• 제목/요약/키워드: spectroscopic analysis method

검색결과 207건 처리시간 0.024초

Integral Field Spectroscopic Data Reduction Method for High Resolution Infrared Observation

  • Lee, Sung-Ho;Pak, Soo-Jong;Choi, Min-Ho
    • Journal of Astronomy and Space Sciences
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    • 제27권4호
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    • pp.309-318
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    • 2010
  • We introduce a technical approach for reducing three-dimensional infrared (IR) spectroscopic data generated by integral field spectroscopy or slit-scanning observations. The first part of data reduction using IRAF presents a guideline for processing spectral images from long-slit IR spectroscopy. Multichannel image reconstruction, Image Analysis and Display (MIRIAD) is used in the later part to construct and analyze the data cubes which contain spatial and kinematic information of the objects. This technic has been applied to a sample data set of diffuse 2.1218 ${\mu}m$ $H_2$ 1-0 S(1) emission features observed by slit-scanning around Sgr A East in the Galactic center. Details of image processing for the high-dispersion infrared data are described to suggest a sequence of contamination cleaning and distortion correction. Practical solutions for handling data cubes are presented for survey observations with various configurations of slit positioning.

가변입사각 분광타원 법을 이용한 유기 발광 박막의 광학상수 및 두께 결정 (Determination of optical constants and thickness of organic electroluminescence thin films using variable angle spectroscopic ellipsometry)

  • 김상열;류장위;김동현;정혜인
    • 한국광학회지
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    • 제12권6호
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    • pp.472-478
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    • 2001
  • 가변입사각 분광타원법(Variable Angle Spectroscopic Ellipsometry)을 사용하여 유기발광소자(OLED)의 발광층인 유기박막 의 광학상수와 두께를 결정하였다. 광투과영역에서 모델링분석으로 박막의 평균두께와 굴절률 분산식을 결정하고, 광흡수영역으로 확장하여 유기막의 다층구조, 각 층의 두께와 밀도 그리고 각 파장에서의 복소굴절률을 결정하였다. 분광광도계를 사용하여 구한 투과율 스펙트럼을 가변입사각 분광타원법을 사용하여 결정한 다층구조 및 복소굴절률로 계산한 투과율 스펙트럼과 비교하여 분석의 정확성을 확인하였다.

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Study of Stray-light Analysis and Suppression Methods for the Spectroscopic System of a Solar-radiation Observer Instrument

  • Zheng, Ru;Liu, Bo;Wang, Lingyun;Gao, Yue;Li, Guangxi;Li, Changyu
    • Current Optics and Photonics
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    • 제5권3호
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    • pp.220-228
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    • 2021
  • To improve the measurement accuracy of a solar-radiation observer instrument, aiming at the problem of multiorder-stray-light interference caused by the diffraction of the flat-field concave grating in the spectroscopic system, straylight suppression methods for different forms of optical traps are studied. According to the grating surface-scattering distribution-function model, the bidirectional scattering distribution function (BSDF) of a dust-polluted surface and the flat-field concave grating's transition area of the spectroscopic system is calculated, and a Lyot stop with blade baffle is designed to suppress this kind of stray light. For diffraction multiorder stray light, based on the theory of light-energy transmission, a design for precise positioning of the trench optical trap is proposed. The superiority of the method is verified through simulation and actual measurement. The simulation results show that in a spectroscopic system approximately 160 mm × 140 mm × 80 mm in size, the energy of the stray light is reduced by one order of magnitude by means of the trench optical trap and Lyot stop, and the number of beams is reduced from 5664 to 1040. The actual measurements show that the stray-light-suppression efficiency is about 69.4%, which is effective reduction of the amount of stray light.

근적외 분광분석법에 의한 고춧잎의 Ascorbic Acid 함량 측정 (Rapid Determination of Ascorbic Acid in Red Pepper Leaves by Near-Infrared Reflectance Spectroscopic Analysis)

    • 한국식품영양과학회지
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    • 제27권3호
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    • pp.393-398
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    • 1998
  • The loss of ascorbic acid in dried red pepper leaves prepare with different drying methods of air-, oven-, microwave oven-, and vacuum drying with blanching or without was determined by a HPLC method. Vacuum drying showed the least loss of ascorbic acid than the other drying methods. Additionally, the feasibility of near infrared reflectance spectroscopy(NIRS) to determine the contents of ascorbic acid in the red pepper leaves was studied. NIRS was found to be an efficient way of determining ascorbic acid contents in red pepper leaves, requiring only 30 seconds of an analytical time.

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Spectroscopic Analysis of Gain Bandwidth in Raman Amplifier with Multiwavelength Pumping Scheme Using Actual Band Model

  • Felinskyi, Georgii;Han, Young-Geun;Lee, Sang-Bae
    • Journal of the Optical Society of Korea
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    • 제8권4호
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    • pp.156-162
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    • 2004
  • The spectroscopic model is proposed to analyze the gain bandwidth of a fiber Raman amplifier (FRA) with a multiple wavelength pumping scheme based on Raman gain theory. The oscillatory lineshape, which is the analytic function to analyze Raman gain spectra, allows us to estimate the gain bandwidth of the FRA. Based on the proposed theoretical modeling, we design and analyze the characteristics of the FRA using the combined multiwavelength pumping sources. We achieved the extended gain bandwidth of the FRA over 80 nm with the small gain ripple less than 0.5 dB. Threshold pumping power and effective noise figure for the FRA can be also analyzed by using the proposed model, which is also applicable for versatile fibers with other doping materials. The proposed analysis method can be useful for the design of FRA with the multiwavelength pumping scheme.

레이저 국소증착에 의한 탄소 미세 구조물 제조 및 분광분석 (Fabrication of micro carbon structures using laser-induced chemical vapor deposition and Raman spectroscopic analysis)

  • 한성일;김진범;;정성호
    • 한국레이저가공학회지
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    • 제5권2호
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    • pp.17-22
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    • 2002
  • Characteristics of micro carbon structures fabricated with laser-induced chemical vapor deposition (LCVD) are investigated. An argon ion laser (λ=514.5nm) and ethylene gas were utilized as the energy source and precursor, respectively. The laser beam was focused onto a graphite substrate to produce carbon deposit through thermal decomposition of the precursor. Average growth rate of a carbon rod increased for increasing laser power and pressure. Micro carbon rods with good surface quality were obtained at near the threshold condition. Micro carbon rods with aspect ratio of about 100 and micro tubular structures were fabricated to demonstrate the possible application of this method to the fabrication of three-dimensional microstructures. Laser Raman spectroscopic analysis of the micro carbon structures revealed that the carbon rods are consisting of amorphous carbon.

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Synthesis and spectroscopic characterization of zinc ferrite nanoparticles

  • Arora, Shefali;Nandy, Subhajit;Latwal, Mamta;Pandey, Ganesh;Singh, Jitendra P.;Chae, Keun H.
    • Advances in nano research
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    • 제13권5호
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    • pp.437-451
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    • 2022
  • Synthesis approaches usually affect the physical and chemical properties of ferrites. This helps ferrite materials to design them for desired applications. Some of these methods are mechanical milling, ultrasonic method, micro-emulsion, co-precipitation, thermal decomposition, hydrothermal, microwave-assisted, sol-gel, etc. These methods are extensively reviewed by taking example of ZnFe2O4. These methods also affect the microstructure and local structure of ferrite which ultimately affect the physical and chemical properties of ferrites. Various spectroscopic techniques such as Raman spectroscopy, Fourier Transform Infrared spectroscopy, Ultra Violet-Visible spectroscopy, Mossbauer spectroscopy, extended x-ray absorption fine structure, and electron paramagnetic resonance are found helpful to reveal this information. Hence, the basic principle and the usefulness of these techniques to find out appropriate information in ZnFe2O4 nanoparticles is elaborated in this review.

Determination of Toner Content by Diffuse Reflectance for Office Paper Recycling Studies

  • Oki, Tatsuya;Owada, Shuji;Yotsumoto, Hiroki;Tanuma, Hirokazu
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 2001년도 The 6th International Symposium of East Asian Resources Recycling Technology
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    • pp.111-116
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    • 2001
  • Waste office paper, photocopied or laser printed, has recently increased along with office automatization. In waste office paper, toner ink is used as the printing medium in place of conventional oil ink. Since toner ink cannot be saponificated by alkali and be decolored by bleaching, different from the case of oil ink, toner remains on regenerated paper as black specks. Although cascade recycling of waste office paper is compelled at present, the demand for low-grade paper is limited. From such circumstances, a new separation process for waste office paper is demanded to achieve parallel recycling. At the first stage of separation studies, the sharpness of separation is evaluated using small separators to obtain fundamental data. In a lab-scale separator, the sample amount of one feed is generally a few grams. However, the sample amount used for brightness, ERIC, and image analysis that are generally used to evaluate the efficiency of deinking are not small for lab-scale tests of these analyses. This paper describes an investigation of a sheet preparation method by a small amount of sample under 0.5g and compares the precision of toner content determination of spectroscopic analysis and image analysis from the viewpoint of separation evaluation. The easiness and convenience of the operation using only general-purpose equipments has also been set as a principle purpose. From the viewpoint of an analysis that yields high precision with a small amount of sample in short time, the method calculating the absorption coefficient from diffuse reflectance in the visible region is the most rational method in this study.

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국내 토양 휴믹물질의 특성 규명 및 DB 구축에 대한 연구 (Characterization of Humic and Fulvic Acids Extracted at the Soils of Korea and Its DB Establishment)

  • 이창훈;유지호;신현상;정근호;이창우
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2003년도 총회 및 춘계학술발표회
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    • pp.397-400
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    • 2003
  • In this study, humic and fulvic acids in soils at the vicinity of domestic atomic power plants(NPPs), located in Yungkwang(YK), Uljin(UJ), Kori(KR), Koseong(KS), Wolseong(WS) area, and in volcanic ash soils of the Cheju island(Mt. Hanla(HL), Manjanggul(MJ)) were isolated, and characterized using chemical(elemental analysis, proton exchange capacity, molecular size distribution) and spectroscopic(UV/Vis., IR, FL, $^{13}$ C NMR spectra) methods. The results were compared with one another and compiled for their DB establishments. The humic substances distribution (humic acid, fulvic acid, Humin) in the soils were also determined by IHSS standard method. Main purpose of this study was to provide a basic data needed to evaluate the effect of humic substances on the migrational behaviour of radioactive elements in contaminated surface soil.

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Spectroscopic study of Planetary hosting star HD 20794

  • Rittipruk, Pakakaew;Yushchenko, Alexander V.;Kang, Young-Woon
    • 천문학회보
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    • 제41권1호
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    • pp.43.4-44
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    • 2016
  • We observed the high resolution spectra of a solar-neighborhood planetary hosting star HD 20794. The analysis of spectroscopic data was performed using URAN and SYNTHE programs. These spectra allow us to determine the effective temperatures, surface gravities, microturbulent velocities and, chemical abundances. Bond et al. (2008) found chemical abundance for 11 elements, but using the Spectrum synthesis method we have so far determine about 30 elements. We have derived iron metallicity $[FeI/H]=-0.42{\pm}0.03$, $[FeII/H]=-0.43{\pm}0.012$, and surface gravity, log g = 4.48, in good agreement with values from previous investigation.

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