• Title/Summary/Keyword: surface textured

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Texture development in cold-roiled and heat-treated Ni tapes (냉간가공과 열처리한 Ni 테이프에서의 집합조직 발달)

  • 이동욱;지봉기;임준형;주진호;정충환;박순동;전병혁;홍계원;김찬중
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07a
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    • pp.535-538
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    • 2002
  • Cube-textured Ni substrates for YBCO coated conductors were fabricated by cold-rolling and annealing of Ni powder compacts. To establish the optimum sintering temperature, tensile test was performed for the Ni rod sintered at various temperatures. The Ni rods prepared at above 100$0^{\circ}C$ showed good mechanical properties due to the complete densification of the Ni rods. The Ni rods were rolled to final thickness of 100 ${\mu}{\textrm}{m}$ and then annealed at 100$0^{\circ}C$ for various annealing time for texture development. The texture analysis made by 2 $\theta$ scan and pole-figure showed that the cube texture was developed in a short time of a few munitues. The FWHM of in-plane and out of plane texture of the prepared Ni tapes was 8-10$^{\circ}$. The AEM surface roughness of the Ni tapes was as smooth as 3 nm.

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Take Off Characteristics of Slider for Various LZT Disks and Ambient Pressures (레이저 범프와 대기압 변화에 대한 하드디스크 슬라이더의 부상 특성)

  • Lee, Sang-Min;Kim, Dae-Eun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.10 s.181
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    • pp.2646-2653
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    • 2000
  • The performance of slider of a hard disk drive affects the durability of the system. Particularly, the flying ability of the slider is critical in terms of surface damage and head crash. In this work, the take-off characteristics of the slider for various types of laser zone textured bump geometries were investigated. Also, the effect of ambient pressure on the flying characteristics of the slider was experimentally observed. An index of air density which can be used as a parameter for evaluating the flying characteristic is introduced.

Nano-tribology of laser textured hard disk by contact start/stop test (CSS test에 의한 레이저 텍스쳐 디스크의 나노-트라이볼로지)

  • Kim, Woo-Seok;Hwang, Pyung;Kim, Jang-Kyo
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2000.06a
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    • pp.1589-1595
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    • 2000
  • 레이저 텍스쳐와 미케니칼 텍스쳐 컴퓨터 하드디스크의 마찰과 마코 매카니즘이 Contact Start/Stop test 실행후의 특성들에 대해 연구되었다. 다양한 분석적이고 기계적인 테스트 기술들이 이용되었다. 형상, 조도, 화학적 조성, 기계적 성질, CSS 로부터 기인된 코팅의 마찰특성들에 대해 그 변화들을 조사하였다. 즉, AFM(Atomic Force Microscopy), Nano-Indentation, Nano-Scratch, TOF-SIMS(Time of Flight Secondary Ion Mass Spectroscopy), AES(Auger Electronic Spectroscopy)등이 이 연구에 적용되었다. 레이저 텍스쳐 범프의 표면조도와 미케니칼 텍스쳐 지역의 표면조도는 각각 대략적으로 4nm 와 7nm 감소되었다. 탄성계수와 경도값은 CSS test후에 증가하였고 가장 바깥쪽의 코팅층의 변형강화가 생겨났다. 자성층과 Ni-P 층 사이에 점착성의 문제가 확인되었다. TOF-SIMS 분석은 C 와 $C_2F_5$의 세기에 있어서 감소를 드러냈고 이것은 코팅 표면에 윤활제 요소의 마모를 확실시 할수 있는 결과로 나타났다.

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Fabrications of YBCO Coated Conductors Using Tilted Single Crystalline Nickel Tapes

  • Kim, Ho-Sup;Yoo, Ja-Eun;Jung, Kook-Chae;Youn, Do-Jun
    • Progress in Superconductivity
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    • v.2 no.1
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    • pp.33-38
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    • 2000
  • Ni tapes were textured by taking advantage of their secondary recrystallization. The obtained 18cm long tapes had textures of single crystalline qualities with their [001] axes tilted with respect to the surface and their [010] axes parallel to the rolling direction. The reproducibility of this texturing was checked by taking statistics on the crystal orientations of 24 Ni tapes. $YBCO/CeO_2/YSZ/CeO_2$ films grown on the Ni tape had the same crystalline orientations. Magnetic field dependent I-V relations were measured on a 5cm section of the tape. $J_c$ defined by $20{\mu}V/mm$ criterion was $1.5\times10^5A/cm^2$ at 77K under zero field and was reduced by $\sim$50% under the applied magnetic field of 5T.

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Development of advanced laser processing for the fabrication of HTS metallic tapes for power applications (전력용 고온초전도 금속테이프 제작을 위한 첨단 레이저공정 개발)

  • Lee, Sang-Yeol
    • Proceedings of the KIEE Conference
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    • 1997.11a
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    • pp.688-691
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    • 1997
  • Good quality superconducting $YBa_2Cu_30_{7-{\delta}}$(YBCO) thin films were grown on Hastelloy (Ni-Cr-Mo alloys) with yttria-stabilized zirconia(YSZ) buffer layers by in situ pulsed laser deposition in a multi-target processing chamber. Generally, Hastelloy exhibits excellent resistance to corrosion, fatigue, thermal shock, impact, and erosion. However, it is difficult to make films on flexible metallic substrates due to interdiffusion problems between metallic substrates and superconducting overlayers. To overcome this difficulty, it is necessary to use YSZ buffer layer since it will not only limit the interdiffusion process but also minimize the surface microcrack formation due to smaller mismatch between the film and the substrate. In order to enhance the crystallinity of YBCO films on metallic substrates, YSZ buffer layers were grown at various temperatures different from the deposition temperature of YBCO films. On YSZ buffer layer grown at higher temperature than that for depositing YBCO film, the YBCO thin film was found to be textured with c-axis orientation by x-ray diffraction and had a zero-resistance critical temperature of about 85K.

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Oxygenation of Zone-melting NbBaCuO superconductor (구역용융법으로 제작된 NdBaCuO 초전도체의 산소흡착 특성)

  • Soh, Dea-Wha;Fan, Zhanguo;Kim, Hee-Nam;Li, Xinyu;Gao, Weiying;Kim, Tae-Wan
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11b
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    • pp.292-295
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    • 2001
  • The NdBaCuO superconducting samples were prepared by the Zone melting under low oxygen partial pressure. After the zone-melting the oxygenation process of the NdBaCuO samples in a oxygen flow furnace was studied. In order to compare the oxygenation condition the sintering NdBaCuO samples were studied also. In the study it is found that the optimum temperature for the oxygenation is $350^{\circ}C$, and the oxygen flow speed, the sample volume and the surface area of the sample would influence the oxygenation and the oxygen content.

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Study on the Frictional Behavior, Wear and Corrosion Resistance of Textured TiN Coated Layers (집합조직이 존재하는 TiN 코팅 층의 마찰, 마멸, 내부식 특성에 관한 연구)

  • 김희동;김인수;성동영;이민구
    • Transactions of Materials Processing
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    • v.12 no.4
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    • pp.394-400
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    • 2003
  • TiN coated films exhibit excellent mechanical properties such as high wear, erosion and corrosion resistances and a high thermal stability. Therefore, they are widely applied to a coating material in tools, ornaments, parts and semiconductors. However, the fracture of TiN coated films frequently occurs. The distribution of preferred orientations, i.e., texture, of TiN coated films strongly influences the fracture behavior of these films. In the present study. various TiN coating layers having different textures were prepared by the reactive ion physical vapor deposition and the texture dependence of friction coefficient, erosion and corrosion in these coating layers was investigated. The sample depicting the (115) texture parallel to the coating layer normal displayed a flatter surface than that observed from the sample having the (111) texture. The friction coefficient of TiN thin films was hardly dependent on the texture of coated samples. The samples having (115) texture displayed higher wear, erosion and corrosion resistances than the samples having (111) texture.

Microstructure and Microwave Dielectric Properties of ZrTiO4 Thin Films Prepared by Metal-organic Decomposition (금속유기분해 법으로 제조한 ZrTiO4 박막의 미세구조 및 고주파 유전특성)

  • Park, Chang-Sun;Sun, Ho-Jung
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.22 no.1
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    • pp.53-60
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    • 2009
  • $ZrTiO_4$ dielectric thin films were coated by metal-organic decomposition, and annealed by rapid thermal processing up to $900^{\circ}C$ for their crytallization. Crystallized single-phase $ZrTiO_4$ thin films were fabricated above the annealing temperature of $800^{\circ}C$, but their grains were randomly oriented without specific textured orientation. Best dielectric properties were presented by the sample annealed at $800^{\circ}C$ which had crystalline structure and flat surface. Dielectric constant of the film was maintained at 32 throughout full frequency range up to 6 GHz, and dielectric loss was varied between 0.01 and 0.04.

Characteristics of ZnO Thin Films Grown on p-type Si and Sapphire Substrate by Pulsed Laser Deposition

  • Lee, K. C.;Lee, Cheon
    • KIEE International Transactions on Electrophysics and Applications
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    • v.3C no.6
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    • pp.241-245
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    • 2003
  • ZnO thin films on (l00) p-type Si and sapphire substrates have been deposited by a pulsed laser deposition technique using an Nd:YAG laser with a wavelength of 266 nm. The influence of the deposition parameters such as oxygen pressure, substrate temperature and laser energy density on the properties of the grown films was studied. The experiments were performed for substrate temperatures in the range of 200∼50$0^{\circ}C$ and oxygen pressure in the range of 100∼700 sccm. All of the films grown in this experiment show strong c-axis orientation with (002) textured ZnO peak. With increasing substrate temperature, the FWHM (full width at half maximum) and surface roughness were decreased. In the case of using sapphire substrate, the intensity of PL spectra increased with increasing ambient oxygen flow rate. We investigated the structural and morphological properties of ZnO thin films using X-ray diffraction (XRD), scanning electron microscopy (SEM) and atomic force microscopy (AFM).

LED Light Coupler Design for a Ultra Thin Light Guide

  • Lee, J.H.;Chang, W.;Choi, D.
    • Journal of the Optical Society of Korea
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    • v.11 no.3
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    • pp.113-117
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    • 2007
  • A LED light coupler is proposed for coupling light from a mini side LED of 0.4 mm height to a very thin (${\sim}0.3 mm$) light guide. Due to the ultra thinness of the light guide, conventional light couplings between LEDs and light guides do not provide adequate coupling efficiency. The designed LED coupler is a compound lens of 3.5 mm length, 1.2 mm height, and 3.3 mm width. The courier first collimates the light from the LED and then concentrates the light in a manner similar to a compound parabolic concentrate, (CPC) into the light guide. The exit surface of the coupler is additionally textured to have micro patterns in order to control the radiance profile.