• 제목/요약/키워드: solution measure

검색결과 904건 처리시간 0.03초

양자기술기반 가스 누출 감지 시스템 개발 (Development of Gas Leak Detecting System Based on Quantum Technology)

  • 권오성;박민영;반창우
    • 한국가스학회지
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    • 제25권5호
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    • pp.57-62
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    • 2021
  • 가스는 일반 가정 및 산업현장에서 폭 넓게 사용되는 에너지원이기도 하고, 석유화학 및 반도체 공정에서 넓게 사용되는 공정 물질이기도 하다. 그러나 사용이 쉬운 반면에 누출 시, 폭발 및 인체흡입 등으로 대규모 인명피해를 발생시키기도 한다. 따라서 가정 및 산업현장에서 안심하고 사용할 수 있는 가스 시설물 안전관리 솔루션은 필수적이다. 특히 가스시설의 노후화에 따라 고도화된 가스안전 솔루션의 개발 필요성이 대두되고 있는 실정이다. 본 논문은 가스 시설물에 더 이상 나눌 수 없는 최소 에너지 단위인 광자를 조사하고, 반사된 광자의 수를 분석해 원거리에서 가스 누출 여부 및 농도를 측정하는 기술을 개발하였다. 이는 기존의 전기/화학식 가스 센서나 적외선 기반의 가스 누출 감지기의 한계인 짧은 탐지 거리, 미세 누출 감지 불가 등의 기술적 한계를 극복하였다.

Development and validation of a qualitative GC-MS method for THCCOOH in urine using injection-port derivatization

  • Sim, Yeong Eun;Kim, Ji Woo;Kim, Jin Young
    • 분석과학
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    • 제34권2호
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    • pp.68-77
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    • 2021
  • Cannabis is one of the most abused drugs in Korea. The main psychoactive component in cannabis, Δ9-tetrahydrocannabinol, is metabolized to 11-nor-9-carboxy-Δ9-tetrahydrocannabinol (THCCOOH) and THCCOOH-glucuronide (THCCOOH-glu) in the human liver, whereby the amount of THCCOOH-glu found in urine is twice as high as that of THCCOOH. The analytical process adapted by the majority of urine drug-testing programs involves a two-step method consisting of an initial immunoassay-based screening test followed by a confirmatory test if the screening test result is positive. In this study, a qualitative gas chromatography-mass spectrometry (GC-MS) method was developed and validated for the detection of THCCOOH in human urine, where THCCOOH-glu was converted into THCCOOH by alkaline hydrolysis. For purification of the urine extract prior to instrumental analysis, high-speed centrifugation was used to minimize interference. In addition, an injection-port derivatization method using ethyl acetate and N,O-bis(trimethylsilyl)-trifluoroacetamide containing 1 % trimethylchlorosilane was employed to reduce the time required for derivatization, and an aliquot of the final solution was injected into the GC-MS. The method was validated by measuring the selectivity, limit of detection (LOD), and repeatability. The sensitivity, specificity, precision, accuracy, Kappa, F-measure, false positive, and false negative rate were determined by comparing the GC-MS results with those obtained using the immunoassay. The LOD was determined to be 0.32 ng/mL, while the repeatability was within 9.1 % for THCCOOH. Furthermore, a comparison study was carried out, whereby the screening immunoassay exhibited a sensitivity of 86.4 % and a specificity of 100 % compared to GC-MS. The applicability of the developed method was examined by analyzing spiked urine and forensic urine samples obtained from suspected cannabis abusers (n = 221).

PC 이벤트 탐지 기능과 보안 통제 절차를 연계시킨 시나리오 기반 금융정보유출 위험 대응 모델에 관한 연구 (A Study on a Scenario-based Information Leakage Risk Response Model Associated with the PC Event Detection Function and Security Control Procedures)

  • 이익준;염흥열
    • 한국전자거래학회지
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    • 제23권4호
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    • pp.137-152
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    • 2018
  • 기존 금융정보유출 행위를 탐지하기 위해 보안솔루션에서 생성한 행위 로그를 수집하여 패턴분석으로 정보유출 이상행위를 탐지하고 차단하는 활동에서 발생되는 한계점을 극복하고, 효과적으로 대응하기 위한 방안으로 첫 번째, PC에서 정보유출 경로(외부에서 읽기, 외부로 저장하기, 외부로 전송하기 등)로 이용되는 PC내 실행 프로그램들을 실시간으로 모니터링하고 두 번째, 해당 프로그램이 실행하는 시점에 연관된 보안 통제 프로세스와 상호 연동하여 정상 통제예외 통제우회 행위인지를 파악한 다음 마지막 단계인 시나리오 기반으로 생성한 처리 절차를 통해 금융정보유출 위험을 통제할 수 있는 위험 관리 모델을 제안함으로서 정보 보호 측면의 보안성 강화 및 업무 효율성 향상의 기대효과를 창출하고자 한다.

Effects of Titratable Acidity and Organic Acids on Enamel Erosion In Vitro

  • Kim, Eun-Jeong;Jin, Bo-Hyoung
    • 치위생과학회지
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    • 제19권1호
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    • pp.1-8
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    • 2019
  • Background: Erosion is a gradual process that occurs fairly quickly, and the full extent of the erosive effects of acidic beverages is not yet clear. The present study aimed to determine the differences in the erosive potentials among four naturally acidic fruit nectars within the same range of titratable acidity and to determine the influence of the components of organic acids on tooth erosion. Methods: Diluted fruit nectars (mandarin 1:1.1, orange 1:1.7, lemon 1:15, grapefruit 1:20) with the same range of titratable acidity (7.9 ml) and their corresponding organic acids (0.05%, 0.1%, 0.3%, and 0.5% citric acid, malic acid, and a citric and malic acid mixture [pH 2.8], respectively) were used. Specimens were placed in conical tubes with 50 ml of each of the test solutions for 1 hour. A microhardness test and scanning electron microscopy were used to measure enamel erosion. Acid separation was carried out using high-performance liquid chromatography to analyze the composition of each test solution. Results: Similar decreases in the Vickers hardness number (VHN) were observed among the groups treated with the following diluted fruit nectars: diluted mandarin nectar ($75.9{\Delta}VHN$), diluted lemon nectar ($89.1{\Delta}VHN$), diluted grapefruit nectar ($91.7{\Delta}VHN$), and diluted orange nectar ($92.5{\Delta}VHN$). No statistically significant differences were found in the enamel surface hardness after erosion (p>0.05). Citric and malic acids were the major organic acids in the test fruits. The lemon and orange groups had the highest malic acid concentrations, and the mandarin group had the lowest malic acid concentration. Conclusion: The titratable acidity and the citric and malic acid contents of the fruits could be crucial factors responsible for enamel erosion. Therefore, fruit-based drinks should be regarded as potentially erosive.

간호사의 문화간호역량 측정도구의 개발 (Development of the Cultural Competence Scale for Registered Nurses (CCS-RN))

  • 김경원;김선희;김영희;김현경;박혜숙;이선희;정금희
    • 지역사회간호학회지
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    • 제30권3호
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    • pp.281-294
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    • 2019
  • Purpose: This study is to develop the Cultural Competence Scale for Registered Nurses (CCS-RN) and to examine its validity and reliability. Methods: The item pool was generated based on related scales, a wide review of the literature, and in-depth interviews with nurses according to Purnell's cultural competence model. Content validity was verified by nursing experts. Construct validity using exploratory factor analysis, convergent validity using correlation coefficients, discriminant validity, internal consistency reliability, and test-retest reliability were examined. Results: The CCS-RN consists of a 35-item/7-factor solution with 54.1% of the total variance explained. The convergent validity of CCS-RN was supported. Cronbach's ${\alpha}$ was .94 for the total scale and ranged from .77 to .90 for the seven factors. Test-retest reliability was moderate. Conclusion: The evaluation of the psychometric properties of the CCS-RN shows that this scale is expected to be a valid and reliable measure of cultural competence among nurses. This scale may be useful for assessing nurses' own cultural competence and thus contribute to strengthening cultural competence.

Effect of casein phosphopeptide-amorphous calcium phosphate on fluoride release and micro-shear bond strength of resin-modified glass ionomer cement in caries-affected dentin

  • Agob, Jamila Nuwayji;Aref, Neven Saad;Al-Wakeel, Essam El Saeid
    • Restorative Dentistry and Endodontics
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    • 제43권4호
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    • pp.45.1-45.11
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    • 2018
  • Objectives: This study was conducted to evaluate fluoride release and the micro-shear bond strength of resin-modified glass ionomer cement (RMGIC) in casein phosphopeptide-amorphous calcium phosphate (CPP-ACP)-remineralized caries-affected dentin (CAD). Materials and Methods: Exposed dentin surfaces of 30 human third molar teeth were divided into 2 equal groups for evaluating fluoride release and the micro-shear bond strength of RMGIC to CAD. Each group was subdivided into 3 equal subgroups: 1) control (sound dentin); 2) artificially demineralized dentin (CAD); 3) CPP-ACP remineralized dentin (remineralized CAD). To measure fluoride release, 15 disc-shaped specimens of RMGIC (4 mm in diameter and 2 mm in thickness) were bonded on one flat surface of the dentin discs of each group. Fluoride release was tested using ion chromatography at different intervals; 24 hours, 3, 5, 7 days. RMGIC micro-cylinders were built on the flat dentin surface of the 15 discs, which were prepared according to the assigned group. Micro-shear bond strength was measured after 24 hours water storage. Data were analyzed using 1- and 2-way analysis of variance and the post hoc least significant difference test (${\alpha}=0.05$). Results: Fluoride detected in solutions (at all intervals) and the micro-shear bond strength of RMGIC bonded to CPP-ACP-remineralized dentin were significantly higher than those bonded to artificial CAD (p < 0.05). Conclusions: Demineralized CAD consumes more fluoride released from RMGIC into the solution for remineralization than CPP-ACP mineralized dentin does. CPP-ACP increases the micro-shear bond strength of RMGIC to CAD.

예인수조 LDV를 이용한 평판 경계층과 와이어 타입 난류촉진장치의 상호작용에 관한 연구 (Towed Underwater LDV Measurement of the Interaction of a Wire-Type Stimulator and the Boundary Layer on a Flat Plate)

  • 박종열;서정화;이신형
    • 대한조선학회논문집
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    • 제58권4호
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    • pp.243-252
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    • 2021
  • The present study aims to investigate the interaction of a wire-type turbulence stimulator and the laminar boundary layer on a flat plate by flow field measurement. For the towing tank tests, a one-dimensional Laser Doppler Velocimetry (LDV) attached on a two-axis traverse was used to measure the streamwise velocity component of the boundary layer flow in zero pressure gradient, disturbed by a turbulence stimulator. The wire diameter was 0.5 and 1.0 mm according to the recommended procedures and guidelines suggested by the International Towing Tank Conference. Turbulence development by the stimulator was identified by the skin friction coefficient, mean and Root Mean Square (RMS) of the streamwise velocity. The laminar boundary layer with the absence of the wire-type stimulator was similar to the Blasius solution and previous experimental results. By the stimulator, the mean and RMS of the streamwise velocity were increased near the wall, showing typical features of the fully developed turbulent boundary layer. The critical Reynolds number was reduced from 2.7×105 to 1.0×105 by the disturbances caused by the wire. As the wire diameter and the roughness Reynolds number (Rek) increased, the disturbances by the stimulator increased RMS of the streamwise velocity than turbulent boundary layer.

Force-based seismic design of steel haunch retrofit for RC frames

  • Ahmad, Naveed
    • Earthquakes and Structures
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    • 제20권2호
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    • pp.133-148
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    • 2021
  • The paper presents a simplified force-based seismic design procedure for the preliminary design of steel haunch retrofitting for the seismic upgrade of deficient RC frames. The procedure involved constructing a site-specific seismic design spectrum for the site, which is transformed into seismic base shear coefficient demand, using an applicable response modification factor, that defines base shear force for seismic analysis of the structure. Recent experimental campaign; involving shake table testing of ten (10), and quasi-static cyclic testing of two (02), 1:3 reduced scale RC frame models, carried out for the seismic performance assessment of both deficient and retrofitted structures has provided the basis to calculate retrofit-specific response modification factor Rretrofitted. The haunch retrofitting technique enhanced the structural stiffness, strength, and ductility, hence, increased the structural response modification factor, which is mainly dependent on the applied retrofit scheme. An additional retrofit effectiveness factor (ΩR) is proposed for the deficient structure's response modification factor Rdeficient, representing the retrofit effectiveness (ΩR=Rretrofitted /Rdeficient), to calculate components' moment and shear demands for the retrofitted structure. The experimental campaign revealed that regardless of the deficient structures' characteristics, the ΩR factor remains fairly the unchanged, which is encouraging to generalize the design procedure. Haunch configuration is finalized that avoid brittle hinging of beam-column joints and ensure ductile beam yielding. Example case study for the seismic retrofit designs of RC frames are presented, which were validated through equivalent lateral load analysis using elastic model and response history analysis of finite-element based inelastic model, showing reasonable performance of the proposed design procedure. The proposed design has the advantage to provide a seismic zone-specific design solution, and also, to suggest if any additional measure is required to enhance the strength/deformability of beams and columns.

Dielectric Properties of BaTiO3 Substituted with Donor Dopants of Nb5+ and Ta5+

  • Kim, Yeon Jung
    • 한국표면공학회지
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    • 제54권4호
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    • pp.178-183
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    • 2021
  • The temperature and frequency dependence of the dielectric constant of the BaTiO3 substituted with two types of donor dopants, Nb5+ and Ta5+, respectively, were compared and analyzed. Dielectric specimens of four specific compositions, Ba0.95Nb0.05TiO3, Ba0.90Nb0.10TiO3, Ba0.95Ta0.05TiO3, and Ba0.90Ta0.010TiO3 were prepared by calcining at 1100 ℃ and sintering at 1300 ℃ to have a perovskite structure to measure capacitance. XRD and SEM analysis were used to observe the structure, with particular focus on the integration into the Nb5+ and Ta5+ substituted BaTiO3 crystal lattice. X-ray diffraction peaks in the (200) and (002) planes were observed between 45.10° and 45.45° of the BaTiO3 solid solution substituted with different fractions of Nb5+ and Ta5+. The dielectric properties were analyzed and the relationship between the properties and structure of the substituted BaTiO3 was established. The fine particles and high density of the substituted BaTiO3 were maintained like pure BaTiO3, and in particular, a shift toward the low temperature side of the phase transition temperature range was clearly found, unlike pure BaTiO3. In addition, the phase transition at a temperature higher than the Curie temperature relatively satisfies the modified Curie-Weiss law.

가변피치 프로펠러의 축기전력 특성에 관한 연구 - 세계로호를 중심으로 - (A Study on the Characteristics of Shaft Electric Motive Force of Controllable Pitch Propeller - Focusing on the M/V Segero -)

  • 박경민;임명환;최상범;안병원
    • 해양환경안전학회지
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    • 제28권1호
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    • pp.135-140
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    • 2022
  • 대부분의 기계는 여러 종류의 금속으로 구성된다. 특히 선박의 축계는 프로펠러 날개의 황동과 스테인리스로 된 축으로 이루어져 있다. 이 이종금속이 바닷물의 전해액에 들어가면 볼타 전지를 이루고, 기전력이 발생된다. 이 기전력은 축계를 받치고 있는 베어링과 축을 전기부식 시키는 원인이 된다. 선박에서는 이 부식을 막기 위해 선박에서는 축 접지 시스템을 설치하여 운용하고 있다. 본 연구는 가변피치 프로펠러의 축기전력을 측정하기 위하여 추진축의 전압과 주기관의 회전수를 동시에 측정하였다. 측정장치는 내셔널인스트루먼트사의 24bit A/D컨버터를 사용하여 측정하였고, 프로그램은 LabVIEW를 사용하였다. 주기관의 회전수와 축기전력의 발생, 블레이드 각도에 따른 기전력과, 배의 항해 방향에 따른 축기전력을 측정하고 분석하였다.