• Title/Summary/Keyword: solution coating method

Search Result 549, Processing Time 0.028 seconds

Structural properties of PZT multilayer thick films of improved densification (PZT 후막의 치밀성 향상에 따른 PZT 다층 후막의 구조적 특성)

  • Yun, Sang-Eun;Lee, Sung-Gap;Park, Sang-Man;Lee, Young-Hie
    • Proceedings of the KIEE Conference
    • /
    • 2006.07a
    • /
    • pp.579-580
    • /
    • 2006
  • Ferroelectric PZT (70/30) thick films were fabricated by the screen printing method. And the PZT (30/70) Precusor solution were infiltrated by the spin-coating method on the PZT thick films to obtain a densification. All PZT thick films were sintered at $1050^{\circ}C$ for 10min. Structural properties, such as crystalline structure, microstructures and compositional ratio, of PZT thick films were investigated with the variation of the number of sol coatings using XRD, SEM and EDS, respectively. All PZT thick films exhibited a perovskite polycrystalline structure without a pyrochloer phase. The thickness of PZT thick films, 4-times screen-printed, was approximately 60fm. And the densification of the PZT thick films increased with increasing the number of sol coatings.

  • PDF

AXISYMMETRIC STAGNATION FLOW NEAR A PLANE WALL COATED WITH A MAGNETIC FLUID OF UNIFORM THICKNESS (균일 두께로 자성유체가 피막된 평면 벽 주의의 축대칭 정체 유동)

  • Ko, Hyung-Jong;Kim, Kyoung-Hoon;Kim, Se-Woong
    • 한국전산유체공학회:학술대회논문집
    • /
    • 2007.10a
    • /
    • pp.39-44
    • /
    • 2007
  • A similarity solution of the Navier-Stokes equation for the axisymmetric stagnation flow near a plane wall coated with a magnetic fluid of uniform thickness is constructed. The shape functions representing the flow in two (magnetic and normal) fluid layer are determined from a third order boundary value problem, which is solved by the Runge-Kutta method with two shooting parameters. Features of the flow including streamline pattern and interface velocity are investigated for the varying values of density ratio, viscosity ratio, and Reynolds number. The results for the interface and wall shear stress, boundary layer and displacement thickness are also presented.

  • PDF

Characterization of ferroelectric SrBi$_2$$Ta_2O_9$/ thin films prepared by Sol-Gel method (Sol-Gel법에의해 제작한 SrBi$_2$$Ta_2O_9$ 장유전체 박막의 특성)

  • 추정우;김영록;김영관;손병청;이전국
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 1996.11a
    • /
    • pp.175-179
    • /
    • 1996
  • Ferroelectric SrBi$_2$Ta$_2$$O_{9}$ thin films were fabricated by tole Sol-Gel method using a spin-on coating with MOD(Metal Organic Dccomposition) solution on Pt/Ti/SiO$_2$/Si(100) substratcs. The films were anncalcd at 80$0^{\circ}C$ for one hour in oxygen atmosphere. The effects of Bi/Ti mole ratios on crystalline orientations, surface morphologies, and subface composition SBT thin films with a Bi/Ta mole ratios from 1.1 to 1.3 were investigated using X-ray Diffractometry (XRD). Atomic Force (AFM), X-Ray Photoelectron Spectroscopy(XPS). Ferroelectric properties of these films were also measured.d.

  • PDF

Electronic properties of PZT(20/80) thick film and PZT(80/20) thin film multilayer with variation of sintering temperature (다층 PZT(20/80) 후막과 PZT(80/20) 박막의 소결온도에 따른 전기적 특성)

  • Noh, Hyun-Ji;Lee, Sung-Gap;Park, Sang-Man;Bae, Seon-Gi
    • Proceedings of the KIEE Conference
    • /
    • 2006.07b
    • /
    • pp.1243-1244
    • /
    • 2006
  • In this paper, PZT(20/80) thick films were fabricated by the screen-printing method. And the PZT(80/20) coating solution was synthesized by the sol-gel method. PZT(20/80) thick films were screen-printed on the alumina substrates. PZT(80/20) thin film was spin-coated on the PZT(20/80) thick films to obtain densification. And the structural and electrical properties of PZT thick films were investigated with variation of sintering temperature. The PZT specimen sintered at $650^{\circ}C$ showed good relative dielectric constant of 219 and dielectric loss of 2.45%. Also the remanent polarization and the coercive field were $16.48{\mu}C/cm^2$ and 35.48kV/cm, respectively.

  • PDF

Structural properties of PZT multilayer thick films of improved densification (PZT 후막의 치밀성 향상에 따른 PZT 다층 후막의 구조적 특성)

  • Yun, Sang-Eun;Lee, Sung-Gap;Park, Sang-Man;Lee, Young-Hie
    • Proceedings of the KIEE Conference
    • /
    • 2006.07b
    • /
    • pp.1245-1246
    • /
    • 2006
  • Ferroelectric PZT (70/30) thick films were fabricated by the screen printing method. And the PZT (30/70) precusor solution were infiltrated by the spin-coating method on the PZT thick films to obtain a densification. All PZT thick films were sintered at $1050^{\circ}C$ for 10 min. Structural properties, such as crystalline structure, microstructures and compositional ratio, of PZT thick films were investigated with the variation of the number of sol coatings using XRD, SEM and EDS, respectively. All PZT thick films exhibited a perovskite polycrystalline structure without a pyrochloer phase. The thickness of PZT thick films, 4-times screen-printed, was approximately $60{\mu}m$. And the densification of the PZT thick films increased with increasing the number of sol coatings.

  • PDF

Effects of Electrostatic Force on Movement of Sprayed Aerosol Particles in Continuous Galvanizing Process (용융도금강판의 제조 공정에 있어서 2-유체 분사 액적의 운동에 미치는 정전대전력의 영향)

  • Kim, S.H.;Kim, H.M.;Chung, H.C.;Chung, W.S.
    • Journal of ILASS-Korea
    • /
    • v.5 no.3
    • /
    • pp.45-54
    • /
    • 2000
  • A novel electrostatic splaying method for solidifying a galvanized coating layer was studied. Our experimental results and computer simulations showed that electric field could assist the fine droplets to attach on the steel surface and change the sprayed droplets trajectory especially in the space near the steel surface. It was necessary to apply the electric voltage higher than - 20 kV to obtain the enough electrostatic attraction force between droplets and the steel sheet.

  • PDF

Preparation of Conductive $TiO_2$ thin film by Electrospray Depositon (Electrospray를 통한 전도성 박막의 제조)

  • Lee, Kyung-Hwa;Kim, Han-Seong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2008.06a
    • /
    • pp.381-382
    • /
    • 2008
  • $TiO_2$ colloidal solution was electrosprayed for preparing a conductive thin film with high quality. Electrospray is a technique of liquid dispersion electrically and a good method of manufacturing nanoparticle, nanofiber, porous membrane, film preparation and coating. Water and ethanol were used as solvents and their mixing ratio was varied for studying the influence of solvent volatile on nanoparticle dispersion. Various nozzles to control the thru-put of solutions.were examined. Integrated analytical method and scanning electron microscope were used to analyze integrity and microscopic images.

  • PDF

Synthesis of Highly Concentrated ZnO Nanorod Sol by Sol-gel Method and their Applications for Inverted Organic Solar Cells

  • Kim, Solee;Kim, Young Chai;Oh, Seong-Geun
    • Korean Chemical Engineering Research
    • /
    • v.53 no.3
    • /
    • pp.350-356
    • /
    • 2015
  • The effects of the zinc oxide (ZnO) preparing process on the performance of inverted organic photovoltaic cells (OPVs) were explored. The morphology and size of ZnO nanoparticles were controlled, leading to more efficient charge collection from device and higher electron mobility compared with nanospheres. Nanosized ZnO particles were synthesized by using zinc acetate dihydrate and potassium hydroxide in methanol. Also, water was added into the reaction medium to control the morphology of ZnO nanocrystals from spherical particles to rods, and $NH_4OH$ was used to prevent the gelation of dispersion. Solution-processed ZnO thin films were deposited onto the ITO/glass substrate by using spin coating process and then ZnO films were used as an electron transport layer in inverted organic photovoltaic cells. The analyses were carried out by using TEM, FE-SEM, AFM, DLS, UV-Vis spectroscopy, current density-voltage characteristics and solar simulator.

Electronic properties of PZT(20/80) thick film and PZT(80/20) thin film multilayer with variation of sintering temperature (다층 PZT(20/80)후막과 PZT(80/20)박막의 소결온도에 따른 전기적 특성)

  • Noh, Hyun-Ji;Lee, Sung-Gap;Park, Sang-Man;Bae, Seon-Gi
    • Proceedings of the KIEE Conference
    • /
    • 2006.07c
    • /
    • pp.1703-1704
    • /
    • 2006
  • In this paper, PZT(20/80) thick films were fabricated by the screen-printing method. And the PZT(80/20) coating solution was synthesized by the sol-gel method. PZT(20/80) thick films were screen-printed on the alumina substrates. PZT(80/20) thin film was spin-coated on the PZT(20/80) thick films to obtain densification. And the structural and electrical properties of PZT thick films were investigated with variation of sintering temperature. The PZT specimen sintered at $650^{\circ}C$ showed good relative dielectric constant of 219 and dielectric loss of 2.45%. Also the remanent polarization and the coercive field were $16.48{\mu}C/cm^2$ and 35.48kV/cm, respectively.

  • PDF

Structural properties of PZT multilayer thick films of improved densification (PZT 후막의 치밀성 향상에 따른 PZT 다층 후막의 구조적 특성)

  • Yun, Sang-Eun;Lee, Sung-Gap;Park, Sang-Man;Lee, Young-Hie
    • Proceedings of the KIEE Conference
    • /
    • 2006.07c
    • /
    • pp.1705-1706
    • /
    • 2006
  • Ferroelectric PZT (70/30) thick films were fabricated by the screen printing method. And the PZT (30/70) precusor solution were infiltrated by the spin-coating method on the PZT thick films to obtain a densification. All PZT thick films were sintered at $1050^{\circ}C$ for 10 min. Structural properties, such as crystalline structure, microstructures and compositional ratio, of PZT thick films were investigated with the variation of the number of sol coatings using XRD, SEM and EDS, respectively. All PZT thick films exhibited a perovskite polycrystalline structure without a pyrochloer phase. The thickness of PZT thick films, 4-times screen-printed, was approximately $60{\mu}m$. And the densification of the PZT thick films increased with increasing the number of sol coatings.

  • PDF