• Journal of Korean Society of Occupational and Environmental Hygiene
• /
• v.15 no.1
• /
• pp.1-7
• /
• 2005

Although the Fourier Transform Infra-Red spectrophotometric Direct on Filter(FTIR-DOF) method is a useful analytical technique for quantifying quartz content in respirable dust samples, a number of analytical problems must be taken into consideration such as, to name only a few, inhomogeneous deposition of particles, level of environmental humidity, uneven surface of the filter, and interfering minerals in the sample. This study was designed to select the most suitable wavelength and proper filter material for the method, and to investigate effects of humidity and inhomogeneous deposition of particles on the filter. Samples of respirable dust, created in a dust chamber containing standard material of quartz, were collected using a cyclone equipped with a 25mm filter as a collection medium. The results were as follows; 1. Among seven (7) commercially available filters tested for the FTIR-DOF method, the DM 800 filter showed the best analytical performance having the lowest background absorbance bands and no overlapping peaks at 799, 779, and $695cm^{-1}$. 2. The variations of absorbance due to humidity ranged from 1.0% to 3.3% for $799cm^{-1}$, 1.0% to 3.3% for $779cm^{-1}$, and 8.9%~20.9% for $695cm^{-1}$ peaks, respectively. The $699cm^{-1}$ peak was proved to be most vulnerble to environmental humidity for quantitative analysis of quartz. 3. As for effects of inhomogeneous deposition of samples, the highest variation of absorbance of 10.9% ($13.5{\mu}g$) was observed when using the 695cm-1. The variations of absorbance from the other two peaks, 799 and $779cm^{-1}$, ranged from 1.2 to 3.2%, and 1.4 to 4.1%, respectively. Therefore, the $799cm^{-1}$ peak was considered to be most reliable for quantitative analysis of quartz. The results of this study suggest that, for quantitative analysis of quartz in the respirable dust samples, use of the $799cm^{-1}$ peak can minimize the influence of environmental humidity and inhomogeneous deposition of particles on the filter. The FTIR-DOF method, if adopted for routine analysis of quartz in the respirable dust samples, could save sample preparation time and efforts substantially and also could increase analytical throughputs. Since use of the $799cm^{-1}$ peak is prone to be affected by interferences in the sample, further research on minimizing the effects is needed.

• Journal of Korean Ophthalmic Optics Society
• /
• v.20 no.4
• /
• pp.471-476
• /
• 2015

Purpose: We have analyzed the transmittance distribution of various ocular lenses using local transmittance microscope to investigate the optical homogeneity of the lens. Methods: The local transmittance of the laser which is focused on the surface of the spectacle lens was measured by using the photo-detector, lock-in amplifier and motorized-stage. 25 multi-coated lenses with non-tinted of 5 groups and 45 multicoated lenses with tinted of 9 groups were analyzed as a sample respectively. Results: Average and deviation of local transmittance for nontinted lenses were measured almost uniformly with various refractive index and coating. However, deviation of transmittance of for tinted lenses was analyzed as about 3.7 times larger than that of non-tinted lenses. Inhomogeneity of local transmittance of for tinted lenses was also analyzed as about 3.1 times larger than that of non-tinted lenses. Conclusions: We could analyze that standard deviation of transmittance and inhomogeneity of local transmittance of for tinted lenses is larger than that of non-tinted lenses using the local transmittance microscope. These analysis using local transmittance microscope can be utilized as a way to evaluate lens performance and improve optical homogeneity.

• Investigative Magnetic Resonance Imaging
• /
• v.19 no.3
• /
• pp.168-177
• /
• 2015

Purpose: Brain surface intensity model (BSIM)-based cortical thickness analysis does not require complicated 3D segmentation of brain gray/white matters. Instead, this technique uses the local intensity profile to compute cortical thickness. The aim of the present study was to evaluate intra-rater and inter-rater reliability of BSIM-based cortical thickness analysis using images from elderly participants. Materials and Methods: Fifteen healthy elderly participants (ages, 55-84 years) were included in this study. High-resolution 3D T1-spoiled gradient recalled-echo (SPGR) images were obtained using 3T MRI. BSIM-based processing steps included an inhomogeneity correction, intensity normalization, skull stripping, atlas registration, extraction of intensity profiles, and calculation of cortical thickness. Processing steps were automatic, with the exception of semiautomatic skull stripping. Individual cortical thicknesses were compared to a database indicating mean cortical thickness of healthy adults, in order to produce Z-score thinning maps. Intra-class correlation coefficients (ICCs) were calculated in order to evaluate inter-rater and intra-rater reliabilities. Results: ICCs for intra-rater reliability were excellent, ranging from 0.751-0.940 in brain regions except the right occipital, left anterior cingulate, and left and right cerebellum (ICCs = 0.65-0.741). Although ICCs for inter-rater reliability were fair to excellent in most regions, poor inter-rater correlations were observed for the cingulate and occipital regions. Processing time, including manual skull stripping, was $17.07{\pm}3.43min$. Z-score maps for all participants indicated that cortical thicknesses were not significantly different from those in the comparison databases of healthy adults. Conclusion: BSIM-based cortical thickness measurements provide acceptable intra-rater and inter-rater reliability. We therefore suggest BSIM-based cortical thickness analysis as an adjunct clinical tool to detect cortical atrophy.

• Progress in Medical Physics
• /
• v.28 no.1
• /
• pp.33-38
• /
• 2017

Creating individualized build-up material for superficial photon beam radiation therapy at irregular surface is complex with rice or commonly used flat shape bolus. In this study, we implemented a workflow using 3D printed patient specific bolus and describe our clinical experience. To provide better fitted build-up to irregular surface, the 3D printing technique was used. The PolyLactic Acid (PLA) which processed with nontoxic plant component was used for 3D printer filament material for clinical usage. The 3D printed bolus was designed using virtual bolus structure delineated on patient CT images. Dose distributions were generated from treatment plan for bolus assigned uniform relative electron density and bolus using relative electron density from CT image and compared to evaluate the inhomogeneity effect of bolus material. Pretreatment QA is performed to verify the relative electron density applied to bolus structure by gamma analysis. As an in-vivo dosimetry, Optically Stimulated Luminescent Dosimeters (OSLD) are used to measure the skin dose. The plan comparison result shows that discrepancies between the virtual bolus plan and printed bolus plan are negligible. (0.3% maximum dose difference and 0.2% mean dose difference). The dose distribution is evaluated with gamma method (2%, 2 mm) at the center of GTV and the passing rate was 99.6%. The OSLD measurement shows 0.3% to 2.1% higher than expected dose at patient treatment lesion. In this study, we treated Mycosis fungoides patient with patient specific bolus using 3D printing technique. The accuracy of treatment plan was verified by pretreatment QA and in-vivo dosimetry. The QA results and 4 month follow up result shows the radiation treatment using 3D printing bolus is feasible to treat irregular patient skin.

• Korean Journal of Materials Research
• /
• v.24 no.11
• /
• pp.585-590
• /
• 2014

Microstructural evolution in the thickness direction of an oxygen free copper processed by accumulative rollbonding (ARB) is investigated by electron back scatter diffraction (EBSD) measurement. For the ARB, two copper alloy sheets 1 mm thick, 30 mm wide and 300 mm long are first degreased and wire-brushed for sound bonding. The sheets are then stacked and roll-bonded by about 50% reduction rolling without lubrication at an ambient temperature. The bonded sheet is then cut to the two pieces of the same dimensions and the same procedure was repeated on the sheets up to eight cycles. The specimen after 1 cycle showed inhomogeneous microstructure in the thickness direction so that the grains near the surface were finer than those near the center. This inhomogeneity decreased with an increasing number of ARB cycles, and the grain sizes of the specimens after 3 cycles were almost identical. In addition, the aspect ratio of the grains decreased with an increasing number of ARB cycles due to the subdivision of the grains by shear deformation. The fraction of grains with high angle grain boundaries also increased with continuing process of the ARB so that it was higher than that of the low angle grain boundaries in specimens after 3 cycles. A discontinuous dynamic recrystallization occurred partially in specimens after 5 cycles.

• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.2 no.1
• /
• pp.51-59
• /
• 1992

Effect of agglomeration of $Nb_20_5$ of the same primary particle size on formation reaction and sintering of $Pb(Mg_{1/3}\;Nb_{2/3})O_3$ was examined. Both solid state reaction and molten salt synthesis were adopted. With decreasing agglomeration of $Nb_20_5$ increased the rate of formation reaction of perovskite PMN in solid state reaction, but had little influence in molten salt synthesis. It was concluded that the increase in the inhomogeneity of the dispersion state of intermediate pyrochlore with increasing agglomeration of $Nb_20_5$ retarded the formation reaction of perovskite PMN in solid state reaction, while had little influnce in molten salt synthesis due to its solution - precipitation mechanism -mainly depends on powder surface area.

• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.35 no.12
• /
• pp.1257-1264
• /
• 2011

This paper presents 3D simulation by STAR-CCM+ for lean premixed combustion in a stationary gas turbine combustor with separate pilot and main nozzles. The constant for the source term in the flame area density transport equation was modified to account for a low global equivalence ratio and validated against measurement data. A Partially-premixed Coherent Flame Model(PCFM) involves propagation of a laminar premixed flame with the predicted flame surface density and equilibrium assumption in the burned gas with spatial inhomogeneity. The conditions for cooling by radiation and convection are considered for accurate determination of the heat flux on the wall. A parametric study is of the pilot-fuel-to-total-fuel-ratio is carried out. A chemical reactor network (CRN) was constructed on the basis of the 3D simulation results and compared against measurements of NOx.

• Proceedings of the Earthquake Engineering Society of Korea Conference
• /
• 1998.10a
• /
• pp.210-221
• /
• 1998

In the period from the year 1500 to 1980. at least 14 large earthquake with epicenters in the northeastern China and Yellow Sea were felt or destructive in the Korean Peninsula. The most sigmificant events among them were the 1668 July 25 Tancheng earthquake of mamnitude 8.5, and the 1975 Feb. 4 Haicheng earthquake of magnitude 7.3. The Haicheng earthquake of the year 1975 in am extraordinary one among those occurred in the northeastern China in the 20th century in the sense the Shake of the event affected all over the Korean Peninsula. The tremor was felt even at the southeastern tip of the Korea and northern part of Kyushu 700km far away from the epicenter. In order to see the variation and trend of the effect of the Haicheng earthquake on the Korean Peninsula, the two data sets of the northern and southern parts of the peninsula were merged into one combined data set. The spatial variation of intensity shows smooth decrease from the value 4 of the northwestern region near the source to the value 1 of the Cheju Island and Kjushu. However, there are four regions of locally high intensity value. They are the region along downstream of Abrok(Yalu) River with intensity 5, the region around Shinpo of intensity 4, the area comprising Seoul and Chuncheon Cities of intensity 4, and Pohang-Pusan area of intensity 3. We suppose that there might be three types of possible mechanisms. The first one is concerned with the lateral inhomogeneity of velocity in the crust caused by wide distribution of relatively fractured rock. The second one is related with reflections of surface waves caused by the crestal thinning effect at border regions of the Peninsular in contact with the Ulleung Basin and the Japan Basin. The third possibility is local site effect caused by thick Tertiary or Quaternary rocks and soil layers.

• Korean Journal of Metals and Materials
• /
• v.49 no.6
• /
• pp.474-487
• /
• 2011

Bars of OFHC Cu with the diameter of 45 mm were processed by equal channel angular pressing up to 16 passes via route $B_c$, and homogeneity of their microstructures and mechanical properties was examined at every four passes which develop the equiaxed ultrafine grains. In general, overall hardness, yield strength and tensile strength increased by 3, 7, and 2 times respectively compared with those of unECAPed sample. Cross-sectional hardness exhibited a concentric distribution. Hardness was the highest at the center of bar and it decreased gradually from center to surface. After 16 passes, overall hardness decreased due to recovery and partial recrystallization. Regardless of the number of passage, yield strength and tensile strength were quite uniform at all positions, but elongation showed some degree of scattering. At 4 passes, coarse and ultrafine grains coexisted at all positions. After 4 passes, uniform equiaxed ultrafine grains were obtained at the center, while uniform elongated ultrafine grains were manifested at the upper half position. At the lower half position, grains were equiaxed but its size were inhomogeneous. It was found that inhomogeneity of grain morphology and grain size distribution at different positions are to be attributed to scattering in elongation but they did not affect strength. The present results reveal the high potential of practical application of equal channel angular pressing on fabrication of large-sized ultrafine grained bars with quite homogeneous mechanical properties.

• Journal of Korean Tunnelling and Underground Space Association
• /
• v.24 no.3
• /
• pp.231-245
• /
• 2022

When vertical shafts are constructed in soft clay with low strength, there is a risk of basal heave, which causes the excavation surface to heave due to the low bearing capacity of the ground against the imbalance of earth pressure at the excavation surface. Methods of deriving a safety factor have been proposed to evaluate the stability against the basal heave. However, there are limitations in that it is difficult to accurately evaluate the heave stability because many assumptions are included in the theoretical derivation. In this study, assuming that a circular vertical shaft is constructed in soft clay, the existing safety factor equation proposed through a theoretical approach was supplemented. Bearing capacity according to the shaft geometry, inhomogeneity of the soil, and the effect of soil plug were considered theoretically and applied in a previous safety factor equation. A three-dimensional numerical analysis was conducted to simulate the occurrence of basal heave and review the supplemented equation through various case studies. Several series of case studies were conducted targeting various factors affecting heave stability. It was verified that the additionally considered characteristics were properly reflected in the supplemented equation. Furthermore, the effects of each factor constituting the safety factor equation were examined using the results of the numerical analysis performed by simulating various cases. It was confirmed that considering the undrained shear strength increment according to depth had the most significant effect on the calculation of the safety factor.