• 한국재료학회지
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• 제12권10호
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• pp.784-790
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• 2002

For mass product of nanocrystalline ZnO ultrafine powders, self-sustaining combustion process(SCP) and ultrasonic spray combustion method(USCM) were applied at the same time. Ultrasonic spray gun was attached on top of the vertical type furnace. The droplet was sprayed into reaction zone of the furnace to form SCP which produces spherical shape with soft agglomerate crystalline ZnO particles. To characterize formed particles, fuel and oxidizing agent for SCP were used glycine and zinc nitrate or zinc hydroxide. Respectively, with changing combustion temperature and mixture ratio of oxidizing agent and fuel, the best ultrasonic spray conditions were obtained. To observe ultrasonic spray effect, two types of powder synthesis processes were compared. One was directly sprayed into furnace from the precursor solution (Type A), the other directly was heated on the hot plate without using spray gun (Type B). Powder obtained by type A was porous sponge shape with heavy agglomeration, but powder obtained using type B was finer primary particle size, spherical shape with weak agglomeration and bigger value of specific surface area. 9/ This can be due to much lower reaction temperature of type B at ignition time than type A. Synthesized nanocrystalline ZnO powders at the best ultrasonic spray conditions have primary particle size in range 20~30nm and specific surface area is about 20m$^2$/g.

• 한국축산시설환경학회지
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• 제14권2호
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• pp.97-104
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• 2008

본 연구는 지금까지 활용되었거나 새로이 제안된 액상 첨가제를 돈사에 살포하여 분진 농도의 경시적 변화를 관찰하여 제거 효과에 대해 객관적으로 비교 평가하기 위한 것으로 다음과 같은 결론들을 도출했다. 1. 살포 전 밀폐형 돈사내 분진 농도는 다른 연구자의 결과와 비교시 전반적으로 낮았다. 2. 온도의 경우는 살포 후 24시간까지 돈사 내부와 외부 큰 차이가 없었으나, 상대습도는 살포 후 1시간까지 증가하여 외부와 약 10% 가량의 차이를 보였다. 3. 평가대상 모든 액상 첨가제들의 살포직후 분진 평균 저감율은 살포 전 농도 대비 약 30%로 나타났다(p<0.05). 4. 살포 3시간 이후부터는 콩기름을 제외하고 다른 액상 첨가제들의 분진 농도에 대한 경시적 저감 효과가 관찰되지 않았다. 5. 평가대상 모든 액상 첨가제들 중 콩기름의 살포가 제거 효율성 및 안전성 측면 모두 돈사 분진 제어에 대해 가장 효과적인 첨가제였다.

• Journal of Welding and Joining
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• 제26권4호
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• pp.50-54
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• 2008

In this research, anode for SOFC has been manufactured from two different kinds of feedstock materials through thermal spraying process and the properties of the coatings were characterized and compared. One kind of feedstock was manufactured from spray drying method which includes nano-components of NiO, YSZ (300 nm) and graphite. And the other is manufactured by blending the micron size NiO coated graphite, YSZ and graphite powders as feedstock materials. Microstructure, mechanical properties and electrical conductivity of the coatings as-sprayed, after oxidation and after hydrogen reduction containing nano composite which is prepared from spray-dried powders were evaluated and compared with the same properties of the coatings prepared from blended powder feedstock. The coatings prepared from the spray dried powders has better properties as they provide larger triple phase boundaries for hydrogen oxidation reaction and is expected to have lower polarization loss for SOFC anode applications than that of the coatings prepared from blended feedstock. A maximum electrical conductivity of 651 S/cm at $800^{\circ}C$ was achieved for the coatings from spray dried powders which much more than that of the average value.

• Journal of Electrical Engineering and Technology
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• 제10권4호
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• pp.1796-1803
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• 2015

While considering the current scenario, in this world power demand goes on increases day by day. Frequent power outages occur in high voltage transmission line due to the deprived performance of polluted insulators; this affects overall operation of power system and may indirectly impinge on the growth of production sector. Many researchers are keenly taking efforts to provide highly reliable and stable power to neediest. In this paper, A.C pollution flashover performance of disc type glass insulator and composite long rod insulators investigation under various artificial pollutions by varying Equivalent Salt Density Deposition (ESDD) levels. Here, we use different types of pollution methods like binding method, dipping method and spraying methods with different types of pollutants concentration. Based on dimensional analysis, four different Mathematical models have been developed to predict the A.C pollution Flashover Voltage (FOV) of insulators. Both the experimental and mathematically modeled results are compared; it's observed that mathematical model 3 yields better results.

• 한국정밀공학회지
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• 제29권4호
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• pp.449-454
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• 2012

The method for spraying of liquid through an electrical filed has become a printing method since it can make very small droplet. To increase the reliability using the electro-hydrodynamic (EHD) jet printing, the jetting status needs to be monitored. Vision measurement techniques using high speed camera has been used to visualize the jet images. However, it requires image processing of a lot of images after image acquisitions. So, it is difficult to understand jet behavior such as jetting frequency, jet repeatability etc. In this work, a low cost electrical current measurement method was developed to measure electrical current from EHD jet printing. To verify the jetting monitoring capability of developed circuit, images from high speed camera were processed for comparison purpose.

• 대한화학회지
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• 제58권6호
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• pp.524-527
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• 2014

We report a simple yet efficient method to assemble large-scale aligned graphene nanoribbons (GNRs) with a width as small as 30 nm. The $V_2O_5$ nanowires (NWs) were aligned on a graphene surface via spraying a solution of the $V_2O_5$ NWs, and the graphene was selectively etched by the reactive ion etching method using the $V_2O_5$ NWs as a shadow mask. This process allowed us to prepare large scale patterns of the aligned GNRs on a $SiO_2$ substrate. The orientation of the aligned and randomly oriented GNRs was compared by the atomic force microscope (AFM) images. We achieved the highly aligned GNRs along the flow direction of the $V_2O_5$ NWs solution. Furthermore, we successfully fabricated a field effect-transistor with the aligned GNRs and measured its electrical properties. Since our method enable to prepare the aligned GNRs over a large area, it should open up new way for the various applications.

• 한국정밀공학회지
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• 제29권3호
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• pp.295-301
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• 2012

The method for spraying of liquids through an electrical field has become a printing method since it can make very small droplet. For electro-hydrodynamic jet printing to become a reliable jetting tool, the jetting performance should be characterized with respect to various jetting conditions. To optimize jetting conditions, the jetting behavior should be measured. In this study, we present a visualization techniques to measure jetting behavior from electro-hydrodynamic (EHD) inkjet head. Unlike most previous method, we use the CCD camera to measure the jetting behavior. For this purpose, LED light is synchronized with jetting signal and sequential image was obtained by adjusting the delay time of the LED light. Finally, merits and demerits of using CCD camera were discussed to measure jetting image from EHD inkjet head.

• 멤브레인
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• 제22권6호
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• pp.435-440
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• 2012

본 연구에서는 용매열합성법(solvothermal method)을 이용해 나노기공 HKUST-1 분리막을 제조하였다. In-situ 용매열합성법을 이용하는 경우, 매크로 기공의 알루미나 지지체 위에 균일하고 균열이 없는 HKUST-1 층을 형성하기 어렵다. 본 연구에서는 용매열합성 전에 알루미나 지지체의 표면을 가열한 상태에서 용매열합성의 전구체 용액을 분무하므로 연속적이고 균열이 없는 HKUST-1 분리막을 제조할 수 있었다. 합성된 HKUST-1 분리막은 XRD, FE-SEM 및 단일 기체투과 실험 등을 통해 분석하였다.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2006년도 추계 학술발표회 논문집
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• pp.133-136
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• 2006

The main purpose of this study is to develop a Sprayed FRP repair and strengthening method, which is a new technique for strengthening the existing concrete structures by mixing carbon or glass shot fibers and the epoxy or vinyl ester resins with high-speed compressed air in open air and randomly spraying the mixture onto the concrete surface. At present, the Sprayed FRP repair and strengthening method using the epoxy resin has not been fully discussed. In this study, a series of experiments are carried out to evaluate the strengthening effects of the flexural and shear concret beams strengthened with the Sprayed FRP method. The results revealed that the strengthening effects of the flexural and shear specimens are similar, compared to those of the FRP sheet.

• 한국정밀공학회지
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• 제15권11호
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• pp.227-232
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• 1998

The purpose of this study is to develop a numerical method for analyzing the transient heat transfer and evaluating the residual stress. The analysis of heat transfer and thermal stress are carried out by three-dimensional finite element method. Thermal spraying is one of the most common surface coating techniques to be used for many applications. In order to improve the mechanical properties of flame-sprayed ceramic coating layer, the accurate and effective analysis of heat transfer and thermal stress is essentially required.