• Title/Summary/Keyword: standard reference materials

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Evaluation of proficiency and improvement of accuracy on the analysis of brominated flame retardants (PBDEs) in ABS polymer (ABS수지 중 polybrominated diphenyl ether(PBDE)류 분석 숙련도 평가 및 정확도 향상)

  • Ryu, Jehoon;Kim, Dalho
    • Analytical Science and Technology
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    • v.28 no.6
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    • pp.446-452
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    • 2015
  • In order to evaluate and improve the ability of Korean testing laboratories to measure Polybrominated diphenyl ethers in acrylonitrile-butadiene-styrene (ABS), a proficiency test was organised by Korea Research Institute of Standards and Science (KRISS) based on ISO/IEC 17043. The proficiency test material used was 10 g of a granular ABS fortified with a mixture of congeners of PBDE (BDE-154, 183, 206, 209). Homogeneity and stability were investigated to assess the adequacy of the test material. The certified value established by KRISS based on the national reference was used for assigned value of each PBDE. The test materials were distributed to the 16 participating laboratories. The participating laboratories were requested to analyse the samples employing the methods used in their routine analysis. Each laboratory was given it’s own code to secure the anonymity. Participants results were evaluated with z-scores according to ISO/IEC 17043. The standard deviation for proficiency assessment was set by standard deviation of the participants results except for outlier. The results, the laboratory's performance and improvement of accuracy were discussed.

Phytoplankton as Standard Test Species for Marine Ecotoxicological Evaluation (해양생태독성평가를 위한 표준시험생물로서의 식물플랑크톤에 관한 연구)

  • Park Gyung-Soo;Lee Sang-Hee;Lee Seung-Min
    • Journal of Environmental Science International
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    • v.14 no.12
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    • pp.1129-1139
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    • 2005
  • A series of experiments was conducted to identify the potential of five phytoplankton species as standard test species for marine ecotoxicological tests. The candidate phytoplankton species are Skeletonema costatum, Heterosigma akashiwo, Prorocentrum micans, Isochrysis galbana, and Tetraselmis suecica. Salinity tolerance and sensitivity on potassium dichromate as a reference material were identified. Toxicity of eleven ocean dumped sewage sludges and four red tide expellent extracts were estimated by the inhibition of population growth rates (PGR) of marine diatom S. costatum, While most species revealed relatively weak tolerance on salinity, T. suecica demonstrated the highest salinity tolerance ranged from $5\~35$ psu and the others $15\~35$ psu. H. akashiwo revealed the highest sensitivity as 72h $IC_{50}$=0.76mg/L and T. suecica the lowest as 72h $IC_{50}$=8.89mg/L on potassium dichromate. Sludge extracts from industrial waste, domestic sewage and livestock farm waste sludge showed high toxicity as 72h $IC_{50}$<$2\%$ and lowest toxicity from filtration bed sludge as 72h $IC_{50}$=$30.50\%$ NOEC (No Observed Effective Concentration) of sludge extract ranged from <$0.4\%$ to $1.6\%$ and this indicated high phytotoxicity of ocean dumped sewage sludge. The test sensitivity of phytoplankton PGR inhibition was much higher than those of marine rotifer Brachionus plicatilis mortality test and bioluminescent inhibition test by marine bacteria Vibrio fischeri, and comparable with the sea urchin (Strongylocentrotus intermedius) fertilization test. As a result the phytotoxicity test using phytoplankton PGR inhibition ($IC_{50}$) must be a useful tool for marine phyto-toxicological evaluation of ocean dumped materials.

Study on Airborne Particulate Matter ($PM_{10}$) Monitoring in Urban and Rural Area by Using Gent SFU Sampler and Instrumental Neutron Activation Analysis (중성자 방사화분석법과 Gent SFU 샘플러를 이용한 도시의 농촌지역의 대기분지($PM_{10}$)관측 연구)

  • 정용삼;문종화;김선하;박광원;강상훈
    • Journal of Korean Society for Atmospheric Environment
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    • v.16 no.5
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    • pp.453-467
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    • 2000
  • The aim of this research is to collect and characterize fine particles (FPM:$\leq$2.5${\mu}{\textrm}{m}$) and coarse particles (CPM: 2.5~10${\mu}{\textrm}{m}$) using a low volume air sampler provided by the IAEA, at urban (Taejon) and rural area(Wonju) for a period of about two years(April 1996 to May 1998) and to promote a use of nuclear analytical techniques for air pollution studies. For the collection of airborne particulate matter (PM(sub)10), the Gent stacked filter unit sampler and polycarbonate membrane filters were employed. The concentration of trace elements in collected APM samples were determined byu instrumental Neutron Activation Analysis. For validation of the analytical data, internal quality control were implemented by using both the comparison of the analytical results of standard reference materials(NIST SRM 1648) and interlaboratory comparison for proficiency test (NAT-3). The standard uncertainty was less than 15% and Z-score of two samples were within $\pm$1. The monitoring of (PM(sub)10) mass concentration and elemental concentrations were carried out weekly. The average mass concentration of (PM(sub)10) in urban and rural areas were 59.2$\pm$36.5$\mu\textrm{g}$/㎥ and 41.4$\pm$23.7$\mu\textrm{g}$/㎥, respectively. To investigate the emission source, the enrichment factors were calculated for the fine and coarse particle fractions at two sites, respectively and these values were classified for anthropogenic and soil origin elements.

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Comparative Study of the Surface Roughness of Working Models Fabricated by Dental CAD/CAM Scannable Stone and Type IV Gypsum Products (치과용 캐드캠 스캔전용 석고와 Type IV 석고로 제작된 작업모형의 표면조도 비교 연구)

  • Kim, Sa-Hak;Kim, Jae-Hong
    • Journal of dental hygiene science
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    • v.14 no.4
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    • pp.455-460
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    • 2014
  • This study compared the surface roughness and surface characteristics between a type IV stone and scannable stone. Materials used were a type IV stone, two different kind of scannable stone. Ten specimens per experimental group were prepared according to manufacturer's direction. Surface roughness of specimen was measured using profilometer. The measurement was based on the standard of Japanese Industrial Standards 1994. The mean and standard deviations of each reference point were analyzed using one-way ANOVA and Scheff$\acute{e}$ post hoc test. The program used to handle statistical analysis was SPSS 20.0 and the significance level was set at 0.05. The difference of surface roughness was statistically significant in order of Scannable Stone $10.07{\pm}0.02{\mu}m$, Scannable Stone $20.08{\pm}0.03{\mu}m$, Type IV $0.10{\pm}0.04{\mu}m$. These results will have to be confirmed in further clinical application researches.

A study on Problems of the G-SEED Process and their Improvements - Focusing on case studies of office buildings - (녹색건축인증제도 진행과정의 문제점 및 개선방향 연구 - 업무시설 중심으로 -)

  • Jang, Hyun-Sook;Lee, Sang-Ho
    • KIEAE Journal
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    • v.14 no.1
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    • pp.91-99
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    • 2014
  • Environmental issues have become gradually important around the globe, which has increased society needs for the environment-friendly construction. In an effort to realize the environmental protection and energy efficiency, the British BREEAM has been developed, which is followed by the USA LEED, Japanese CASBEE and other national certification systems based on their own conditions. In this end, the Republic of Korea has implemented its own certification system named GBCS(Green Building Certification System) in 2002, and now actively promoted the G-SEED(Green Standard for Energy and Environmental Design) after GBCS modifications and amendments. The purpose of this study is to identify possible problems to be encountered in the process of the G-SEED for office facilities and to provide relevant solutions. In this end, three office facilities have been selected, which had obtained the G-SEED. This study has analyzed reasons of change of assessment scores between the preliminary certification and the main certification phases, has identified problems through in-depth interviews with practicing professionals(design, construction, eco-friendly consulting firm) and then has reached a conclusion for improvements. This study will be possibly used as reference materials for improvements of the green building certification system, and further detailed studies on respective parts will be required for improvements.

Extension Possibility of Indoor Air Standards in Office Building by Health Risk Assessment (건강위해성평가에 의한 사무실 실내공기오염물질의 관리항목 확대)

  • Roh, Young-Man;Lee, Cheol Min;Kim, Yoon Shin;Kim, Seok Won;Kim, Chi-Nyon;Kim, Hyun-Wook;Cho, Kee Hong;Choi, Ho Chun;Kim, Jung Man
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.16 no.1
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    • pp.54-67
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    • 2006
  • This study was performed to deduct the extension possibility of the standards establishment for $NO_2$, $O_3$, Asbestos, Radon, total volatile organic compounds (TVOC) excluded in the indoor air part of Industrial Safety Acts in Korea. The air pollutants were sampled for 30 office buildings from August to September, 2005 in the metropolitan area. The airborne concentrations of $NO_2$, $O_3$, Radon and TVOC were 0.0092 ppm, 0.0035 ppm, 0.57 pCi/L and $423{\mu}g/m^3$, respectively. The management plan and reduction methods is required in the aspect of indoor air quality(IAQ) because the emission sources of those also exist in indoor as well as outdoor even though those were not exceeded the standards of the Ministry of Environment in Korea. The standard for TVOC in the new and remodeling office has to be established based on the risk assessment when hazard index exceeded "1" in the worst case scenario. In the state of art, the management of each volatile organic compounds has a difficulty due to not enough data for toxicological reference. Therefore, it is suggested that first of all, the standard for TVOC be established and then expanded to each materials for decision-making of improvement of IAQ in office.

Multiagent Enabled Modeling and Implementation of SCM (멀티에이전트 기반 SCM 모델링 및 구현)

  • Kim Tae Woon;Yang Seong Min;Seo Dae Hee
    • The Journal of Information Systems
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    • v.12 no.2
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    • pp.57-72
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    • 2003
  • The purpose of this paper is to propose the modeling of multiagent based SCM and implement the prototype in the Internet environment. SCM process follows the supply chain operations reference (SCOR) model which has been suggested by Supply Chain Counsil. SCOR model has been positioned to become the industry standard for describing and improving operational process in SCM. Five basic processes, plan, source, matte, deliver and return are defined in the SCOR model, through which a company establishes its supply chain competitive objectives. A supply chain is a world wide network of suppliers, factories, warehouses, distribution centers and retailers through which raw materials are acquired, transformed or manufactured and delivered to customers by autonomous or semiautonomous process. With the pressure from the higher standard of customer compliance, a frequent model change, product complexity and globalization, the combination of supply chain process with an advanced infrastructure in terms of multiagent systems have been highly required. Since SCM is fundamentally concerned with coherence among multiple decision makers, a multiagent framework based on explicit communication between constituent agents such as suppliers, manufacturers, and distributors is a natural choice. Multiagent framework is defined to perform different activities within a supply chain. Dynamic and changing functions of supply chain can be dealt with multi-agent by cooperating with other agents. In the areas of inventory management, remote diagnostics, communications with field workers, order fulfillment including tracking and monitoring, stock visibility, real-time shop floor data collection, asset tracking and warehousing, customer-centric supply chain can be applied and implemented utilizing multiagent. In this paper, for the order processing event between the buyer and seller relationship, multiagent were defined corresponding to the SCOR process. A prototype system was developed and implemented on the actual TCP/IP environment for the purchase order processing event. The implementation result assures that multiagent based SCM enhances the speed, visibility, proactiveness and responsiveness of activities in the supply chain.

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Improvement and Verification of a Cholesterol Analytical Method to Analyze Cholesterol Content in Seafood (수산물의 콜레스테롤 분석을 위한 콜레스테롤 분석법 개선 및 검증)

  • Jung, So Hee;Jeong, Yu Rin;Shin, Hye Young;Kim, Yeon-Kye;Yoon, Na-Young
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.55 no.2
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    • pp.218-223
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    • 2022
  • Cholesterol is an essential component for maintaining health; however, excessive consumption can lead to diseases. Thus, continuous monitoring of cholesterol content is important in food research. The cholesterol analysis method used in Korea follows the Korean Food Standards Codex. As this method uses gas chromatography, derivatization of the sample is required, and analysis time is more than 30 min. Kim developed a new method using liquid chromatography; however saponification by the non-heat saponification method is insufficient. To address these limitations, a new cholesterol analysis method was developed and verified. The correlation coefficients for the cholesterol standard (STD) were maintained above 0.99. The limit of detection and limit of quantitation of cholesterol STD were 2.41 ㎍/mL and 7.31 ㎍/mL, respectively. The accuracies for cholesterol were 92.21-99.02%. The developed analytical method was also verified using three standard reference materials, and their accuracies were 93.71-97.09%. In addition, the cholesterol content of fishes was analyzed, and the values were compared with those recorded by the United States Department of Agriculture. Our results suggest that this method could be used as a new analytical method for cholesterol in seafood.

LI-RADS Version 2018 Treatment Response Algorithm: Diagnostic Performance after Transarterial Radioembolization for Hepatocellular Carcinoma

  • Jongjin Yoon;Sunyoung Lee;Jaeseung Shin;Seung-seob Kim;Gyoung Min Kim;Jong Yun Won
    • Korean Journal of Radiology
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    • v.22 no.8
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    • pp.1279-1288
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    • 2021
  • Objective: To assess the diagnostic performance of the Liver Imaging Reporting and Data System (LI-RADS) version 2018 treatment response algorithm (TRA) for the evaluation of hepatocellular carcinoma (HCC) treated with transarterial radioembolization. Materials and Methods: This retrospective study included patients who underwent transarterial radioembolization for HCC followed by hepatic surgery between January 2011 and December 2019. The resected lesions were determined to have either complete (100%) or incomplete (< 100%) necrosis based on histopathology. Three radiologists independently reviewed the CT or MR images of pre- and post-treatment lesions and assigned categories based on the LI-RADS version 2018 and the TRA, respectively. Diagnostic performances of LI-RADS treatment response (LR-TR) viable and nonviable categories were assessed for each reader, using histopathology from hepatic surgeries as a reference standard. Inter-reader agreements were evaluated using Fleiss κ. Results: A total of 27 patients (mean age ± standard deviation, 55.9 ± 9.1 years; 24 male) with 34 lesions (15 with complete necrosis and 19 with incomplete necrosis on histopathology) were included. To predict complete necrosis, the LR-TR nonviable category had a sensitivity of 73.3-80.0% and a specificity of 78.9-89.5%. For predicting incomplete necrosis, the LR-TR viable category had a sensitivity of 73.7-79.0% and a specificity of 93.3-100%. Five (14.7%) of 34 treated lesions were categorized as LR-TR equivocal by consensus, with two of the five lesions demonstrating incomplete necrosis. Interreader agreement for the LR-TR category was 0.81 (95% confidence interval: 0.66-0.96). Conclusion: The LI-RADS version 2018 TRA can be used to predict the histopathologic viability of HCCs treated with transarterial radioembolization.

Evaluation of Wind load Safety for Single G-type Greenhouse Using Korean Design Standard (건축구조기준을 활용한 농가지도형 G형 비닐하우스의 풍하중 안전성 평가)

  • Lee, Woogeun;Shin, Kyungjae
    • Journal of The Korean Society of Agricultural Engineers
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    • v.66 no.1
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    • pp.39-48
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    • 2024
  • Plastic greenhouses are simple structures consisting of lightweight materials such as steel pipes and polyvinyl chloride. However, serious damage occurs due to heavy winds and typhoon every year. To prevent a collapse of structural members, the Ministry of Agriculture and Rural Development has distributed plans and specifications for disaster-resistant standards. Despite these efforts, more than 50% of greenhouses still do not satisfy the disaster-resistant standards. Among the greenhouses that do not meet these standards, 85% are single-span greenhouses proposed 20 years ago. Consequently, there is a need to evaluate the safety of wind loads for the single-span greenhouse. Unfortunately, there are no design specifications for the greenhouses under wind loads. Therefore, a Korean design standard (KDS) has been utilized. KDS is defined with reference to wind speeds occurring once every 500 years, raising concerns about potential overdesign when considering the durability of plastic greenhouses. To address this, the modified wind load, considering the durability of the plastic greenhouse, was calculated, and a safety evaluation was conducted for sigle G-type plastic greenhouse. It was observed that the moment acting on the windward surface was substantial, and there was a risk of the foundation being pulled out if the basic wind speed exceeded 32 m/s. In terms of the combination strength ratio, it was less than 1.0 only on the leeward side when the basic wind speed was 24 m/s and 26 m/s. However, in all other cases, it exceeded 1.0, indicating an unsafe condition and highlighting the necessity for reinforcement.