• Title/Summary/Keyword: soak time

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SiH4 Soak Effects in the W plug CVD Process (텡스텐 플러그 CVD 공정에서 SiH4 Soak의 영향)

  • 이우선;서용진;김상용;박진성
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.1
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    • pp.1-4
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    • 2003
  • The SiH$_4$soak step is widely used to prevent the WF$_{6}$ attack to the underlayer metal using the chemical vapor deposition (CVD) method. Reduction or skipping of the SiH$_4$soak process time if lead to optimizing W-plug deposition process on via. The electrical characteristics including via resistance and the structure of W-film are affected by the time of SiH$_4$soak process. The possibility of elimination of SiH$_4$soak process is confirmed In the case of W- film grown on the stable Ti/TiN underlayer.

$SiH_4$ Soak Effects for Optimization of Tungsten Plug Deposition on TiN Barrier Metal

  • Kim, Sang-Yang;Seo, Yong-Jin;Lee, Woo-Sun;Chung, Hun-Sang;Kim, Chang-Il;Chang, Eui-Goo;Chung, Yong-Ho
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.05b
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    • pp.54-56
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    • 2001
  • The $SiH_4$ soak step is widely used during the CVD Tungsten(W) plug deposition process on the Ti/TiN barrier metal to prevent the $WF_6$ attack to the underlayer metal. We tried to reduce or skip the time of $SiH_4$ soak process to optimize W-plug deposition process on Via. The electrical characteristics including Via resistance and the structure of W film are affected according to $SiH_4$ soak time. The elimination possibility of $SiH_4$ soak process was confirmed in the case of that the CVD W film grows on the stable Ti/TiN underlayer.

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Changes in Puffer Fish Quality Induced by Soak Time in Maturing Water during Maturation of Puffer Fish Prepared via the Cutting Cranial Nerve Method (MSK Method) (뇌신경절단법(MSK법)으로 치사한 활어복의 숙성시 숙성수 침지시간에 따른 어육의 품질변화)

  • Mun, Seung-Kwon;Yoo, Seung-Seok
    • Korean journal of food and cookery science
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    • v.26 no.4
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    • pp.428-433
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    • 2010
  • The aim of this research was to determine the relationship between quality of puffer fish and soak time in maturing water. This research used the cutting cranial nerve method, which is called the MSK method. The data was analyzed using the SPSS program. Based on salinity analysis result, both moisture content and pH were measured after 20 min of soaking. As the salinity of the maturing water increased, the moisture content initially decreased then increased once the salinity was greater than 3%. However, the concentration of the maturing water did not influence the pH level. The texture properties were measured to assess the effect of soak time in the maturing water. Hardness of the sample was highest (3.99) at 20 min, and cohesiveness also showed a maximum value (0.26) at 20 min. Gumminess and chewiness were highest 1.04 and 4.09, respectively, when the fish was matured for 20 min. Sensory properties were evaluated, and springiness, umami flavor, texture, and overall preference were highest at 20 min of soak time. The results showed that maturing the puffer fish for 20 min provided the best quality of texture and sensory characteristics for the fish.

Optimum time-censored ramp soak-stress ALT plan for the Burr type XII distribution

  • Srivastava, P.W.;Gupta, T.
    • International Journal of Reliability and Applications
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    • v.15 no.2
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    • pp.125-150
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    • 2014
  • Accelerated life tests (ALTs) are extensively used to determine the reliability of a product in a short period of time. Test units are subject to elevated stresses which yield quick failures. ALT can be carried out using constant-stress, step-stress, progressive-stress, cyclic-stress or random-stress loading and their various combinations. An ALT with linearly increasing stress is ramp-stress test. Much of the previous work on planning ALTs has focused on constant-stress, step-stress, ramp-stress schemes and their various combinations where the stress is generally increased. This paper presents an optimal design of ramp soak-stress ALT model which is based on the principle of Thermal cycling. Thermal cycling involves applying high and low temperatures repeatedly over time. The optimal plan consists in finding out relevant experimental variables, namely, stress rates and stress rate change points, by minimizing variance of reliability function with pre-specified mission time under normal operating conditions. The Burr type XII life distribution and time-censored data have been used for the purpose. Burr type XII life distribution has been found appropriate for accelerated life testing experiments. The method developed has been explained using a numerical example and sensitivity analysis carried out.

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Effects of Preparation Methods and Aging Temperatures on the Properties of Rice-doenjang (전처리 방법 및 숙성온도 변화에 따른 쌀된장의 특성 변화)

  • Kim, Young-Soo;Chung, Kun-Sub;Jung, Sung-Won
    • Applied Biological Chemistry
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    • v.38 no.1
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    • pp.83-89
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    • 1995
  • Changes in physical, chemical and microbiological characteristics of rice-doenjang prepared with two different methods with or without soak treatment were investigated during 60 days of aging at $32^{\circ}C$ and $15^{\circ}C$. The pH of soak-treated rice-doenjang decreased slowly, but that of nonsoak-treated rice-doenjang decreased rapidly at the initial aging stage with the aging temperature of $32^{\circ}C$, resulting in pH 5.1 after the 60 days of aging time. Reducing sugar contents increased up to the $30{\sim}50$ days of aging time and decreased thereafter. The contents of soluble nitrogen, formol nitrogen, ammoniacal nitrogen and amino nitrogen were more affected by preparation methods than by aging temperatures. Color values depended not only on preparation methods but also on aging temperatures. There were no significant differences in the bacterial counts of rice-doenjang, while apparent differences in the yeast and mold counts by aging temperatures were observed. These results suggested that the properties of soak-treated rice-doenjang were less changed than those of nonsoak-treated rice-doenjang by aging time and temperature. And, with a view point of nitrogen compounds, aging time could be reduced by soak treatment.

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Influence of Manufacturing Environment on Delamination of Mixed Cross Laminated Timber Using Polyurethane Adhesive

  • SONG, Dabin;KIM, Keonho
    • Journal of the Korean Wood Science and Technology
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    • v.50 no.3
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    • pp.167-178
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    • 2022
  • To investigate the influence of manufacturing environment on bonding performance of mixed cross laminated wood (CLT) using polyurethane (PUR) adhesive, a boiling water soak delamination test according to the temperature and relative humidity was conducted. The 5-ply mixed CLT consisted of Japanese Larch for external and middle layer and yellow poplar for internal layer. The PUR adhesives with different opening times of 10 and 30 minutes were used. The mixed CLT was manufactured according to pressing times of PUR and manufacturing environments of summer and winter. In case of summer environment, the delamination rate of the mixed CLT with pressing time of 4 hours using a PUR adhesive with open time of 10 minutes met the requirements of KS F 2081. In case of winter environment, the delamination rate of the mixed CLT didn't meet the requirements of KS standard. However, it was possible to confirm the effect of improving the adhesive performance by adjusting the pressing time according to the open time of the adhesive under the manufacturing conditions. The delamination rate of CLT with open time 30 minutes PUR, manufactured by indirect moisture supply methods was 11.2% better than direct moisture supply methods. As a result of delamination test in the same condition of relative humidity and adhesive, it was found that the temperature of manufacturing environment influences the adhesive performance.

Manufacturing lightweight aggregate uses high content of sewage sludge for non-structural concrete

  • Phung Trong-Quyen;Kim, Duck-Mo;Mun, Kyoung-Ju;Soh, Yang-Seob
    • Proceedings of the Korea Concrete Institute Conference
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    • 2003.11a
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    • pp.124-127
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    • 2003
  • Sewage sludge and clay used as raw materials in the study. Green aggregates contain different contents by dried weight of the sewage sludge, up to 80 percent is manufactured and burning conditions of soak temperature, soak time and rate of temperature increase. influence of burning condition and mixing ratio on specific gravity of burned aggregate are discussed. The appropriate burning condition to all aggregates is evaluated. Aggregates result form the thermal treatment get specific gravity under 0.8, water absorption fewer than 7.5 percent, and aggregate crushing value from 28 to 53. As the result, aggregates can be available as the lightweight aggregate for non-structural concrete.

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Applicability of inorganic waste as binder at manufacturing of Light weight aggregates using high content sewage sludge (하수슬러지 인공경량골재 제조를 위한 무기계 폐기물의 점결제 적용성 평가)

  • Kim, Dug-Mo;Mun, Kyoung-Ju;Soh, Yang-Seob
    • Proceedings of the Korea Concrete Institute Conference
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    • 2005.05b
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    • pp.157-160
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    • 2005
  • The purpose of this study is to efficiently treat the sewage sludge discharged from sewage treatment plants and evaluate the feasibility of the manufacture of lightweight aggregates(LWA) using a large quantity of sewage sludge and inorganic waste binder ;f1y-ash, waste-stone, tailing, phosphogypsum. Then they were burned in different soak temperatures from 1190$^{circ}C$ to 1290$^{circ}C$ with fixed soak time and heating rate at 5 minutes and 20$^{circ}C$/min respectively in order to produce lightweight aggregate (LWA). Experiment were generated to evaluate the quality of LWA as well as the relationship between burning condition and product's quality.

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Quality Characteristic of lightweight aggregate using sewage sludge and fly-ash for non-structural concrete under different condition (소성조건 변화에 따른 하수슬러지와 석탄회를 이용한 비구조용 경량골재의 품질 특성)

  • Kim, Dug-Mo;Mun, Kyoung-Ju;Soh, Yang-Seob
    • Proceedings of the Korea Concrete Institute Conference
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    • 2004.11a
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    • pp.201-204
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    • 2004
  • The purpose of this study is recycling of sewage sludge and fly-ash. In this experiment, green aggregates, which is a mixture of sewage sludge and clay and fly-ash, with different content of sewage sludge (up to $80wt\%$). Then they were burned in different soak temperatures from $1190^{\circ}C\;to\;1290^{\circ}C$ with changed soak time and heating rate at 5, 7, 10 minutes and $20^{\circ}C/min$, $30^{\circ}C/min$ respectively in order to produce lightweight aggregate (LWA). Data of both experiment series were generated to evaluate the quality of LWA as well as the relationship between burning condition and product's quality.

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Effect of Overlayer Thickness of Hole Transport Material on Photovoltaic Performance in Solid-Sate Dye-Sensitized Solar Cell

  • Kim, Hui-Seon;Lee, Chang-Ryul;Jang, In-Hyuk;Kang, Wee-Kyung;Park, Nam-Gyu
    • Bulletin of the Korean Chemical Society
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    • v.33 no.2
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    • pp.670-674
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    • 2012
  • The photovoltaic performance of solid-state dye-sensitized solar cells employing hole transport material (HTM), 2,2',7,7'-tetrakis-(N,N-di-p-methoxyphenyl-amine)-9,9'-spirobifluorene (spiro-MeOTAD), has been investigated in terms of HTM overlayer thickness. Two important parameters, soak time and spin-coating rate, are varied to control the HTM thickness. Decrease in the period of loading the spiro-MeOTAD solution on $TiO_2$ layer (soak time) leads to decrease in the HTM overlayer thickness, whereas decrease in spin-coating rate increases the HTM overlayer thickness. Photocurrent density and fill factor increase with decreasing the overlayer thickness, whereas open-circuit voltage remains almost unchanged. The improved photocurrent density is mainly ascribed to the enhanced charge transport rate, associated with the improved charge collection efficiency. Among the studied HTM overlayer thicknesses, ca. 230 nm-thick HTM overlayer demonstrates best efficiency of 4.5% at AM 1.5G one sun light intensity.