• 제목/요약/키워드: synthetic solution

검색결과 611건 처리시간 0.027초

블록체인을 활용한 내부자 유출위협 데이터 공유 연구 (A Study on Insider Threat Dataset Sharing Using Blockchain)

  • 윤원석;장항배
    • Journal of Platform Technology
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    • 제11권2호
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    • pp.15-25
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    • 2023
  • 본 연구는 유출위협 탐지 연구에 활용되는 유출위협 데이터 셋의 한계점을 분석하고 현재의 문제를 극복하기 위해 보안솔루션을 활용하여 공개된 유출위협 데이터와 비교 분석한다. 이를 통해 유출위협 탐지에 적합한 데이터 포맷을 설계하고 블록체인 기술을 사용하여 서로 다른 기관 및 기업 간 유출위협 정보를 안전하게 공유할 수 있는 시스템을 구현한다. 현재 연구원들에게 공개된 유출위협 데이터 셋에서 실제 사건을 기반으로 수집한 데이터 셋은 없다. 공개된 데이터 셋은 연구를 위해 임의로 만들어진 가상의 합성데이터로 학습모델로 사용 시 실제 환경에서의 많은 한계점이 존재한다. 본 연구에서는 이러한 한계점들을 개선하기 위해서 프라이빗 블록체인 설계하여 소속이 다른 기관끼리 안전한 정보공유를 위해 참여자 간 합의와 검증을 통해 신뢰성을 높이고 정보의 무결성과 정합성을 유지하는 방안을 도출하였다. 제시한 방법은 유출위협 수집기를 통해 데이터를 수집하고 블록체인 기반 공유 시스템을 통해 합성데이터가 아닌 실제 위협을 가했던 양질의 데이터 셋을 수집하여 현재의 유출위협 데이터 셋 문제를 해결하고 향후 내부자 유출위협 탐지 모델에 기여할 것으로 사료된다.

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Parameter estimation of four-parameter viscoelastic Burger model by inverse analysis: case studies of four oil-refineries

  • Dey, Arindam;Basudhar, Prabir Kr.
    • Interaction and multiscale mechanics
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    • 제5권3호
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    • pp.211-228
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    • 2012
  • This paper reports the development of a generalized inverse analysis formulation for the parameter estimation of four-parameter Burger model. The analysis is carried out by formulating the problem as a mathematical programming formulation in terms of identification of the design vector, the objective function and the design constraints. Thereafter, the formulated constrained nonlinear multivariable problem is solved with the aid of fmincon: an in-built constrained optimization solver module available in MatLab. In order to gain experience, a synthetic case-study is considered wherein key issues such as the determination and setting up of variable bounds, global optimality of the solution and minimum number of data-points required for prediction of parameters is addressed. The results reveal that the developed technique is quite efficient in predicting the model parameters. The best result is obtained when the design variables are subjected to a lower bound without any upper bound. Global optimality of the solution is achieved using the developed technique. A minimum of 4-5 randomly selected data-points are required to achieve the optimal solution. The above technique has also been adopted for real-time settlement of four oil refineries with encouraging results.

Development of Nanostructured Light-Absorbers for Ultrasound Generation by Using a Solution-Based Process

  • Sang, Pil Gyu;Heo, Jeongmin;Song, Ju Ho;Thakur, Ujwal;Park, Hui Joon;Baac, Hyoung Won
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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    • pp.377-377
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    • 2016
  • Under nanosecond-pulsed laser irradiation, light-absorbing thin films have been used for photoacoustic transmitters for ultrasound generation. Especially, nanostructured absorbers are attractive due to high optical absorption and efficient thermoacoustic energy conversion: for example, 2-dimensional (2-D) gold nanostructure array, synthetic gold nanoparticles, carbon nanotubes (CNTs), and reduced graphene oxides. Among them, CNT has been used to fabricate a composite film with polydimethylsiloxane (PDMS) that exhibits excellent photoacoustic conversion performance for high-frequency, high-amplitude ultrasound generation. Previously, CNT-PDMS nanocomposite films were made by using a high-temperature chemical vapor deposition (HTCVD) process for CNT growth. However, this approach is not suitable to fabricate large-area CNT films (>several cm2). This is because a chamber dimension of HTCVD is limited and also the process often causes nonuniform CNT growth when the film area increases. As an alternative approach, a solution-based process can be used to overcome these issues. We develop PDMS composite transmitters, based on the solution process, using several nanostructured light-absorbers such as CNTs, nanoink powders, and imprinted regular arrays of gold nanostructure. We compare fabrication processes of each composite transmitters and photoacoustic output performance.

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폐굴껍질에 의한 합성폐수 중의 인 제거 (Phosphorus Removal from Synthetic Wastewater by Waste Oyster Shells)

  • 정경훈;정오진;최형일
    • 한국환경보건학회지
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    • 제26권3호
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    • pp.43-49
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    • 2000
  • A laboratory experiments were performed to investigate the effects of several factors on the phosphorus removal by waste oyster shells. The waste oyster shells used in this experiments were crushed particle, calcined particle and extracted solution. A higher efficiencies of phosphorus removal were observed, when a particle size of crushed and calcined particle were smaller. The effluent concentration of phosphorus was around 1.6mg/ι in continuous column experiment which packed with crushed particle of waste oyster shell at the influent concentration of PO4-P of 10 mg/ι. But the clogging of column occurred with increasing of throughput volume of influent. The efficiency of phosphorus removal increased with increasing of dosage amount of crushed, calcined particle and extracted solution. When the calcined particle which contained only about 1/10~1/100 of crushed particle was used, the efficiency of phosphorus removal was correspondingly equivalent to the removal efficiency obtained from crushed particle. The efficiency of phosphorus removal by calcined particle after 9 runs repeated use was decreased about 21.5% as that of the first run. The removal efficiency of 100% could have been achieved at the HRT of 18 hours during the continuous treatment of phosphorus by the solution extracted from calcined particle.

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산성황산동 용액 내에서 동판위에 녹청 형성에 관한 기초적 조사 (An Investigation on the Patination of Copper in Acidic Copper Sulfate Solution)

  • 윤승열
    • 한국표면공학회지
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    • 제5권3호
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    • pp.77-85
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    • 1972
  • A method of preparation of synthetic ignorgaic coating on copper (patina) has been presented . An Eh--pH diagram was constructed for the present Cu-H2O-SO$_4$ system using the most recently available thermodynamic data. In the path of the patination at room temperature the general behaviour of copper in acidic copper sulfate solutions with potassium chlorate as an oxidizing agent appeared to follow those predictable in this Eh-pH diagram. In the presence 0.05 molar cupric sulfate at a temperature of about 28$^{\circ}C$ a green brochantite (CuSO$_4$$.$3Cu(OH)$_2$) layer was formed on copper sheet in 20 days. In a solution having an initial pH of 3.5 the development of a brochantite coating has been observed to take place in two stages. In the first, a layer of cuprous oxide formed on the copper at a relatively rapid rate. In the ensuing step the outer layer of cuptrite was oxidized at much slower rate to form brochantite. The syntetic coatings appeared to consist of crystal-lites of brochanitite growing perpendicular to the cuprose oxide surface. The outer tips of the -crystallites were reasily broken off and gave to the layer a rather chalky character. Underneath, at the brochantite Cu$_2$O interface, however, the green layers were firmely attached. The effect of reagent concentration , solution agitation , and moderate temperature increase were investigated to improve the quality of coating. So also in a qualitative way were the effect of light.

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완충 수용액중 로이신엔케팔린 및 [D-알라$^2]$-로이신엔케팔린아미드의 물리화학적 안정성 (Physicochemical Stability of Leucine Enkephalin and $[D-Ala^2]$-Leucine Enkephalinamide in Buffered Aqueous Solution)

  • 박인숙;전인구
    • 약학회지
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    • 제38권5호
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    • pp.488-495
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    • 1994
  • To evaluate the feasibility of transmucosal delivery of leucine enkephalin (Leu-Enk) and its synthetic analog, $[D-Ala^2]$-leucine enkephalinamide (YAGFL), their physicochemical stabilities in aqueous buffered solutions were first investigated using a stability indicating high performance liquid chromatography. The degradation of Leu-Enk and YAGFL followed the pseudo-first-order kinetics. From the pH-rate profiles, it was found that the maximal stability of the two pentapeptides was at the pH of about 5.0. The shelf lives $(t_{90%})$ for the degradation of Leu-Enk and YAGFL at pH 5.0 and $40^{\circ}C$ were found to be 48.13 and 50.9 days, respectively. From the temperature dependence of the degradation, activation energies for Leu-Enk and YAGFL were calculated to be 13.61 and 13.47 kcal/mole, respectively. A higher ionic strength and a higher initial peptide concentration in buffered solution slowed the degradation of the two pentapeptides. The addition of 2-hydroxypropyl-${\beta}$-cyclodextrin into the peptide solution did not affect the stability significantly.

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Seawater-driven forward osmosis for direct treatment of municipal wastewater

  • Sun, Yan;Bai, Yang;Tian, Jiayu;Gao, Shanshan;Zhao, Zhiwei;Cui, Fuyi
    • Membrane and Water Treatment
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    • 제8권5호
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    • pp.449-462
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    • 2017
  • Direct treatment of municipal wastewater by forward osmosis (FO) process was evaluated in terms of water flux decline, reverse salt diffusion, pollutants rejection and concentration efficiency by using synthetic seawater as the draw solution. It was found that when operating in PRO mode (active layer facing the draw solution), although the FO membrane exhibited higher osmotic water flux, more severe flux decline and reverse salt diffusion was also observed due to the more severe fouling of pollutants in the membrane support layer and accompanied fouling enhanced concentration polarization. In addition, although the water flux decline was shown to be lower for the FO mode (active layer facing the feed solution), irreversible membrane fouling was identified in both PRO and FO modes as the water flux cannot be restored to the initial value by physical flushing, highlighting the necessity of chemical cleaning in long-term operation. During the 7 cycles of filtration conducted in the experiments, the FO membrane exhibited considerably high rejection for TOC, COD, TP and $NH_4{^+}-N$ present in the wastewater. By optimizing the volume ratio of seawater draw solution/wastewater feed solution, a concentration factor of 3.1 and 3.7 was obtained for the FO and PRO modes, respectively. The results demonstrated the validity of the FO process for direct treatment of municipal wastewater by using seawater as the draw solution, while facilitating the subsequent utilization of concentrated wastewater for bioenergy production, which may have special implications for the coastline areas.

규질 이암으로부터 제올라이트의 수열 합성에 관한 연구 (Hydrothermal Synthetic Study of Zeolites from Siliceous Mudstone)

  • 노진환
    • 한국광물학회지
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    • 제13권4호
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    • pp.171-185
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    • 2000
  • Siliceous mudstones are embedded on a large scale in the Tertiary formations of Pohang area. Some useful zeolites such as NsP, (Na, TMA)P, analcime and hydroxysodalite were synthesized from the siliceous mudstones by treating with the variety of solution, i.e ., NaOH, NaOH+NaCl, NaOH, NaOH+$NaAlO_2$and NaOH+TMAOH at the low-temperature hydrothermal system ranging 60~12$0^{\circ}C$. Major precursor of zeolites is found as opal-CT in the zeolite-forming reaction. Smectite, which is included in considerable amounts in the mudstone, appears to play a major role of Al-source in the zeolite synthesis. In comparison, chalcedonic quartz and mica are rather insoluble in alkaline solution, and thus, these are observed as major impurities in the reaction products. An addition of $NaAlO_2$to NaOH solution is effective for eliminating these impurities in the reaction procedure, through these are partly dissolved when elevating the reaction temperature, concentration, and time. Phase change from NaP to hydroxysodalite takes place at the NaOH concentrations of 3.0~4.0 M, and the reaction is not sensitive to the temperature shift. NaP is more stable at lower NaOH concentration and higher activity of $Na_{+}$ whereas analcime is sensitive to the temperature change and stable at higher than $100^{\circ}C$ and 2.0~4.0 M in NaOH concentration. For the pure NaP synthesis without any other products, the treatment of mudstones with 1:1 solution of NaOH and $NaAlO _2$ turns out to be quite effective. NaP was successfully synthesized together with analcime at $100^{\circ}C$ as well as lower concentrations of NaOH+NaCl solution. In addition, the organic type, (Na, TMA)P was formed together with smectite in the 1:1 solution of NaOH and TMAOH.

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볏짚 잿물 매염에 의한 소목 염색에서 명반 첨가가 색상변화에 미치는 영향 (Effect of Aluminum Potassium Sulfate Addition on the Color Change in Caesalpinia Sappan Dyeing by Rice Straw Ash Solution)

  • 서희성;전동원;김종준
    • 한국의류학회지
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    • 제29권11호
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    • pp.1465-1474
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    • 2005
  • The primary purpose of this study is to investigate the differences in the characteristics of the mordants, synthetic aluminum mordants and ash solutions as natural mordants, used in Caesalpinia sappan dyeing. By introducing aluminum potassium sulfate in the ash solutions, the behavior of the aluminum in the ash solutions were observed. In the rice straw ash solutions, adjusted to the levels of pH6 and pH10, the aluminum potassium sulfate was introduced to achieve various concentration levels. From the analysis of the ash solution of pull, $K^+$ and $Na^+$ ion concentrations were found to be extremely high, while $Al^+$ ion concentration was 0. The color development in the Caesalpinia sappan dyeing by ash solution mordanting was found to be mainly governed not by the mordanting actions of the metallic ions but by those of alkali components. In the case of cotton, the application of pH10 ash solution promoted reddish color development compared to the case of non-mordanting, regardless of the aluminum potassium sulfate addition. In the case of silk, the application of pH10 ash solution increased a* value and decreased b* value compared to the case of non-mordanting.

Bone Charcoal에 의한 폐수증의 중금속 흡착특성 (Adsorption Characteristics of Heavy Metals in Wastewater on Bone Charcoal)

  • 정팔진;곽동희;이재욱
    • 한국물환경학회지
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    • 제16권4호
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    • pp.555-563
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    • 2000
  • The study was conducted to evaluate the adsorption equilibrium of heavy metals on bone charcoal made of livestock bone which was sintered at $550{\sim}600^{\circ}C$. Analysis of bone charcoal by XRD and FT-IR showed that crystal structure was similar to that of synthetic hydroxyapatite. Adsorption equilibrium capacity of single component (Pb, Cd, and Zn) on bone charcoal could be expressed as Langmuir, Freundlich, and Sips equations. Sips isotherm was best among the three isotherms. The values predicted by IAST(ideal adsorbed solution theory) showed good relationship to the experimental data in multicomponent adsorption equilibrium. Adsorption affinity was in order of Pb, Cd, and Zn. The order was same in case of activated carbon or synthetic hydroxyapatite. Through the study results. it would be expected that bone charcoal made of livestock could be used in field of wastewater treatment plants as adsorbent to remove heavy metal.

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