• Proceedings of the KSME Conference
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• 2004.11a
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• pp.337-341
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• 2004

Bulk metallic glasses(BMG) with good mechanical properties have problems that engineering application fields have been limited because of limitation of the alloy size. In order to solving this problem, the friction welding of BMG has been tried using the superplastic-like deformation behavior under the supercooled liquid region. The apparatus for friction welding test was designed and constructed using pneumatic cylinder and gripper based on a conventional lathe. Friction welding have been tried to combination of same BMG alloy and crystalline alloys. The results of welding test were evaluated by X-ray diffraction, measurement of hardness and mechanical properties test. In order to obtain the optimized welding test conditions the temperature of friction interface was measured using Infrared thermal imager.

• Transactions of Materials Processing
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• v.11 no.3
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• pp.255-261
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• 2002

The grain size of 7010 Al alloy was refined to submicrometer level by using equal channel angular pressing (ECAP) and additional warm rolling. The mechanisms of grain refinement in ECAP process were fragmentation of coarse grain to ultra fine subgrains after a few passes and continuous recrystallization of the subgrains with the increase o( passes. Because of ultrafine grain size, essentially low temperature and high strain rate superplasticity was observed after ECAP process and warm rolling to form a sheet metal. The maximum elongation of 700% was obtained for an ECA pressed specimen after IS passes without warm rolling at $450^{\circ}C$ with strain rate of 5x$10^{-3}$/sec.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.05a
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• pp.80-83
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• 2004

High temperature deformation behavior of AZ31 Mg alloy was investigated in this study on the basis of a processing map $(\varepsilon\approx0.6)$. To construct a processing map, compression tests were carried out at wide range of temperatures and strain rates $(T=250\~500^{\circ}C,\;\varepsilon=10^{-4}\~100/s)$. Two regions of high deformation efficiency $(\eta)$ were identified as: (1) a dynamic recrystalization (DRX) domain at $250^{\circ}C$ and 1/s and (2) a superplasticity domain at $450^{\circ}C$ and $10^{-4}/s$. Possible deformation mechanisms operating at high temperature were discussed in relation to the activation energy. A two-stage deformation method was found to be effective in enhancing the superplasticity of AZ31 Mg alloy. From the two-stage deformation method, tensile elongation of $1200\%$ was obtained at the superplastic domain.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2006.05a
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• pp.67-69
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• 2006

Since magnesium alloy has a limited formability at room temperature, forming should be carried out at the elevated temperature. If the initial grain size is small, superplasticity could be expected over $400^{\circ}C$. Using superplastic behavior, blow forming can be used to overcome the low formability of Mg alloys. In the present study, the optimization of blow forming of AZ31 alloy at the elevated temperature was investigated. Finite element simulation was carried out and verified with the blow forming experiments.

• Transactions of the Korean Society of Mechanical Engineers
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• v.15 no.5
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• pp.1563-1571
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• 1991

본 연구에서는 가상일 원리로 부터 유한 요소 수식화를 updated-Lagrangian 형태로 유도하였으며, 유도된 수식화를 연속체 유한 요소로 유한 근사화 하였다. 이 때 초소성 재료의 거동은 비압축성, 비선형 점성 유ㄷ옹으로 묘사하였다. 유한 요소 프로그램은 성형 기구 해석과 하중 압력을 제어하는 기법으로 구성되어 있으며 하중 압력의 제어는 성형 시간이 최소가 되게 하기 위하여 변형률 속도 민감 계수가 최대가 되고, 국부 변형에 의한 두께 감소를 방지하며 변형률 속도는 일정하게 유지되면서 성 형이 될 수 있도록 하였다. 즉 하중 압력 제어는 상당 변형률 속도가 최대가 되게하 여 성형 시간을 최소화하게 구성하였다.개발된 유한 요소 프로그램은 정수압 벌징 가공에 적용하였으며 최적 압력 시간 선도, 성형 형상, 두께 및 두께 변형률 분포, 상 당 변형률 분포 등을 구하였다.

• Journal of the Korean Ceramic Society
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• v.46 no.4
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• pp.345-349
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• 2009

In Part II, the paper will describe a three-phase alumina-based nanoceramic composite demonstrating superplasticity at a surprisingly lower temperature and higher strain rate. One important factor in the processing of these nanocomposites was the use of the electrical field assisted sintering method, SPS. These improvements in mechanical properties were briefly discussed in the context of the results from the microstructural investigations. SPS forming approach provides a new route for low temperature and high-strain-rate superplasticity for nanostructured materials and should impact and interest a broad range of scientists in materials research and superplastic forming technology.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.1292-1293
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• 2006

A non-equilibrium powder metallurgy processing such as an MA/SPS (Mechanical Alloying / Spark Plasma Sintering) process is examined in a Ti-48moll%Al. TiAl intermetallic compound is a potential light-weight/high-temperature structural material. One of the major problems, however, limiting the practical use of the material is its poor workability. From this point, the powder metallurgy (PM) processing route has been attractive alternative of the conventional processing for such material The MA/SPS process is able to apply to a LIGA process. Optimization of the pseudo-superplasticity enables to fabricate micro-parts made of fine grained ceramics composites of TiAl by the LIGA process.

• Journal of the Korean institute of surface engineering
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• v.32 no.3
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• pp.356-359
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• 1999

To obtain a biomaterial that has both biological affinity and high mechanical strength, hydroxyapatite granules were implanted into the surface of pure titanium film coated titanium alloy. The film was coated by reactive DC sputtering method on the alloy substrate. Hydroxyapatite granules (32- $38\mu\textrm{m}$ in diameter)were spread over titanium alloy substrate and pressed to implant the granules in the substrate. They can be implanted into substrate under 17MPa at $800^{\circ}C$ for 10minutes. The only tops of the granules were exposed and they were firmly stuck in substrate. The hydroxyapatite implanted titanium alloy composites were expected to be useful for biomaterials as artificial bones and dental roots.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.25 no.12
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• pp.1933-1943
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• 2001

A micromechanical model is presented for superplasticity in which heterogeneous microstructures are coupled with deformation behavior. The effects of initial distributions of grain size, and their evolutions on the mechanical properties can be predicted by the model. Alternative stress rate models such as Jaumann rate and rotation incremental rate have been employed to analyze uniaxial loading and simple shear problems and the appropriate modeling was studied on the basis of hypoelasticity and elasto-viscoplasticity. The model has been implemented into finite element software so that full process simulation can be carried out. Tests have been conducted on Ti-6Al-4V alloy and the microstructural features such as grain size, distributions of grain size, and volume fraction of each phase were examined for the materials that were tested at different strain rates. The experimentally observed stress-strain behavior on a range of initial grain size distributions has been shown to be correctly predicted. In addition, the effect of volume fraction of the phases and concurrent grain growth were analyzed. The dependence of failure strain on strain rate has been explained in terms of the change in mechanism of grain growth that occurs with changing strain rate.

• Journal of Powder Materials
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• v.3 no.4
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• pp.271-278
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• 1996

In this study, the effect of the transition elements on the microstructure and mechanical properties of rapidly solidified Al-Mg-X alloys was investigated. As a result of the rapid solidification processing, fine equiaxed grains with a mean diameter of 2 $\mu$m were observed in these alloys. Many fine particles were found to be distributed rather homogeneously throughout the matrix with relatively large particles occasionally at grain boundaries. The ultimate tensile strengths of Al-Mg-X alloys were found to decrease rather remarkably at 150 $^{\circ}C$ without the gain of the ductility at 150 $^{\circ}C$, which may result from segregation of $\beta$ ($Al_{3}Mg_{2}$) precipitates. Fine dimples were observed on the fracture surfaces for all alloy systems and the variation of the size and shape of dimples was not observed upon alloy systems. The ductility at 530 $^{\circ}C$ was found to be ~100%, suggesting that grain boundary sliding did not contribute to ductiliy despite he grain size stabilization. The absence of superplastic behavior may be associated with low boundary misorientation in rapidly solidified Al-Mg-X alloys.