• Title/Summary/Keyword: solution mixing

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Development of Reagent Solution for Identifying the Chloride-based Packaging Materials (염소계 합성수지 포장재 식별용 진단시약 개발)

  • Oh, Jae Young
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.19 no.3
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    • pp.139-141
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    • 2013
  • In respect of environmental hazard or human safety, the use of the chloride-based packaging materials like polyvinyl chloride (PVC) blister and film, Polyvinylidene chloride (PVDC) laminated film has been restricted with national regulations. In this study, I intended to develope the reagent solution for identifying the chloride-based packaging materials, so that it was made by mixing methanol ($CH_3OH$) saturated with sodium hydroxide (NaOH) and pyridine as solvent with same ratio. The efficacy of this reagent solution was verified by the analysis of chemical mechanism and experiments that showed the color change (brown) of the specimens. This analysis methode using reagent solution is so simple, convenient, inexpensive and immediate that I expect it will be useful in the field of packaging.

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Influence of "Historical Effects" on the Rheological Properties of a Polyacrylonitrile Copolymer Solution

  • Cheng, Yumin;Zhang, Huibo;Zhang, Shuangkun;Liu, Weiwei;Wang, Jing;Cheng, Run;Ryu, SeungKon;Jin, Riguang
    • Carbon letters
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    • v.14 no.1
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    • pp.45-50
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    • 2013
  • Polyacrylonitrile (PAN) copolymers of different molecular weights were synthesized by a suspension polymerization and precipitation polymerization method. The rheology behaviors of the synthesized PAN copolymers were investigated in relation to their molecular weight, solid content and melting temperature. The influence of "historical effects" on the spinning solution of PAN was studied by analyzing the laws of viscosity considering the diversification time and temperature. The viscosity disciplines of each spinning solution conformed well to the rheological universal laws in a comparison of the suspension polymerization product with that of precipitation polymerization. Viscosity changes in the swelling process of dissolution were gentler in the suspension polymerization product; a small amount of water will quickly debase the solution viscosity, and high-speed mixing can greatly shorten the time required by the spinning solution to reach the final viscosity.

Effect of Dampening Component on Printed Quality of Textbook in lithography printing (평판인쇄의 축임물 조성이 교과서 인쇄품질에 미치는 영향)

  • Koo, Chul-Whoi;Sim, Woo-Seok;Ha, Young Baeck
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.48 no.1
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    • pp.134-141
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    • 2016
  • Dampening in printing is not only used with plain water but also used with various substances like dampening additive, in order to improve the wetting property by lowering the surface tension and to control material for modifing the ink transfer characteristic with proper emulsification. We have studied the printing quality according to these, looking into interrelationship among the dampening solution's pH, electrical conductivity and IPA content, prescribing the proper usage and minimum usage of fountain solution and dampening additive. In this study, it shows good result when mixing at the 7 wt% dampening with additive solution, which is result from the color density of printed sheets in accordance with the change of dampening solution condition. And the printed density value calculated 1 hour after printing, it shows relatively safe value at the etch liquid 4 wt% and IPA addition 2 wt%. The dry down at this test showed similar results regardless of various dampening conditions on coated paper, but in case of uncoated paper, the dry down showed a quite gap of different due to the fast penetration to the paper.

A Study on the Pb-contaminated Soil Remediation by Organic Acid Washing (유기산을 이용한 납 오염토양의 복원에 관한 연구)

  • 정의덕
    • Journal of Environmental Science International
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    • v.9 no.5
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    • pp.437-441
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    • 2000
  • A study on the removal of Pb ion from Pb-contaminated soil was carried out using ex-site extraction process. Tartaric acid (TA) and iminodiacetic acid sodium salt(IDA) as a washing agent were evaluated as a function of concentration reaction time mixing ratio of washing agent and recycling of washing agent. TA showed a better extraction performance than IDA. The optimum washing condition of TA and IDA were in the ratio of 1:15 and 1:20 between soil and acid solution during 1 hr reaction. The total concentrations of Pb ion by TA and IDA at three repeated extraction were 368.8 ppm and 267.5 ppm respectively. The recovery of Pb ion from washing solution was achieved by adding calcium hydroxide and sodium sulfide form the precipitation of lead hydroxide and lead sulfide and optimum amounts of sodium sulfide and calcium hydroxide were 7 g/$\ell$ for the TA washing solution and 4 g/$\ell$, 5g/$\ell$ for the IDA washing solution respectively. The efficiency of recycle for TA and IDA washing solution were 78.8% , 95.1%, and 89.2%, 96.6% at third extractions under $Na_2S$ and $Ca(OH)_2$, respectively.

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Type of Solution and the Effects of Temperature Change in a Rapid Appraisal of Cement Fineness with a Liquid Densimeter (액체밀도계에 의한 시멘트의 분말도 신속평가에서 용액 종류 및 온도변화의 영향)

  • Lee, Jae-Jin;Kim, Min-Sang;Moon, Byeong-Yong;Kim, Yeong-Tae;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2017.05a
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    • pp.167-168
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    • 2017
  • With the recent increase in demand for construction there has been an increase in the use of the raw material cement when mixing concrete; managing quality of cement powder, therefore, is most important. Therefore this study sought at first to develop a rapid appraisal using the Hydrometer method researched previously, for it was thought that when suspending cement in a solution and applying the Hydrometer method to it the temperature changes in the solution would have a great effect on the density value of the Hydrometer method; yet there has been no report of such influence factors. Therefore after analyzing the influence factors that the type of suspending solution and changes in temperature could have on rapid appraisal of fineness, using the Hydrometer method, this study was able to determine that using water at 20℃ was the most appropriate, and with every temperature increase of 10℃ the value of fineness should also be increased above or below 7% as well.

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Continuous Processing of Monodispersed Zirconia Powders (초음파 혼합 연속공정에 의한 단분산 지르코니아 분체의 합성)

  • Rhee, Jhun;Jo, Dong-Soo
    • Journal of the Korean Ceramic Society
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    • v.29 no.12
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    • pp.919-925
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    • 1992
  • Continuous synthesis process for monodispersed zirconia powders with ultrasonic wave mixing was developed. Reactant solutions were flowed through a T-tube with small diameter and then mixed in a microscale with ultrasonification. Reaction and aging were followed during the mixed solution of reactants is in plug flowing through a narrow long teflon tubing. Zr(n-OC4H9)4 in ethanol and H2O in ethanol were used as reactants. From this process monodispersed, spherical, non-agglomerated, singlet hydrated zirconia powders with 0.6 $\mu\textrm{m}$ average size were obtained. Geometrical standard deviation of the particle size distribution was less than 1.2 with ultrasonic mixing, and the geometrical standard deviation was not affected by the flow rate of the reactants.

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A Study About Biochip Combined with Micro Mixer and Reactor for DNA Ligation (마이크로 혼합기와 반응기로 구성된 DNA 결찰용 바이오칩에 관한 연구)

  • Kang, Do-Hyoung;Ahn, Yoo-Min;Hwang, Seung-Yong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.32 no.8
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    • pp.624-632
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    • 2008
  • In this research, we developed new PDMS-glass based microbiochip consisted of the micromixer and microreactor for DNA ligation. The micromixer was composed of a straight channel integrated with nozzles and pillars, and the microreactor was composed of a serpentine channel. We coated the PDMS chip surface with the 0.25wt.% PVP solution to prevent the bubble generation which was caused by the hydrophobicity of the PDMS. The new micomixer was passive type and the mixing was enhanced by a convective diffusion using the nozzle and pillar. The 10.33mm long micromixer showed the good mixing efficiency of 87.7% at 500 l/min flow rate. We could perform the DNA ligation successfully in the microbiochip, and the ligation time was shortened from 4 hours in conventional laboratory method to 5 min in the microbiochip.

The Effect on the Properties of High Flowing Concrete Using Low Heat Portland Cement by Material and Mixing Variations (저열 포틀랜드 시멘트를 사용한 고유동콘크리트의 사용재료 및 배합 변동에 따른 특성 평가)

  • 하재담;김태홍;유재상;이종열;권영호
    • Proceedings of the Korea Concrete Institute Conference
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    • 2001.11a
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    • pp.303-308
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    • 2001
  • Recently, concrete structures have become larger and higher and are demanding high performance concrete with lower heat to prevent thermal cracking, far greater workability, high strength and durability, Application of low heat portland(Type IV) cement for the high performance concrete is the best solution to satisfied those requirements. Here are explained the effect on the properties of high flowing concrete using low heat portland cement by material and mixing variations. Variables for sensitivity test were selected items like finess modulus of aggregates, particle size of limestone powder, unit water, superplasticizer, viscosity agent and concrete temperature. The results of this study were be applied to slurry wall of #215 and #216 of underground LNG tank in Inchon.

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Synthesis of Nanostructured Fe-Co Alloy Powders from Metal Salts

  • Lee, Young-Jung;Lee, Jea-Sung;Seo, Young-Ik;Kim, Young-Do
    • Journal of Powder Materials
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    • v.13 no.5 s.58
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    • pp.336-339
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    • 2006
  • Magnetic properties of nanostructured materials are affected in complicated manner by their microstructure such as pain size (or particle size), internal strain and crystal structure. Thus, studies on the synthesis of nanostructured materials with controlled microstructure are necessary fur a significant improvement in magnetic properties. In the present work, nanostructured Fe-Co alloy powders with a grain size of 50 nm were successfully fabricated from the powder mixtures of (99.9% purity) $FeCl_2$ and $CoCl_2$ by chemical solution mixing and hydrogen reduction.

Evaluation of Mechanical Properties and Resistance to Thermal Shock of YBCO-Ag Superconductors (YBCO-Ag 초전도체의 기계적 성질 및 열충격 내성에 대한 평가)

  • 주진호
    • Journal of Powder Materials
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    • v.5 no.2
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    • pp.139-144
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    • 1998
  • We have evaluated the role of Ag additions on the strength, fracture toughness, elastic modulus and resistance to thermal shock of $YBa_2Cu_3O_{7-x}$(YBCO) superconductor. Addition of 10 vol.% Ag improved strength and fracture toughness, whereas, decreased elastic modulus of YBCO. In addition, YBCO-Ag composites improved resistance to thermal shock probably due to enhanced strength, fracture toughness and thermal conductivity as a result of Ag addition. It is to be noted that YBCO-Ag made by mixing with $AgNO_3$ solution showed slightly higher strength, fracture toughness and resistance to thermal shock, compared to that made by mixing with metallic Ag powder. These improvements are believed to be due to the microstructure of more finely and uniformly distributed Ag particles.

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