• 제목/요약/키워드: surface treatment agent

검색결과 401건 처리시간 0.024초

콘크리트 표면 처리 방법 및 용사면에 따른 Zn-Al 금속 용사 피막의 물리적 특성 평가 (Evaluation of physical properties of Zn-Al metal spray coating according to concrete surface and treatment method)

  • 장종민;양현민;이한승
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2022년도 봄 학술논문 발표대회
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    • pp.59-60
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    • 2022
  • When a metal sprayed film of several hundred ㎛ on the concrete surface is possible to 80 dB of shielding effect electromagnetic waves (ElectroMagnetic Pulse, EMP). Therefore, in this study, as a way to secure EMP shielding performance by applying a metal spray coating showing excellent EMP shielding performance to a concrete structure, the metal spray welding efficiency and thin film adhesion performance according to the concrete spray direction and surface treatment method were evaluated. Metal sprayed efficieny according to the metal spraying direction and method was confirmed that the difference was insignificant by applying the roughening agent. However, the method of strengthening the concrete surface and applying the sealing agent show maximum adhesion strength of 3.98 MPa compared to other methods, and it is judged that this method can be utilized for the metal spraying method for concrete EMP shielding.

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도재의 표면처리에 따른 레진시멘트와의 전단결합강도 및 표면상태에 관한 연구 (A STUDY OF SHEAR BOND STRENGTH AND SURFACE CONDITION BETWEEN SURFACE TREATED PORCELAIN AND RESIN CEMENT)

  • 박상혁;박상진
    • Restorative Dentistry and Endodontics
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    • 제22권1호
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    • pp.144-155
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    • 1997
  • This study evaluated shear bond strength between porcelain and resin cement according to various surface treatments of porcelain, and surface condition of debonded porcelain. 50 porcelain specimens(Celay block A2M7) and composite resin specimens(Clearfil Photo-Bright) were prepared, and divided into 5 experimental groups according to the treatment method of porcelain surface. 5 experimental groups by surface treatments were as follows; CONTROL Group : No surface treatment was done on the surface of porcelains. SAND Group : The surface of porcelains were sandblasted with $50{\mu}m$ aluminum oxide for 5 seconds. HF Group: The surface of porcelains were etched with 8% Hydrofluoric acid for 4 minutes. SIL Group: The surface of porcelains were coated with silane coupling agent and heated at $100^{\circ}C$ for 5 minutes. SAND+HF+SIL Group : The surface of porcelains were sandblasted with $50{\mu}m$ aluminum oxide for 5 seconds and etched with 8% Hydrofluoric acid for 4 minutes, and coated with silane coupling agent and heated at $100^{\circ}C$ for 5 minutes. After surface treatments on the prepared porcelain surface two pastes of Panavia 21$^{(R)}$ were mixed, they were applied between composite resin block and porcelain surface, and then excessive resin cements were removed, and its margin was surrounded with Oxyguard II. All specimens were stored for 24 hours in water at $37^{\circ}C$ and tested with Instron testing machine between porcelains and resin cements, and debonded porcelain surfaces were observed under Scanning Electon Microscope(Hitachi S-2300) at 20kvp. The values from each group were compared statistically by Student's t-test. The obtained results were as follows; 1. The shear bond strength without surface treatment of porcelain was the lowest among all experimental groups(p<0.05). 2. The detached porcelain surface with sandblasting alone had more remarkable cracks than with only Hydrofluoric Acid or Silane coupling 2gent, but showed the lowest value of shear bond strength among surface treated groups(p<0.05), 3. When porcelain surface was treated by hydrofluoric acid, it affected shear bond strength more than silane coupling agent, but there were no significant statistical differences(p>0.05). 4. When three methods were combined to increase shear bond strength between porcelains and resin cements, its value was the highest than the others(p<0.05). 5. In Scannig Electron Micrograph of detached porcelain surface with no treatment, the sample revealed adhesive failure between the porcelain and resin cement whereas detached porcelain surface with combination of three method cohesive failure on the porcelain.

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카본블랙류 미세입자 포집을 위한 유리섬유 필터백의 고분자 표면처리에 관한 연구 (A study on the Polymer surface treatment of GF-filter bag for collection of fine Particle like carbon black)

  • 이봉;최희락;문창권
    • 동력기계공학회지
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    • 제12권3호
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    • pp.55-59
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    • 2008
  • In this paper, we have investigated on collection efficiency of fine particle of glass fiber-filter bag according to the surface treatment. The solution consisted of polytetrafluoroethylene(teflon), graphite powder, silicon resin and water was used as a basic surface treatment agent. Tensile strength of glass filter-bag increased with up to 3hrs and then decreased with surface treatment time. Tensile strength and initial modulus of the glass fiber-filter bag treated by iodine after basic surface treatment for 3hrs were lower than those of basic surface treatment for 3hrs, however collection efficiency and fracture strain were higher than those of basic surface treatment for 3hrs. Glass fiber-filter bag with lower initial modulus and more strain will be extend the durable period and the one treated by iodine after basic surface treatment 3or 3hrs is expected high collection efficiency of fine particle. This method makes it possible to manufacture glass fiber-filter bag of the optimum condition.

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Silane coupling agent인 MPS 농도별처리에 따른 열중합 레진과 자가중합 레진 간의 전단결합강도 (Effects of Treatment of Silane Coupling Agent in MPS Concentration on the Shear Bond Strength between Self Curing Resins and Heat Curing Resin)

  • 최에스더;권은자
    • 한국콘텐츠학회논문지
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    • 제15권2호
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    • pp.344-351
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    • 2015
  • 본 논문은 치과에서 많이 사용되고 있는 silane coupling agent로 표면 처리한 의치상 레진과 자가중합 레진 간의 전단 결합력에 미치는 영향에 대해 알아보고자 하였다. 의치상 레진에 silane coupling agent 농도별 표면 처리 후 자가중합레진을 주입하여 전단결합강도를 측정하였다. Silane coupling agent(MPS)의 농도별 표면 처리에 따른 의치상 레진과 자가중합레진 간의 전단결합강도에서는 Vertex self curing resin에서 5%, 7%에서 유의적으로 높게 나타났고(P<0.05), Kooliner에서는 5%에서 유의적으로 가장 높게 나타났다(P<0.05). 따라서 의치상 레진과 자가중합레진 사이에 MPS 5%를 이용한 표면처리가 전단결합강도에 효과적으로 영향을 미치는 것이라 사료된다.

정전기 방지를 위한 기능성 펄프 트레이 개발 (Development of Functional Pulp Tray for Prevention of Static Electricity)

  • 이지영;김철환;남혜경;박형훈;권솔;이영민
    • 펄프종이기술
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    • 제47권5호
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    • pp.52-60
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    • 2015
  • Static electricity is an imbalance of electric charges within or on the surface of a material. All packed items that are particularly sensitive to static discharge must be protected by antistatic treatment. Otherwise, static electricity generated by an electrical insulator may cause serious damages to some sensitive electronics. In order to remove or prevent a buildup of static electricity, packed items must be treated with the application of an antistatic agent, which helps any excess charge to be evenly distributed. Functional pulp tray used for packing of electronic goods was developed with application of an antistatic agent. As the concentration of the antistatic agent increased, charging voltage and surface resistance of molded pulps decreased. The increase of humidity in surrounding atmosphere around molded pulps led to the decrease of accumulation of static charges. In conclusion, the surface treatment of the antistatic agent not only reduced or eliminated buildup of static electricity in the surface, but also prevented generation of tiny dirts from molded tray.

수리된 복합레진 수복물의 전단결합강도 연구 (SHEAR BOND STRENGTH OF REPAIRED COMPOSITE RESIN RESTORATIONS)

  • 최수영;정선와;황윤찬;김선호;윤창;오원만;황인남
    • Restorative Dentistry and Endodontics
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    • 제27권6호
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    • pp.569-576
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    • 2002
  • This study was peformed to evaluate the interfacial shear bond strength of base (direct and indirect) and repair composites with aging and surface treatment methods. Direct composite resin specimens ($Charisma^{\circledR}$, Heraeus Kulzer, Germany) were aged for 5 min, 1 hour, 24 hours, and 1 week in $37^{\circ}C$ distilled water before surface treatment, and then divided into five groups Group 1, grinding; Group 2, grinding and application of bonding agent, Group 3, grinding, etching with 37% phosphoric acid for 30sec, and application of bonding agent, Group 4, grinding, etching with 37% phosphoric acid for 30sec, silane treatment, and application of bonding agent ; Group 5, grinding, etching with 4% hydrofluoric acid for 30sec. silane treatment, and application of bonding agent. Indirect composite resin specimens ($Artglass^{\circledR}$, Heraeus Kulzer, Germany) were aged for 1 week in $37^{\circ}C$ distilled water and divided into seven groups Group 1 - Group 5, equal to Charisma specimens; Group 6, grinding, etching with 37% phosphoric acid for 60sec, silane treatment, and application of bonding agent; Group7, grinding, etching with 4% hydrofluoric acid for 60 sec, silane treatment, and application of bond-ing agent. The repair material($Charisma^{\circledR}$) was then added on the center of the surface (5 mm in diameter. 5 mm in height). The shear bond strength was tested and the data was analyzed using one-way ANOVA and the Student- Newman-Keuls test. The following conclusions were drawn. 1 The shear bond strength of $Charisma^{\circledR}$ specimens aged for 1 hour was significantly higher in Group 2 and Group 5 than in Group 1 (p<0.05), and that of $Charisma^{\circledR}$ specimens aged for 1 week was signifi-cantly higher in Group 3 and Group 5 than in Group 1 (p<0.05). No significant difference was found in the bond strength of specimens aged for 5 min and 24 hours. 2. In Group 2 of the $Charisma^{\circledR}$ specimens, there was significant difference between the bond strength of 24 hours and that of 1 week (p<0.05). 3. In Group 4 of the $Charisma^{\circledR}$ specimens, the shear bond strength of specimens aged for 24 hours was significantly higher than the others(p<0.05) 4. There was no significant difference between the shear bond strength of the $Artglass^{\circledR}$ specimens, 5. Most of the $Charisma^{\circledR}$ specimens showed cohesive fractures. Artglass^{\circledR}$ specimens that were etched with acid (phosphoric or hydrofluoric) for 30 sec showed more cohesive fractures.

광중합형 복합레진 수리시 표면처리가 전단결합강도에 미치는 영향 (THE EFFECT OF SURFACE TREATMENTS ON THE SHEAR BOND STRENGTH OF REPAIRED COMPOSITES)

  • 문장원;이광원;박수정
    • Restorative Dentistry and Endodontics
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    • 제24권1호
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    • pp.156-165
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    • 1999
  • The purpose of this study was to evaluate the effect of surface treatments on the shear bond strength between new and old composites. Circular cavities prepared on the center of acrylic resin mold and the prepared cavities were filled with composite resin. They randomly assigned into control group and 8 groups according to the difference in surface treatments of old composites; Control group: no surface treatment, Group 1: surface treated with #120 SiC paper & bonding agent, Group 2: surface treated with #400 SiC paper & bonding agent, Group 3: surface treated with #120 SiC paper, 32% $H_3PO_4$ & bonding agent, Group 4: surface treated with #400 SiC paper, 32% $H_3PO_4$ & bonding agent, Group 5: surface treated with #120 SiC paper, primer & bonding agent, Group 6: surface treated with #400 SiC paper, primer & bonding agent, Group 7: surface treated with #120 SiC paper, 32% $H_3PO_4$, primer & bonding agent, Group 8: surface treated with #400 SiC paper, 32% $H_3PO_4$, primer & bonding agent. New composites were applicated on the old composites of experimental groups. The shear bond strengths for the experimental specimen were measured and the results were analyzed by using one way ANOVA. The observations of surface morphology after SiC paper roughening and debonded surface morphology after shear bond strength test were done by SEM. The results were as follows; 1. Shear bond strengths for specimens roughened with #120 SiC paper matching with the particle size of coarse diamond bur were significantly higher than those for the specimens with #400 SiC paper(P<0.05). By SEM, the surface of the specimens roughened with #120 SiC paper was more irregular than the specimens with #400 SiC paper. 2. Shear bond strengths for specimens treated with 32% $H_3PO_4$ etchant, primer, bonding resin were significantly higher than those for specimens treated with 32% $H_3PO_4$ and bonding resin(P<0.05). 3. Shear bond strengths for the specimens treated with 32% $H_3PO_4$ etchant and bonding resin were significantly higher than those for specimens treated with only bonding resin(P<0.05). There was no remarkable change of surface morphology after 32% $H_3PO_4$ etching. 4. It was possible to observe mixed fracture patterns (the cohesive fracture of old composite and the adhesive fracture between old and new composite) in the specimens roughened with #120 SiC paper, but almost adhesive fracture in the specimens roughened with #400 SiC paper.

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Wool 직물의 나노 발수 발유가공 (Water and Oil Repellency of Wool Fabric Treated with Nano-type Finishing Agent)

  • 최보련;한삼숙;이문철
    • 한국염색가공학회지
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    • 제20권6호
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    • pp.26-34
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    • 2008
  • Wool fabric having high moisture content were treated with fluorocarbon-based water and oil repellent finishing agents by pad-dry-cure system. Three types of finishing agents which were regular-type or nano-type were adapted to compare the surface chemical composition, water and oil repellent property, crease recovery angle, and durability to repeated laundering. From the surface chemical compositions resulted by ESCA and C1s curve-fitting, it was shown that the regular-type finishing agent were easily taken off from the finished wool fabrics after repeated laundering. On the other hand, the fluoroalkyl groups of nano-type finishing agents turned round from fabric surface to fiber internal after repeated laundering. The water repellency of the wool fabrics treated with regular-type agent had a little changes according to the treatment condition changes and sharply decreased with repeated laundering. However, these values when treated with nano-type agents increased with the concentration and cure temperature and were maintained after 20 times laundering. The wool fabrics treated with nano-type agent had a great oil repellency irrespective of treatment conditions. Furthermore, the wrinkle recovery values of the wool fabrics treated with nano-type agents were higher than those of the fabrics treated with regular-type agent and were unchanged after 20 times laundering.

보강제 변화에 따른 실리콘 고무의 전기 특성 (Electric Properties of Silicone Rubber on Reinforcing Agent Dependence)

  • 이성일
    • 대한안전경영과학회지
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    • 제6권1호
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    • pp.301-309
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    • 2004
  • An inorganic filling agent, ATH (alumina trihydrate) was used to induce inorganic-organic coupling by mixing with stearic acid, acryl silane, vinyl silane as surface treatment agents in order to apply as a high voltage insulating material. Volumetric resistivity was shown to vary with surface treatment agents, and the highest value was obtained in case of the mixture with vinyl silane. The dielectric breakdown intensity was shown to decrease gradually and saturate to a stable value, possibly due to the increase of cross link density in the vinyl radicals introduced to silica surface, resulting in stable dielectric breakdown intensity in the final stages. Tracking and flame retardant properties were also shown to be the best among the samples investigated in this study.

탄소섬유 표면처리에 따른 탄소섬유/폴리프로필렌 복합재료의 기계적 물성 평가 (Evaluation of Mechanical Property of Carbon Fiber/Polypropylene Composite According to Carbon Fiber Surface Treatment)

  • 한송희;오현주;김성수
    • 대한기계학회논문집A
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    • 제37권6호
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    • pp.791-796
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    • 2013
  • 본 연구에서는 탄소섬유의 표면처리에 따른 탄소섬유/폴리프로필렌 복합재료의 기계적 물성을 평가하였다. 탄소섬유와 폴리프로필렌 사이의 계면 결합력을 증가시키기 위해 실란 커플링제 처리와 플라즈마 처리 같은 탄소섬유의 표면처리를 실시하였다. XPS, SEM 그리고 단일섬유 인장강도 시험을 통해 표면 처리된 탄소섬유의 표면 특성을 분석하였으며, Short beam 전단시험을 통해 표면 처리에 따른 복합재료의 계면 전단 강도를 측정하였다. 실험 결과로부터 플라즈마 처리 시간에 따라 복합재료의 계면 전단 강도는 증가하였으며, 1 분 동안 플라즈마 처리 후 실란 커플링제 처리된 시편의 계면 전단 강도는 처리하지 않은 시편에 비해 48.7% 증가하였다.