• Title/Summary/Keyword: steel specimen

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HAZ TOUGHNESS AND MICROSTRUCTURE IN HIGH NITROGEN AUSTENITIC STAINLESS STEEL

  • Sato, Yoshihiro;Shiotsu, Tomoya;Nakagawa, Takafumi;Kikuchi, Yasushi
    • Proceedings of the KWS Conference
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    • 2002.10a
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    • pp.38-42
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    • 2002
  • HAZ(Heat Affected Zone of weldm ents) properties were investigated for a high nitrogen austenitic stainless steel with a chemical composition of Fe-0.02C-0.15Si-6.00Mn-10.0Ni-23.0Cr-2.00Mo-0.48N-0.14V. Thermal cycle of HAZ was simulated by the thermal cycle simulator (Gleeble 1500). The heat treatment was applied to the Charpy test size sample without notch under various peak temperatures and/or the holding times condition. V-notch Charpy test was performed at the temperature range of 273~77 K. Metallographic examination also was carried out by using optical microscopy, scanning electron microscopy and transmission electron microscopy. The simulated specimens revealed a slight embrittlement compared with the base materials. The impact toughness of the specimens deteriorated with the decreasing test temperature. The results from Charpy V-notch test, however, showed that significant degradation of absorbed energy caused by brittle fracture was not observed for the specimen tested in the test temperature range.

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Characteristic Evaluation according to Heat Treatment Conditions of Super Duplex Stainless Steel with Additive 0.2% N - Part 2: Fatigue Crack Propagation Behavior (0.2% N을 첨가한 수퍼 2상 스테인리스강의 열처리 조건에 따른 특성 평가 - 제2보: 피로균열진전 거동)

  • Ahn, Seok-Hwan;Kang, Heung-Joo;Seo, Hyun-Soo;Nam, Ki-Woo;Lee, Kun-Chan
    • Journal of Ocean Engineering and Technology
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    • v.23 no.5
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    • pp.79-84
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    • 2009
  • Super duplex stainless steel has long life in severe environments by showing the enough strength and corrosion resistance. Therefore, the fracture mechanics approach needs to support the structural strength integrity for the used material. In this study, fatigue crack propagation behavior was investigated to super duplex stainless steel with 0.2% nitrogen. The various volume fraction and distribution of austenite structure for applied specimen in test were obtained by changing the heat treatment temperature and cycle. From test results, fatigue crack propagation rate showed two kinds of tendency between da/dN and ${\Delta}K$ according to distribution of austenite structure and structure anisotropy.

Influence of coarse aggregate properties on specific fracture energy of steel fiber reinforced self compacting concrete

  • Raja Rajeshwari, B.;Sivakumar, M.V.N.
    • Advances in concrete construction
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    • v.9 no.2
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    • pp.173-181
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    • 2020
  • Fracture properties of concrete depend on the mix proportions of the ingredients, specimen shape and size, type of testing method used for the evaluation of fracture properties. Aggregates play a key role for changes in the fracture behaviour of concrete as they constitute about 60-75 % of the total volume of the concrete. The present study deals with the effect of size and quantity of coarse aggregate on the fracture behaviour of steel fibre reinforced self compacting concrete (SFRSCC). Lower coarse aggregate and higher fine aggregate content in SCC results in the stronger interfacial transition zone and a weaker stiffness of concrete compared to vibrated concrete. As the fracture properties depend on the aggregates quantity and size particularly in SCC, three nominal sizes (20 mm, 16 mm and 12.5 mm) and three coarse to fine aggregate proportions (50-50, 45-55, 40-60) were chosen as parameters. Wedge Split Test (WST), a stable test method was adopted to arrive the requisite properties. Specimens without and with guide notch were investigated. The results are indicative of increase in fracture energy with increase in coarse aggregate size and quantity. The splitting force was maximum for specimens with 12.5 mm size which is associated with a brittle failure in the pre-ultimate stage followed by a ductile failure due to the presence of steel fibres in the post-peak stage.

A Study on the Radiograph Inspection of Specimen in Welding Pass Using ATOS 80 High-strength Steel (ATOS 80 고장력강의 용접 패스에 따른 용접부 방사선검사에 관한 연구)

  • Baek, Jung-Hwan;Choi, Byung-Ky
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.21 no.6
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    • pp.915-919
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    • 2012
  • In constructing all kinds of equipment and steel structure, parts with discontinuities such as weld defects formed in the welded structure can generate fatigue cracks that results in damage or accidents. In this study, weld zones are investigated with X-rays and the latent images are put on film. Weld zone defects can be verified by developing the film. As weld defects are investigated by radiographic testing and correlated with the welding condition, more appropriate welding conditions can be found. According to the result of X-ray radiographic inspection of butt welding ATOS 80 high-strength steel with a thickness of 12mm, the best conditions for welding without creating weld defects are 4 weld-passes, a protective gas of 20% $CO_2$ and 80% Ar, a protective gas flow of 20L/min, a welding current of 200A, an arc voltage of 24V, a welding speed of 14.4cm/min, a welding rod angle of $50^{\circ}$, a welding gap of 5 mm with a ceramic base, and sand pre-heating to $160^{\circ}$ Celsius prior to welding.

The Effect of Tempering Temperature on Ultrasonic Velocity Property at the Quenched SCM 440 Steel (퀜칭한 SCM 440 강에서 초음파 전파특성에 미치는 템퍼링온도의 영향)

  • Lee, K.W.;Kim, M.I.;Park, U.S.
    • Journal of the Korean Society for Heat Treatment
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    • v.4 no.3
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    • pp.54-62
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    • 1991
  • The effect of tempering temperature on the ultrasonic propagation velocity at SCM 440 steel quenched from $870^{\circ}C$ and $1000^{\circ}C$ has been studied by metallurgical and crystallographical observation. The measurements of ultrasonic velocity were made on the specimen by appling an immersion ultrasonic pulse-echo technique with a constant frequency of 10 MHz. The quenched microstructure of this steel was a lath martensite. As the tempering temperature was increased, the martensite was transformed into the tempered martensite composed of cementite and carbide. The ultrasonic velocity increased with increasing the tempering temperature. It was thought that these were resulted from the microstructural transformation. The change of ultrasonic propagation velocity with quenching and tempering heat treatment was resulted from microstrain due to the change of internal stress. Considering these results concerning to the change of ultrasonic propagation velocity. the phenomena of microstructural transformation were estimated. Consequently, it was thought that the degree of quenching and tempered heat treatment of steel could be nondestructively evaluated with the change of ultrasonic propagation velocity.

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Effect of Microstructure on Fracture Behavior of Multi-phase Low-density Steel (다상계 저비중강의 파괴거동에 미치는 미세조직의 영향)

  • Shin, Sun-Kyoung;Park, Seong-Jun;Cho, Kyung Mox
    • Journal of the Korean Society for Heat Treatment
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    • v.26 no.6
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    • pp.306-316
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    • 2013
  • Microstructure and fracture behavior of a multi-phase low-density steel were investigated. After hot-rolling and heat treatment, the microstructure of low-density steel was composed of coarse ferrite grains and elongated bands which include second phases such as austenite, martensite and ${\kappa}$-carbide depending on holding time during isothermal heat treatment. After tensile test, microcracks were observed at martensite or ${\kappa}$-carbide interface in the elongated bands. Coarse ferrite grains showed cleavage fracture behavior regardless of second phase. The cleavage fracture of ferrite could be attributed to their coarse grain size and solute atoms that increase ductile-to-brittle transition temperature of ferrite. Despite of the tendency of cleavage fracture in coarse ferrite grains, a specimen having coarse spheroidized ${\kappa}$-carbide particles in the elongated bands showed high total elongation of 30%. Thus, the easiness of plastic deformation in the elongated band seems to play an important role in retardation of cleavage crack formation in coarse ferrite grains.

A Study on the Measurement of Residual Stress in Rolled Steel for Automobile using X-ray Diffraction (X선 회절을 이용한 자동차 압연강의 잔류응력 측정에 관한 연구)

  • 홍순혁;이동우;조석수;주원식
    • Transactions of the Korean Society of Automotive Engineers
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    • v.10 no.6
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    • pp.150-157
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    • 2002
  • In textured material, diffraction angle $2{\theta}$ usually shows a nonlinear relation against $sin^2{\psi}$ due to elastic anisotropy of crystals. SPHD and SPCD steel is cold-rolled carbon steel for automobile. The characteristics X-ray for stress measurement is Cr $K_{\alpha}\;and\;Mo\;K_{\alpha}$ characteristic X-ray. The $2{\theta}-sin^2{\psi}$ diagram under elastic strain seems to have a linear behavior using regression line of data but has a nonlinear behavior in distribution of data by Cr $K_{\alpha}$ characteristic X-ray. As the plastic strain of specimen increases, the nonlinearity of $2{\theta}$ with respect to $sin^2{\psi}$ increases remarkably. On the other hand, the diffraction angle $2{\theta}$ by Mo $K_{\alpha}$ characteristic X-ray shows a good linearity on $2{\theta}-sin^2{\psi}$ diagram under plastic strain as well as elastic strain. Therefore, this paper presents the measurement of residual stress in cold-rolled carbon steel for automobile using penetration depth of Mo $K_{\alpha1}$ characteristic X-ray and multiplicity factor of crystal diffraction plane.

Effect of Prior Structure on Torsional Fatigue Strength of Induction Surface Hardened Medium Carbon Steel (고주파 표면경화된 중탄소강의 비틀림 피로강도에 미치는 초기조직의 영향)

  • Kim, Heung-Jip;Chung, In-Sang
    • Journal of the Korean Society for Heat Treatment
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    • v.11 no.4
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    • pp.247-257
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    • 1998
  • In order to evaluate the relation between prior structure and fatigue strength on a induction surface hardened medium carbon steel(SAE1050M) for automotive drive shafts, torsional fatigue test were conducted with various cases of different hardened depths and applied loads. Prior structures of the steel such as pearlite, fine pearlite and spheroidal pearlite were prepared by conventional nomalizing, tempering after quenching and spheroidized annealing, respectively. Maximum torsional fatigue strength can be obtained when the case depth is 18~25% diameter of the bar in each prior structure. The effect of case depth on the torsional fatigue strength was different depending on applied load to specimen, but the most good fatigue life was shown in the case of pearlitic structure when the case depth was 4.0~5.5mm(18~25% of bar diameter). Among three different prior structures, energy consumption, to obtain high strength or to get the same case depth, was the most saved in the case of pearlitic structure.

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Influence of Phase Evolution and Texture on the Corrosion Resistance of Nitrogen Ion Implanted STS 316L Stainless Steel (질소 이온이 주입된 STS 316L 스테인리스 강에서의 상변화와 집합조직이 내식성에 미치는 영향)

  • Jun, Shinhee;Kong, Young-Min
    • Korean Journal of Materials Research
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    • v.25 no.6
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    • pp.293-299
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    • 2015
  • In this study, nitrogen ions were implanted into STS 316L austenitic stainless steel by plasma immersion ion implantation (PIII) to improve the corrosion resistance. The implantation of nitrogen ions was performed with bias voltages of -5, -10, -15, and -20 kV. The implantation time was 240 min and the implantation temperature was kept at room temperature. With nitrogen implantation, the corrosion resistance of 316 L improved in comparison with that of the bare steel. The effects of nitrogen ion implantation on the electrochemical corrosion behavior of the specimen were investigated by the potentiodynamic polarization test, which was conducted in a 0.5 M $H_2SO_4$ solution at $70^{\circ}C$. The phase evolution and texture caused by the nitrogen ion implantation were analyzed by an X-ray diffractometer. It was demonstrated that the samples implanted at lower bias voltages, i.e., 5 kV and 10 kV, showed an expanded austenite phase, ${\gamma}_N$, and strong (111) texture morphology. Those samples exhibited a better corrosion resistance.

An Electrochemical Study on the Effect of Salt Affecting to Corrosion Behavior of Concrete Reinforced Steel in Natural Sea Water (천연해수에 침지된 콘크리트 내부의 철근부식거동에 미치는 염분의 영향에 관한 전기화학적 연구)

  • 김광근;류보현;점성종;김기준;문경만
    • Journal of Ocean Engineering and Technology
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    • v.14 no.4
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    • pp.23-29
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    • 2000
  • When the concrete structures were being made with sand containing chloride ion it was knows that corrosion rate of reinforced steel embedded in concrete with chloride ion was higher than that of concrete with on chloride ion. In this study, the operation of Friedel salts affecting the corrosion behavior of reinforced steel embedded in cement mortar was investigated with electrochemical view. Corrosion potential of reinforced steel embedded in cement mortar with sand containing chloride ion was shifted noble direction than that of cement mortar with no chloride ion after immersed 5 month in natural sea water and also corrosion current density decreased with shifting corrosion potential to noble direction. However Friedel salts appeared from surface to 2.5cm of inside direction of mortar specimen, which is located at 11.5$\circ$(2$\theta$) in XRD analysis and the amount of Ca(OH)2 by SEM photograph in cement mortar with chloride ion was larger than that of cement mortar with mo chloride ion. Eventually it is suggested that Friedel salts was resulted from chloride ion and it acted as the corrosion inhibitor.

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