• Title/Summary/Keyword: sub-atmosphere

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Microstructural Characteristics of Al2O3/Cu Nanocomposites Depending on Fabrication Process (Al2O3/Cu 나노복합체 제조공정에 따른 미세조직 특성)

  • Kang, Kae-Myung;Oh, Sung-Tag
    • Korean Journal of Materials Research
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    • v.13 no.1
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    • pp.59-63
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    • 2003
  • The microstructural characteristics of $Al_2$$O_3$/Cu composites hot-pressed at different temperatures for atmosphere switching from $H_2$to Ar have been studied. When the composite atmosphere was switched at $1000^{\circ}C$ it led to more homogeneous microstructure than when the atmosphere was switched at $1450^{\circ}C$. The strong sensitivity of Cu to atmosphere, especially the oxygen content in the atmosphere, was found to be responsible for the observed change, based upon the interfacial phenomena related to the formation of $CuAlO_2$. The practical implication of these results is that an optimum processing condition for the design of homogeneous microstructure and stable properties can be established.

Effect of Sintering Atmosphere Changing Temperature on Microstructure and Mechanical Property of Al2O3/Cu Nanocomposites (소결분위기 변환온도가 Al2O3/Cu 나노복합재료의 미세조직과 파괴강도에 미치는 영향)

  • Oh Sung-Tag;Yoon Se-Joong
    • Journal of Powder Materials
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    • v.11 no.5
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    • pp.421-426
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    • 2004
  • The microstructure and mechanical property of hot-pressed $Al_2O_3/Cu$ composites with a different temperature for atmosphere changing from H$_{2}$ to Ar have been studied. When atmosphere-changed from H$_{2}$ to Ar gas at 145$0^{\circ}C$, the hot-pressed composite was characterized by inhomogeneous microstructure and low fracture strength. On the contrary, when atmosphere-changed at low temperature of 110$0^{\circ}C$ the composite showed more homogeneous microstructure, higher fracture strength and smaller deviation in strength. Based on the thermodynamic consideration and microstructural analysis, it was interpreted that the Cu wetting behavior relating to the formation of CuAlO$_{2}$ is probably responsible for strong dependence of microstructure on atmosphere changing temperature. The reason for a strong sensitivity of fracture strength and especially of its deviation to atmosphere changing temperature was explained by the microstructural inhomogeneity and by the role of CuAlO$_{2}$ phase on the interfacial bonding strength.

Nitrogen Doping in Polycrystalline Anatase TiO2 Ceramics by Atmosphere Controlled Firing

  • Chang, Myung Chul
    • Journal of the Korean Ceramic Society
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    • v.56 no.4
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    • pp.374-386
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    • 2019
  • A process for nitrogen doping of TiO2 ceramics was developed, whereby polycrystalline titania particles were prepared at 450-1000℃ with variation of the firing schedule under N2 atmosphere. The effect of nitrogen doping on the polycrystallites was investigated by X-ray diffraction (XRD) and Raman analysis. The microstructure of the TiO2 ceramics changed with variation of the firing temperature and the firing atmosphere (N2 or O2). The microstructural changes in the nitrogen-doped TiO2 ceramics were closely related to changes in the Raman spectra. Within the evaluated temperature range, the nitrogen-doped titania ceramics comprised anatase and/or rutile phases, similar to those of titania ceramics fired in air. Infiltration of nitrogen gas into the titania ceramics was analyzed by Raman spectroscopy and XRD analysis, showing a considerable change in the profiles of the N2-doped TiO2 ceramics compared with those of the TiO2 ceramics fired under O2 atmosphere. The nitrogen doping in the anatase phase may produce active sites for photocatalysis in the visible and ultraviolet regions.

Quality Characteristics of Pork Belly Meat Stored in a Container Automatically Controlled under High CO2 Atmosphere (고 CO2농도 기체조성으로 자동제어된 용기에 저장된 삼겹살의 품질특성)

  • Soo Yeon, Jung;Dong Sun, Lee;Duck Soon, An
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.28 no.3
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    • pp.217-221
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    • 2022
  • Container system automatically controlled in its atmosphere of high CO2/low O2 was devised to contain and store pork belly meat at chilled temperature. The meat in the container system was compared in the quality preservation at 0℃ for 21 days to that in air-filled container and vacuum package. The container atmosphere could be controlled to be of 47~60% CO2 and 7~10% O2 through time-controlled intermittent CO2 injection. The controlled atmosphere in the developed system was effective in suppressing pH change and aerobic bacterial growth contributing to sensory quality preservation. Compared to control of air-filled container, vacuum packaging showed lower microbial growth and slower pH change on the meat but with high drip loss. The devised container system to keep high CO2 and mildly low O2 concentrations is effective in the meat quality preservation on overall, and may be extended to a variety of meat products with possible modification tuned for product requirements.

Analysis of Correlation between Particulate Matter in the Atmosphere and Rainwater Quality During Spring and Summer of 2020 (봄·여름철 대기 중 미세먼지와 빗물 수질 상관성 분석)

  • Park, Hyemin;Kim, Taeyong;Heo, Junyong;Yang, Minjune
    • Korean Journal of Remote Sensing
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    • v.37 no.6_2
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    • pp.1859-1867
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    • 2021
  • This study investigated seasonal characteristics of the particulate matter (PM) in the atmosphere and rainwater quality in Busan, South Korea, and evaluated the seasonal effect of PM10 concentration in the atmosphere on the rainwater quality using multivariate statistical analysis. The concentration of PM in the atmosphere and meteorological observations(daily precipitation amount and rainfall intensity) are obtained from automatic weather systems (AWS) by the Korea Meteorological Administration (KMA) from March 2020 to August 2020. Rainwater samples (n = 216, 13 rain events) were continuously collected from the beginning of the precipitation using the rainwater collecting device at Pukyong National University. The samples were analyzed for pH, EC (electrical conductivity), water-soluble cations(Na+, Mg2+, K+, Ca2+, and NH4+), and anions(Cl-, NO3-, and SO42-). The concentration of PM10 in the atmosphere was steadily measured before and after the precipitation with a custom-built PM sensor node. The measured data were analyzed using principal component analysis (PCA) and Pearson correlation analysis to identify relationships between the concentration of PM10 in the atmosphere and rainwater quality. In spring, the daily average concentration of PM10 (34.11 ㎍/m3) and PM2.5 (19.23 ㎍/m3) in the atmosphere were relatively high, while the value of daily precipitation amount and rainfall intensity were relatively low. In addition, the concentration of PM10 in the atmosphere showed a significant positive correlation with the concentration of water-soluble ions (r = 0.99) and EC (r = 0.95) and a negative correlation with the pH (r = -0.84) of rainwater samples. In summer, the daily average concentration of PM10 (27.79 ㎍/m3) and PM2.5 (17.41 ㎍/m3) in the atmosphere were relatively low, and the maximum rainfall intensity was 81.6 mm/h, recording a large amount of rain for a long time. The results indicated that there was no statistically significant correlation between the concentration of PM10 in the atmosphere and rainwater quality in summer.

Distribution Characteristics and Background Air Classification of PM2.5 OC and EC in Summer Monsoon Season at the Anmyeondo Global Atmosphere Watch (GAW) Regional Station (안면도 기후변화감시소의 여름철 PM2.5 OC와 EC 분포 특성 및 배경대기 구분)

  • Ham, Jeeyoung;Lee, Meehye;Ryoo, Sang-Boom;Lee, Young-Gon
    • Atmosphere
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    • v.29 no.4
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    • pp.429-438
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    • 2019
  • Organic carbon (OC) and elemental carbon (EC) in PM2.5 were measured with Sunset Laboratory Model-5 Semi-Continuous OC/EC Field Analyzer by NIOSH/TOT method at Anmyeondo Global Atmosphere Watch (GAW) Regional Station (37°32'N, 127°19'E) in July and August, 2017. The mean values of OC and EC were 3.7 ㎍ m-3 and 0.7 ㎍ m-3, respectively. During the study period, the concentrations of reactive gases and aerosol compositions were evidently lower than those of other seasons. It is mostly due to meteorological setting of the northeast Asia, where the influence of continental outflow is at its minimum during this season under southwesterly wind. While the diurnal variation of OC and EC were not clear, the concentrations of O3, CO, NOx, EC, and OC were evidently enhanced under easterly wind at night from 20:00 to 8:00. However, the high concentration of EC was observed concurrently with CO and NOx under northerly wind during 20:00~24:00. It indicates the influence of thermal power plant and industrial facilities, which was recognized as a major emission source during KORUS-AQ campaign. The diurnal variations of pollutants clearly showed the influence of land-sea breeze, in which OC showed good correlation between EC and O3 in seabreeze. It is estimated to be the recirculation of pollutants in land-sea breeze cycle. This study suggests that in general, Anmyeondo station serves well as a background monitoring station. However, the variation in meteorological condition is so dynamic that it is primary factor to determine the concentrations of secondary species as well as primary pollutants at Anmyeondo station.

Salting of Chinese Cabbage under Sub-atmosphere (감압하에서 배추의 소금절임)

  • 정자림;김미정;김순동
    • Journal of the East Asian Society of Dietary Life
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    • v.3 no.2
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    • pp.99-106
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    • 1993
  • The aim of this study is to elevate the efficiency of salting with low salt concentration in order to improve the quality of salted Chinese cabbage. The efficiency of salting was tested with various sub-atmosphere(760mmHg to 0mmHg), temperature(20$^{\circ}C$ and 30$^{\circ}C$), and concentration of salt(3%, 5% and 10%). The salting efficiency was estimated by amounts of juice, calcium elution, sodium penetration and the state of tissue. The amunts of juice eleuted from Chinese cabbage was increased significantly with the decrease of atmosphere and the time to reach the highest amounts was reduced. This tendency was promoted, with increase of salinigy(from 3% to 10%)and the increase of temperature(more juice at 30$^{\circ}C$ than 20$^{\circ}C$). The amounts of eluted calcium from Chinese cabbage tissue during salting under sub-atmosphere was directly proportional to amounts of juice and was inversely proportional to penetrated sodium. The salting time was reduced with elevation of sub-atmosphere. It was desirable to take between 5.5 and 9 hours to salt under the condition of 3% of salting, 20$^{\circ}C$, and 560-0mmHg. It took between 4.4 and 5 hours under 5% of salt and between 4 and 4.5 hours under 10% of salt. However, it was undesirable because the drying phenomenon and the transparency of tissue appeared under 30$^{\circ}C$ and 160-0mmHg.

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Analysis on Vertical Structure of Sea Fog in the West Coast of the Korean Peninsula by Using Drone (드론을 활용한 한반도 서해 연안의 해무 연직구조 분석)

  • Jeon, Hye-Rim;Park, Mi Eun;Lee, Seung Hyeop;Park, Mir;Lee, Yong Hee
    • Atmosphere
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    • v.32 no.4
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    • pp.307-322
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    • 2022
  • A drone has recently got attention as an instrument for weather observation in lower atmosphere because it can produce the high spatiotemporal resolution weather data even though the weather phenomenon is inaccessible. Sea fog is a weather phenomenon occurred in lower atmosphere, and has observational limitations because it occurs on the sea. Therefore, goal of this study is to analyze the vertical structures about inflow, development and dispersion of sea fog using the high-resolution weather data with the meteorological sensor-equipped drone. This study observed sea fogs in the west coast of the Korean peninsula from March to October 2021 and investigated one sea fog inflowed into the coast on June 8th 2021. θe - qv diagrams (θe: equivalent potential temperature, qv: water vapor ratio) and vertical wind structures were analyzed. At inflow of sea fog, moist adiabatically stable layer was formed in 0-300 m and prevailing wind was switched from south-southwesterly to west-southwesterly under 120 m. Both changes are favorable for sea fog on the location. θe and qv plummeted in a layer 0-183 m. The inflowed sea fog developed from 183 m to 327 m by mixing with ambient atmosphere on top of sea fog. Also, strong mechanical turbulence near ground drove a vertical mixing under stable layer. At dispersion of sea fog, as θe on ground gradually increased, air condition was changed to neutral. Evaporation occurred on both bottom and top in sea fog. These results induced dissipation of sea fog.

Antioxidant Packaging as Additional Measure to Augment CO2-enriched Modified Atmosphere Packaging for Preserving Infant Formula Powder

  • Jo, Min Gyeong;An, Duck Soon;Lee, Dong Sun
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.26 no.1
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    • pp.19-23
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    • 2020
  • Al-laminated packaging film incorporating ascorbic acid or tocopherol at inner food contact layer was tested in the potential to improve antioxidative preservation of powdered infant formula under CO2-enriched atmosphere. Product of 200 g was packaged with the packaging film containing 0.3% antioxidant in sealant layer of low density polyethylene and stored at 30℃ for 286 days with periodic measurement of package atmosphere and product's quality attributes. The CO2-flushed package resulted in shrinkage of tight contact between the product and the film not allowing gas sampling of package atmosphere after 140 days. Package of tocopherol-incorporated film allowed some ingress of oxygen after 112 days presumably due to its weakening of heat-seal area. The increased oxygen concentration in the tocopherol-added film package led to the concomitant increase of peroxide value, an index of lipid oxidation. On the other hand, packaging of ascorbic acid-added film pouch could suppress lipid oxidation marginally in consistent manner compared to control package without any antioxidant.

Kimchi Fermentation and Heat Treatment under Sub-atmosphere (감압하에서의 김치숙성과 열처리)

  • 정자림;김미향;김미정;장경숙;김순동
    • Journal of the East Asian Society of Dietary Life
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    • v.4 no.1
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    • pp.95-104
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    • 1994
  • This study was carried out to investigate the effect of sub-atmosphere on the fermentation and heat treatment after fermentation of Kimchi. When the results from the conditions of atmosphere and under-atmosphere were compared, the growth of lactic acid bacteria was increased but the growth of aerobic bacteria was decreased under 560mmHg and 360mmHg. The number of total microorganism was decreased and simultaneously damaged to the tissue of Kimchi under 0mmHg. Kimchi fermented under 560mmHg and 360mmHg had longer storage duration than that of atmosphere. Among the several conditions, the result of heat treatment under 460-260mmHg was the best. the treatment for 4 minutes at 80$^{\circ}C$, 2 minutes at 100$^{\circ}C$, and 1 minute at 120$^{\circ}C$ was good in tissue states and storage.

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