• Korean Journal of Materials Research
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• v.23 no.2
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• pp.81-88
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• 2013

In this study, using a tin chloride solution as the raw material, a nano-sized tin oxide powder with an average particle size below 50 nm is generated by a spray pyrolysis process. The properties of the tin oxide powder according to the nozzle tip size are examined. Along with an increase in the nozzle tip size from 1 mm to 5 mm, the generated particles that appear in the shape of droplets maintain an average particle size of 30 nm. When the nozzle tip size increases from 1 mm to 2 mm, the average size of the generated particles is around 80-100 nm, and the ratio of the independent particles with a compact surface structure increases significantly. When the nozzle tip size is at 3 mm, the majority of the generated particles maintain the droplet shape, the average size of the droplet-shaped particles increases remarkably compared to the cases of other nozzle tip sizes, and the particle size distribution also becomes extremely irregular. When the nozzle tip size is at 5 mm, the ratio of droplet-shaped particles decreases significantly and most of the generated particles are independent ones with incompact surface structures. Along with an increase in the nozzle tip size from 1 mm to 3 mm, the XRD peak intensity increases, whereas the specific surface area decreases greatly. When the nozzle tip size increases up to 5 mm, the XRD peak intensity decreases significantly, while the specific surface area increases remarkably.

• Journal of Fisheries and Marine Sciences Education
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• v.19 no.1
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• pp.1-7
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• 2007

The purpose of this study was to investigate geochemical characteristics of surface sediments in the Keum river estuary adjacent to coastal area. For this study we collected the 21 surface sediments samples. Mean size of surface samples was $3.24{\sim}6.65{\phi}$ on inner estuary and was $2.15{\sim}3.42{\phi}$ on outside estuary. Surface samples were composed of silt on inner estuary and were composed of sand which was more larger than $4{\phi}$ on outside estuary. Most major elements except CaO, $Na_2O$ showed good relationships between variation of contents and grain size. Contents of $Al_2O_3$, $Fe_2O_3$, MgO, $K_2O$, $TiO_2$, $P_2O_5$ and $M_nO$ were increased predominately owing to the variation of mean size of surface samples. Contents of Co, Cr, Cu, Li, Sr, Zn, La, Ce, Pb, Rb, Nd have a good relationships with grain size but Ba, Th, Sm have not. All of major and minor elements contents except $K_2O$ and Ba were less than world mean contents of shallow surface sediments but apprehend a high pollution possibility on silt sediments in the estuaries.

• Korean Journal of Materials Research
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• v.21 no.12
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• pp.690-696
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• 2011

In this study, nano-sized tin oxide powder with an average particle size of below 50 nm is prepared by the spray pyrolysis process. The influence of air pressure on the properties of the generated powder is examined. Along with the rise of air pressure from $0.1kg/cm^2$ to $3kg/cm^2$, the average size of the droplet-shaped particles decreases, while the particle size distribution becomes more regular. When the air pressure increases from $0.1kg/cm^2$ to $1kg/cm^2$, the average size of the dropletshaped particles, which is around 30-50 nm, shows hardly any change. When the air pressure increases up to $3kg/cm^2$, the average size of the droplet-shaped particles decreases to 30 nm. For the independent generated particles, when the air pressure is at $0.1kg/cm^2$, the average particle size is approximately 100 nm; when the air pressure increases up to $0.5kg/m^2$, the average particle size becomes more than 100 nm, and the surface structure becomes more compact; when the air pressure increases up to $1kg/cm^2$, the surface structure is almost the same as in the case of $0.5kg/cm^2$, and the average particle size is around 80- 100 nm; when the air pressure increases up to $3kg/cm^2$, the surface structure becomes incompact compared to the cases of other air pressures, and the average particle size is around 80-100 nm. Along with the rise of air pressure from $0.1kg/cm^2$ to $0.5kg/cm^2$, the XRD peak intensity slightly decreases, and the specific surface area increases. When the air pressure increases up to $1kg/cm^2$ and $3kg/cm^2$, the XRD peak intensity increases, while the specific surface area also increases.

• Journal of the Korean institute of surface engineering
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• v.55 no.6
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• pp.403-407
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• 2022

Grain size of material is important factor in evaluating mechanical properties. Methods for grain size determination are described in ASTM grain size standards. However, conventional method require pretreatment of the surface to clarify grain boundaries. In this study, the grain size from the surface image obtained from scanning electron microscope was measured using the watershed algorithm, which is a region-based method among image segmentation techniques. The shapes of the crystals are similar to each other, but the size and growth height are different. In addition, crystal grains are adjacent to each other, so it is very similar to the shape image of the topography. Therefore, grain boundaries can be efficiently detected using the Watershed algorithm.

• 제어로봇시스템학회:학술대회논문집
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• 1996.10b
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• pp.1404-1407
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• 1996

A quality monitoring system in butt welding process is proposed to estimate weld pool sizes. The geometrical parameters of the weld pool such as the top bead width and the penetration depth plus half back width are utilized to prove the integrity of the weld quality. The monitoring variables used are the surface temperatures measured at three points on the top surface of the weldment. The temperature profile is assumed that it has a gaussian distribution in vertical direction of torch movement and verify this assumption through temperature analysis. A neural network estimator is designed to estimate weld pool size from temperature informations. The experimental results show that the proposed neural network estimator which used gaussian distribution as temperature information can estimate the weld pool sizes accurately than used three point temperatures as temperature information. Considering the change of gap size in butt welding, the experiment were performed on various gap size.

• Transactions of the Korean Society of Automotive Engineers
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• v.2 no.4
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• pp.39-49
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• 1994

An experimental investigation was undertaken in a diesel spray to evaluate wall impingement behavior and droplet size distribution. Emphasis is placed on the possibility of the application for new combustion type which is based on OSKA-D type. Visualization were employed using optical scheme which was a spark shadowgraphy to observe the behavior of wall impingement caused by diesel spray vertically injected at the center of the combustion chamber. Droplet size measurements using Malvern system were made to quantify the visual observations with surface diameter of impingement. The effects of the surface dia. variation on the droplet size during injection with the wall impingement spray are discussed. It was found that for the wall impingement spray the droplet size becomes greatly small rather than the spray without the wall impingement and the droplet deposition rate of the injection fuel is decreased as the surface area of impingement becomes small.

• Korean Journal of Metals and Materials
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• v.49 no.11
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• pp.831-838
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• 2011

Effects of spangle size and crystallographic characteristics on the surface appearance, galling properties, and adhesive strength of hot-dip galvanized steel sheets have been investigated. Both spangle size and crystallographic orientation measured by optical microscopy, scanning electron microscopy, and X-ray diffraction were identified as critical factors influencing the galvanized coating performance. By decreasing the spangle size, surface appearance and galling properties related to the friction coefficient were significantly improved. However, low temperature adhesive-strength with small spangle galvanized steel sheets showed lower values compared to commercially used galvanized coating. The variation of adhesive strength in terms of spangle size has been clarified.

• Journal of Magnetics
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• v.20 no.1
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• pp.21-25
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• 2015

Fine Nd-Fe-B-type particles were prepared by ball milling of different types of Nd-Fe-B precursor materials, such as die-upset magnet, HDDR-treated material, and sintered magnets. Coercivity dependence on the grain and particle size of the powder was investigated. Coercivity of the milled particles was reduced as the particle size decreased, and the extent of coercivity loss was dependent upon the precursor material. Coercivity loss in the finely milled particles was attributed to the surface oxidation. The extent of coercivity loss in the fine particles was closely linked to grain size of the precursor materials. Coercivity loss was more profound for the fine particles with larger grain size. Contrary to the fine particles from the sintered magnets with larger grain size the fine particles (~10 um) from the die-upset magnet and HDDR-treated material with much finer grain size still retained high coercivity (> 10 kOe for die-upset magnet, > 4 kOe for HDDR-treated material).

• Journal of the Korea Academia-Industrial cooperation Society
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• v.14 no.8
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• pp.3650-3655
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• 2013

A state purpose to produce fine blanking die gets to be the maximum size of share surface the study considered that change a size of share area. the clearance affecting most greatly size of share surface fixing as 1% of material thickness and while change share speed, A distance change from share line to V-ring center, A change of V-ring angle. it designed. Each test specimen taken from the share surface size analysis of the V-ring distance of 2mm, the outer $45^{\circ}$ / inner$30^{\circ}$ if the, Shear speed was found that the area of the entire cross section is largest the 6.4m/min.

• Tribology and Lubricants
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• v.20 no.5
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• pp.266-271
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• 2004

The aim of this paper is to investigate the effect of surface texturing on reduction friction and to understand the potential of friction reduction through micro-scale dimple to fabricate by photolithography on pin-on-disk test using flat-on-flat contact geometry. It was verify that the friction property with respect to the same pitch has been influence on the size of dimple under lubricated sliding contact. Also, we can recognize from Stribeck curve that the friction property has a connection with the size of dimple. It can explain a relationship between the friction coefficient and a dimensionless parameter for lubrication condition. The friction property has been an effect on the size of surface texture on reduction friction, not only because the density of dimple, but also because the ratio of diameter/pitch. This ratio of approximately 0.5 recommend under the tested friction condition. It suggested that the ratio of d/p is an important parameter for surface texture design.