concrete block compounded with the PP fiber to increase flexural toughness and to prevent fragility failure. The results of the experiment are as follow. According to the increase of hydro-thermal synthetic reaction and the fiber content, compressive and flexural strength increased. Despite the changes of the hydro-thermal synthetic reaction time, tobermorite was produced on each of the specimens similarly. However, the phase of tobermorite was changed in accordance with the changes of time. Also, $CaCo_{3}$ appeared on the surface of the 9 hour hardened specimen.

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치과용(齒科用) 경석고(硬石膏) 의 표면경도(表面硬度) 강화(强化)에 관(關)한 실험적(實驗的) 연구(硏究) (Experimental Studies on the Improving Surface Hardness of Dental Stone)

  • 김창회
    • 대한치과보철학회지
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    • 제9권1호
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    • pp.23-27
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    • 1969
  • The purpose of this studies is to determine the surface hardness of dental stone and to investigate the methods which increase the surface hardness of dental stone using the dissolved solution of various synthetic resin, the obtained results of hardness value calculated Rockwell Hardness Number by means of Rockwell Hardness Tester. 1) In this experiment, 10% polystyrene dissolved in 100cc amylacetate is excellent solution which provides the surface hardness of dental stone after setting of specimen, and there is no effective way that stone specimen is immersed into polystyrene in amylacetate, polystyrene in benzene and polystyrene in butylacetate above 1 hour. 2) When the stone specimen is immersed into acrylic resin in benzene and melamin resin in amylacetate at least 1 hour to 3 hours, the hardening effect of stone surface is valuable. 3) The stone specimen immersing into urea resin in butylacetate, the surface hardness of the stone specimen decreased within 1 hour, but increased after 3 houre. 4) For the separating medium, the easyfoil is superior to the olive oil in the aspect of improving the hardening effect of the immersed specimen.

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마이크로파 에너지에 의해 결정 크기가 조절된 유기 안료의 합성 (The Synthesis of Crystalline-Size Controlled Organic Pigment by Microwave Energy)

  • 정기석;고진필;박상보;박찬영;민성기;권종호;오인환;박성수
    • 폴리머
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    • 제25권5호
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    • pp.609-616
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    • 2001
  • 본 연구에서는 copper phthalocyanine (CUPc)을 높은 합성 수율로서 성공적으로 합성시킴에 따라 용매를 사용하는 고분자의 합성 분야에 마이크로파 기술의 응용 가능성을 제시하고자 하였다. 가정용 전자레인지의 용기를 개조시키고 마이크로파 출력 조절기를 부착시키는 방법으로 본 실험에 사용되는 가변식 마이크로파 합성 장치를 자체 제작하였다. 화학 분석법, X선 회절장치(XRD), 주사형 전자현미경 (SEM) 및 입도 분석법 (PSA)을 이용하여 재래식 열 공정 및 마이크로파 공정을 사용하여 여러 조건하에서 합성된 시료들의 특성을 비교 분석하였다.

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지의류 추출염액에 의한 견섬유 염색 (Dyeing of Silk with Lichen Extract)

  • 이전숙;이득영
    • 한국염색가공학회지
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    • 제11권6호
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    • pp.43-50
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    • 1999
  • Lichen had been used as dyestuffs before the discovery of synthetic dyes in Europe and by American Indians. To investigate the dyeability of Korean native lichens, 10 kinds of lichen were collected and colorants were extracted from them by boiling in water and fermenting in ammonia water. Silk fabrics were dyed with lichen extract, then the colour differences of dyed silk fabrics were measured before and after color fastness test. The most part of the lichen extracts(Fc, Hh, Me, Pl, Xm, Pr, Cj, Ld, Ry) dyed silk yellowish or reddish brown. The range of colors were 2.4Y 6.5∼10YR 6/7. Pa extract dyed silk purple(1.25RP 5/6). Color differences of laundered specimen with the silk before laundering were very small, but color of the dyed silks after exposing to light showed big differences with the specimen before exposing to light. The colors of the silks dyed with lichens changed from yellowish or reddish brown to greenish brown by laundering and by exposing to light. But the specimen dyed Pa extract changed from purple to blueish purple by laundering and reddish purple by exposing to light.

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소형펀치시험법에 의한 응력부식균열 감수성평가에 관한 연구 (Stress Corrosion Cracking Susceptibility Evaluation by Small Punch Test)

  • 유효선;이송인;정세희
    • 대한기계학회논문집
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    • 제17권8호
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    • pp.2033-2042
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    • 1993
  • In conventional SCC susceptibility test, there are constant strain test, constant load test, slow strain rate test(SSRT) and K$_{ISCC}$ test. Among them, the SSRT method is much more aggressive in producing SCC than the other tests, so that the test time of it is considerably reduced. But this SSRT method has mostly been worked using the uniaxial tensile specimen untill now. Therefore, the SSRT method using the tensile specimen(Ten-SSRT) has much difficulty in SCC susceptibility evaluation of a localized region like weldment and the advantage material of high order. Recentely, the small punch(SP) test method using miniaturized small specimen is the very effective test method for fracture strength evaluation of a localized region like weldment and fusion reactor wall irradiated in the nuclear power plant. This paper investigated the possibility of SCC susceptibility evaluation by the SP-SSRT method using the miniaturized small specimen. Therefore, we obtained the result that the SP-SSRT had the possibility for the evaluations of SCC susceptibility for shorter time to corrosive environment compare to Ten-SSRT which was conventional method.

자동차 점화코일용 절연유의 전기적 특성 (Electrical properties of insulating oils for automobile ignition coil)

  • 신종열;홍진웅
    • 한국자동차공학회논문집
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    • 제7권5호
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    • pp.172-177
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    • 1999
  • In this paper, the physical and electrical properties of the synthetic fluids No. 2 class Ⅶ used the insulating oils for automobile ignition coil are studied. Also, benzotriazole(BTA) as the streaming electrification suppressant additive is added to the oil, and the change of physical and electrical properties due to different BTA concentration is investigated. To investigate the electrical characteristics, the breakdown strength of each specimen by an experiment for AC breakdown and the changes of conductivity by measuring volume resistivity are analyzed. It is considered that the effective content of BTA as charge suppressant additive is about 10[ppm] from the results of AC breakdown and volume resistivity test.

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