• Title/Summary/Keyword: solid content measurement

Search Result 73, Processing Time 0.03 seconds

Freezing Behaviors of Frozen Foods Determined by $^1H$ NMR and DSC

  • Lee, Su-Yong;Moon, Se-Hun;Shim, Jae-Yong;Kim, Yong-Ro
    • Food Science and Biotechnology
    • /
    • v.17 no.1
    • /
    • pp.102-105
    • /
    • 2008
  • The freezing patterns of commercial frozen foods were characterized by using proton nuclear magnetic resonance ($^1H$ NMR) relaxometry and differential scanning calorimetry (DSC). The liquid-like components like unfrozen water were investigated as a function of temperature (10 to $-40^{\circ}C$) and then compared with the unfrozen water content measured by DSC. The formation of ice crystals and the reduction of water in the foods during freezing were readily observed as a loss of the NMR signal intensity. The proton NMR relaxation measurement showed that the decreasing pattern of the liquid-like components varied depending on the samples even though they exhibited the same onset temperature of ice formation at around $0^{\circ}C$. When compared with the unfrozen water content obtained by the DSC, the NMR and DSC results could be closely correlated at the temperature above $-20^{\circ}C$. However, the distinct divergence in the values between 2 methods was observed with further decreasing temperatures probably due to the solid glass formation which was not detected by DSC.

Electrical properties of XLPE and Semiconductor Materials for Power Cable (전력케이블의 가교폴리에틸렌과 반도전 재료의 전기적 특성)

  • Lee, Ju-Hong;Kim, Hyang-Kon
    • Proceedings of the KIEE Conference
    • /
    • 2008.09a
    • /
    • pp.207-210
    • /
    • 2008
  • In this paper, we researched the dielectric properties and voltage dependence on slice XLPE sheet from 22[kV] and 154[kV] power cable. We studied effects for impurities and water for semiconductor shield through a dielectric properties experiment to estimate performance of insulating materials in power cable. Capacitance and $tan{\delta}$ of 22[kV], 154[kV] were 53/43[pF] and $7.4{\times}10^{-4}$, $2.1510^{-4}$. In these results, the trend was increased with the increase of temperature. The tan6 of XLPE/semiconductor layer was increased as compared with that of XLPE. Dielectric properties reliability of tan6 was small. Also, To improve mean-life and reliability of power cable in this study, we have investigated chemical properties showing by changing the content of carbon black that is semiconductive additives for underground power transmission. Specimens were made of sheet form with the three of existing resins and the nine of specimens for measurement. Chemical properties of specimens was measured by FT-ATR (Fourier Transform Attenuated Total Reflectance). The condition of specimens was a solid sheet. We could observe functional group (C=O, carbonyl group) of specimens through FT-ATR. From these experimental result, the concentration of functional group (C=O) was high according to increasing the content of carbon black. We could know EEA was excellent more than other specimens from above experimental results.

  • PDF

Apple Quality Measurement Using Hyperspectral Reflectance and Fluorescence Scattering (하이퍼 스펙트랄 반사광 및 형광 산란을 이용한 사과 품질 측정)

  • Noh, Hyun-Kwon;Lu, Renfu
    • Journal of Biosystems Engineering
    • /
    • v.34 no.1
    • /
    • pp.37-43
    • /
    • 2009
  • Hyperspectral reflectance and fluorescence scattering have been researched recently for measuring fruit post-harvest quality and condition. And they are promising for nondestructive detection of fruit quality. The objective of this research was to develop a model, which measure the quality of apple by using hyperspectral reflectance and fluorescence. A violet laser (408 nm) and a quartz tungsten halogen light were used as light sources for generating laser induced fluorescence and reflectance scattering in apples, respectively. The laser induced fluorescence and reflectance of 'Golden Delicious' apples were measured by using a hyperspectral imaging system. Fruit firmness, soluble solids and acid content were measured using standard destructive methods. Principal component analyses were performed to extract critical information from both hyperspectral reflectance and fluorescence data and this information was then related to fruit quality indexes. The fluorescence models had poorer predictions of the three quality indexes than the reflectance models. However, the prediction models of integrating fluorescence and reflectance performed consistently better than the individual models of either reflectance or fluorescence. The correlation coefficient for fruit firmness, soluble solid content, and tillable acidity from the integrated model was 0.86, 0.75, and 0.66 respectively. Also the standard errors were 6.97 N, 1.05%, and 0.07% respectively.

Chemical Properties Changes of Nanocomposites due to Addition of Carbon nanotubes (탄소나노튜브를 첨가한 나노 복합재료의 화학적 특성 변화 연구)

  • Yang, Jong-Seok;Lee, Kyoung-Yong;Shin, Dong-Hoon;Sung, Baek-Ryong;Park, Dae-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2006.11a
    • /
    • pp.156-157
    • /
    • 2006
  • To improve mean-life and reliability of power cable in this study, we have investigated chemical properties showing by changing the content of Carbon nanotube(CNT) that is semiconductive additives for underground power transmission. Specimens were made of sheet form with the three of existing resins and the five of specimens for measurement. Chemical properties of specimens was measured by FT-ATR (Fourier Transform Attenuated Total Reflectance). The condition of specimens was a solid sheet. We could observe functional group (C=O, carbonyl group) of specimens through FT-ATR. From these experimental result, the concentration of functional group (C=O) was high according to increasing the content of Carbon nanotube. We could know CNT/EEA was excellent more than other specimens from above experimental results.

  • PDF

Elastic Modulus Measurement of a Dry Process Fuel Pellet by Resonant Ultrasound Spectroscopy (초음파 공진 분석법을 이용한 건식공정 핵연료 소결체의 탄성계수 측정)

  • 류호진;강권호;문제선;송기찬;정현규;정용무
    • Journal of Powder Materials
    • /
    • v.11 no.4
    • /
    • pp.314-321
    • /
    • 2004
  • The elastic moduli of simulated dry process fuels with varying composition and density were measured in order to analyze the mechanical properties of a dry process fuel pellet. Resonant ultrasound spectroscopy(RUS) which can determine all elastic moduli with one set of measurements for a rectangular parallelepiped sample was used to measure the elastic moduli of UO$_{2}$ and simulated dry process fuel. The simulated dry process fuel showed a higher value of Young's modulus than UO$_2$ due to the presence of metallic precipitates and solid solution elements in the UO$_{2}$ matrix. The correlation between Young's modulus and porosity(P) of simulated dry process fuel was found to be 231.4-651.8 P (GPa) at room temperature. Dry process fuel with a higher burnup showed higher Young's modulus because total content of fission product element was increased.

Fuel Characteristics of Sewage Sludge in a Fluidized Bed Incinerator (유동상 소각로에서 하수 슬러지 연료 특성)

  • Choi, Jin-Hwan;Choi, Sang-Min
    • 한국연소학회:학술대회논문집
    • /
    • 1999.10a
    • /
    • pp.81-91
    • /
    • 1999
  • Fuel characteristics of sewage sludge as required for the fluidized bed incinerators have been evaluated. Sewage sludge is basically a solid fuel with high percentage of moisture. Moisture content of the fuel directly affects the heating value of the fuel and the exhaust gas composition. When the sludge of transported into the incinerator, sludge cake is subject to the mixing, break-up and heat-up. Fluidization process would enhance these physical processes. The sludge fuel could then undergo the moisture evaporation and devolatilization process. Subsequent oxidation of volatiles as well as the remaining char would then follow. Sludge samples are characterized with high percentage of volatiles out of total combustibles. Quantitative understanding of above listed subprocesses would certainly help in the utilization of fluidized bed incinerators. A limited set of fuel characterization tests including calorimetric analysis, proximate analysis, elemental analysis and thermogravimetric analysis were conducted for the selected sludge samples. The measurement reasults of sludge samples were reported along with some published data. Limited experience in the actual incinerator plant is also presented.

  • PDF

State Estimation and Property Control in an MMA-MA Copolymerization Reactor

  • Park, Myung-June;Hur, Su-Mi;Rhee, Hyun-Ku
    • 제어로봇시스템학회:학술대회논문집
    • /
    • 2001.10a
    • /
    • pp.97.3-97
    • /
    • 2001
  • An experimental study was performed to establish the validity of an on-line state estimator for a semibatch MMA-MA copolymerization reactor by using on-line densitometer and viscometer under two different operating conditions; one without additional solvent feed and the other with solvent fed additionally. A conventional extended Kalman filter (EKF) was used as the state estimator and the experiment was conducted for the purpose of application to the control of copolymer properties. Further analysis was made by using off-line measurement data for the mole fraction of MMA in the remaining monomers and the solid content. It was found that the EKF could provide a good estimate for the states of the copolymerzation system ...

  • PDF

Complex Impedance Analysis of Nb-Doped Barium Titanate Ceramics (Nb이 첨가된 $BaTiO_3$ 세라믹스의 복소 임피던스 해석)

  • 조경호;남효덕;이희영
    • Journal of the Korean Ceramic Society
    • /
    • v.31 no.9
    • /
    • pp.1012-1220
    • /
    • 1994
  • BaTiO3 ceramics doped with 0.1 to 4.0 mol% Nb2O5 were prepared by conventional solid stage sintering process, so as to investigate the effect of the amount of Nb2O5 on the dielectric properties and complex impedance patterns of barium titanates. From the measurement of capacitance, we found that the dielectric constant of BaTiO3 samples with 1 mol% or more Nb2O5 remained approximately constant around room temperature with values higher than 2500. In this paper, the effect of impurity content as well as temperature on complex impedance patterns was discussed in detail. In particular, the grain and grain boundary behavior of samples which showed PTCR characteristics was discussed in terms of measuring temperature.

  • PDF

Evaluation of Organic Compounds and Heavy Metals in Sediments from the Urban Streams in the Busan City (부산시 도심하천 퇴적물의 유기물 및 중금속 오염도 평가)

  • Lee, Junki;Kim, Seogku;Song, Jaehong;Lee, Taeyoon
    • Journal of the Korean GEO-environmental Society
    • /
    • v.11 no.1
    • /
    • pp.35-43
    • /
    • 2010
  • The main purpose of this study is to offer informations about the current conditions and basic data of sediments for the urban streams in the Busan city. Total 14 urban streams were selected and sediment samples were collected. Then, It was investigated the sediment qualities though the measurement of pH, proximate analysis, elemental analysis, COD, organic carbon content, volatile solid content and heavy metal concentration. Results show that COD, organic carbon content, volatile solid content and heavy metal concentration of sediment are determined in the range of $1.20{\sim}75.07mg\;L^{-1}$, 0.19~11.54%, 0.23~34.21% and $0.4{\sim}732.6mg\;kg^{-1}$, respectively. Finally, Analysis data of sediments were compared with USEPA sediment quality standards and ontario sediment quality guidelines. As a result, when compared with USEPA sediment quality standards, total 9 samples were evaluated as heavily polluted and total 3 samples were evaluated as moderately polluted. But, when compared with ontario sediment quality guidelines, total 3 samples were evaluated as Severe effect level and total 10 samples were evaluated as lowest effect level.

Effect of Moisture Content on Viscosity of Starch Dough (전분반죽의 점도에 미치는 수분함량의 영향)

  • Lee, Boo-Yong;Lee, Chang-Ho;Lee, Cherl-Ho
    • Korean Journal of Food Science and Technology
    • /
    • v.27 no.4
    • /
    • pp.582-592
    • /
    • 1995
  • To measure rheological properties of the starch dough, an Extrusion Capillary Viscometer(ECV) cell was self-made and attached to Instron machine(Model 1140). Apparent viscosities of corn and waxy corn starch doughs were measured and their gelatinization degrees were determined by enzymatic analysis. When corn and waxy corn starch doughs with $36{\sim}52%$ moisture content were heated at $60{\sim}100^{\circ}C$, come-up time of the cold point of doughs decreased from 220 sec to 140 sec with increased in the moisture content. In the measurement range of $36{\sim}52%$ moisture content and $60{\sim}100^{\circ}C$ heating temperature, both corn and waxy corn starch doughs showed pseudoplastic flow behaviors. At the same shear rate, both shear stress and viscosity of starch dough decreased as the moisture content increased. At the moisture content above 44%, the shear stress and viscosity of starch dough decreased as the heating temperature increased from $60^{\circ}C\;to\;70^{\circ}C$, but increased as the heating temperature increased from $80^{\circ}C\;to\;100^{\circ}C$. When the moisture content increased and heating temperature, the gelatinization degree of starch dough increased from about 10% to about 62%. The gelatinization degree of waxy corn starch dough was $15{\sim}20%$ higher than that of corn starch dough under the same gelatinization conditions. The effects of moisture content on the viscosity of starch dough were examined by Arrhenius equation. As the moisture content increased, viscosity of starch dough decreased. But the effect of moisture content was greater in the range of $80{\sim}100^{\circ}C$ than in the range of $60{\sim}70^{\circ}C$ heating temperature.

  • PDF