• 한국분말재료학회지
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• 제23권5호
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• pp.391-396
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• 2016

In this study, ultra-fine soft-magnetic micro-powders are prepared by high-pressure gas atomization of an Fe-based alloy, Fe-Hf-B-Nb-P-C. Spherical powders are successfully obtained by disintegration of the alloy melts under high-pressure He or $N_2$ gas. The mean particle diameter of the obtained powders is $25.7{\mu}m$ and $42.1{\mu}m$ for He and $N_2$ gas, respectively. Their crystallographic structure is confirmed to be amorphous throughout the interior when the particle diameter is less than $45{\mu}m$. The prepared powders show excellent soft magnetic properties with a saturation magnetization of 164.5 emu/g and a coercivity of 9.0 Oe. Finally, a toroidal core is fabricated for measuring the magnetic permeability, and a ${\mu}_r$ of up to 78.5 is obtained. It is strongly believed that soft magnetic powders prepared by gas atomization will be beneficial in the fabrication of high-performance devices, including inductors and motors.

• 한국자기학회지
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• 제21권2호
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• pp.77-82
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• 2011

우리 삶의 질을 좌우하는 전자기 기기의 고기능화, 자동화, 소형화 추이에 따라 사용량이 급격히 증가하고 있는 연자성 소재로서 가장 널리 사용되고 있는 전기강판과 에너지 고효율화라는 시대의 요구에 따라 새롭게 부상되고 있는 연자성 복합 분말 소재에 대해 각 연자성 소재 분야에서 철손 제어 인자 및 이들 인자들의 제어 방안에 대해 문헌을 고찰했다. 전기강판에서는 히스테리시스 손실을 낮추기 위해 정련공정을 통해 자구이동을 방해하는 결함을 제거하고 결정립의 크기를 최적화하고 있으며, 와전류 손실의 감소를 위해 합금첨가원소를 통해 비저항을 높이고 판재의 두께를 박판화하고 있다. 이와 동시에 코팅을 통해 자구의 이동이 용이하도록 응력의 방향 및 크기를 제어하며, 압연기술과 열처리 기술을 통해 집합조직을 최적화하여 고투자율 및 저철손을 동시에 충족시켜 나가고 있다. 연자성 복합 분말 소재의 경우, 분말 표면의 복합화를 통해 철계 조성, 코팅, 윤활재 및 바인더, 성형 및 열처리 조건 등에 복합적으로 의존하는 연자성 코어의 최종 자기특성을 제어하고 있다. 온간 및 다단 성형과 같은 새로운 성형공정, 2단 소둔/자성 열처리와 같은 소둔 조건, 나노결정질, 비정질 및 벌크 비정질 등과 같은 새로운 조성, 적절한 코팅층의 변수들을 최적화할 경우, 연자성 복합 소재의 자성특성은 향상될 것으로 기대된다.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1288-1289
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• 2006

Innovative SMC with low iron loss was made from iron powders with evaporated MgO insulation coating. The coating had greater heat-resistance than conventional phosphatic insulation coating, which enabled stress relieving annealing at higher temperature. Magnetic properties of toroidal samples (OD35mm,ID25mm, t5) were examined. The iron loss at 50Hz for Bm = 1.5T was lower 50% of conventional SMC and was almost the same with silicon iron laminations(t0.35). It became clear that MgO insulation coating has enough heat resistance and adhesiveness to powdersurface to obtain innovative SMC with low iron loss.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.788-789
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• 2006

Microstructure and soft magnetic properties of bulk amorphous and/or nanocrystalline $Fe_{73.5}Cu_1Nb_3Si_{13.5}B_9$ alloys prepared by consolidation at 5.5GPa were investigated. The relative density of the bulk sample 1 (from amorphous powders) was 98.5% and the grain sizes were about 10.6nm. While the relative density and grain sizes of bulk sample 2 (from nanocrystalline powders) are 98% and 20.1nm, respectively. Particularly, the bulk samples exhibited a good combined magnetic property: for Sample1, $M_s=125emu/g$ and $H_c=1.5Oe;$ for Sample2, $M_s=129emu/g$ and $H_c=3.3Oe$. The success of synthesizing the nanocrystalline Fe-based bulk alloys will be encouraging for the future development of bulk nanocrystalline soft magnetic alloys.

• 한국재료학회지
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• 제12권6호
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• pp.488-492
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• 2002

Magnetic properties of nanostructured materials are affected in complicated manner by their microstructure such as grain size, internal strain and crystal structure. Thus, studies on the synthesis of nanostructured materials with controlled microstructure are necessary for a significant improvement in magnetic properties. It is well known that when Fe-Co alloy undergoes ordering transformation, soft magnetic properties could be obtained. There are many reports that the magnetic properties of the materials can be changed with variation of grain size. In the present work, nanostructured Fe-50at.%Co alloy powder produced by hydrogen reduction process (HRP) starting with two oxide powder mixtures of $Fe_2O_3\;and\; Co_3O_4$. The mean grain size of the HRP powders was about 40 nm and coercivity of the: powders was about 43 Oe.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.120-121
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• 2006

Magnetic properties of nanostructured materials are affected by the microstructures such as grain size (or particle size), internal strain and crystal structure. Thus, it is necessary to study the synthesis of nanostructured materials to make significant improvements in their magnetic properties. In this study, nanostructured Fe-20at.%Co and Fe-50at.%Co alloy powders were prepared by hydrogen reduction from the two oxide powder mixtures, $Fe_2O_3$ and $Co_3O_4$. Furthermore, the effect of microstructure on the magnetic properties of hydrogen reduced Fe-Co alloy powders was examined using XRD, SEM, TEM, and VSM.

• 한국자기학회지
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• 제10권6호
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• pp.291-296
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• 2000

분말사출성형법에 의한 니켈 함량이 46.6, 47.2 wt%인 퍼말로이 소결체의 제조 방법을 조사하였다. 퍼말로이의 자기특성은 소결체의 잔류탄소 및 산소의 함량에 영향을 받는 것으로 알려져 있다. 본 연구에서는소결체내의 탄소의 함량을 최소화할 수 있는 용매추출과 열분해 방법을 개발하였는데 , 잔류탄소는 분말사출을 위한 결합제의 열분해 조건에 영향을 받으며, 잔류산소는 제조 공정중 소결 분위기에 좌우되는 것으로 밝혀졌다. 분말사출성형으로 제조된 퍼말로이 소결체의 잔류탄소의 함량은 50 ppm. 잔류찬소의 함량은 150 ppm.이었으며 그 자기특성은 보자력 0.46 Oe, 최대투자율14,600의 값을 가졌다.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1195-1195
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• 2006

• 대한전기학회:학술대회논문집
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• 대한전기학회 2000년도 하계학술대회 논문집 C
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• pp.1687-1689
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• 2000

In this study, a measuring system of the initial permeability of soft-ferrite powder was developed by using a differential transformer coil. and was investigated demagnetizing factors. Magnetic powder is extensively used for a magnetic fluid and microwave absorber materials etc. In these applications, it is very important for us to measure the initial permeability of magnetic ceramic powder. Unfortunately there are not any measuring equipment and method directly up to the present.

• 한국분말재료학회지
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• 제16권4호
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• pp.249-253
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• 2009

3-D shape soft magnetic composite parts can be formed by general compaction method of powder metallurgy. In this study, the results on the high density nanostructured Fe-Si/Fe composite prepared by a warm compaction method were presented. Ball-milled Fe-25 wt.%Si powder, pure Fe powder and Si-polymer were mixed and then the powder mixture was compacted at various temperatures and pressures. Pore free density of samples up to 95% theoretical value has been obtained. The warm compacted sample prepared at 650 MPa and 240$^{\circ}C$ had highest compaction properties in comparison with other compacts prepared at 300, 400 MPa and room temperature and 120$^{\circ}C$. The magnetic properties such as core loss, magnetization saturation and coercivity were measured by B-H curve analyzer and vibration sample magnetometer.