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Measurement of Adhesion Strength of Polyurethane Foam to Surface-Treated Carbon Steel and Effect of Water Vapor Absorption (발포 폴리우레탄과 탄소강과의 접착 강도 측정 및 수증기 흡착의 영향)

  • 김장순;조재동;임연수
    • Polymer(Korea)
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    • v.27 no.4
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    • pp.340-348
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    • 2003
  • A previous stud-pull test was modified to measure the bond strength of polyurethane foam to carbon steel substrate. This test was appropriate in that the specimen foamed on Zn phosphated steel (0.95 kN) was broken at higher load than that of smooth galvanizing treated steel (0.38 kN). Among the samples foamed on the substrate atvarious preheating temperatures, the polyurethane foam to the steel held over 60$^{\circ}C$ exhibited very high bond strength. The samples were exposed at water vapor absorption, and, then, their bond strengths were measured. The adhesion was significantly reduced in the samples foamed on the steel at temperatures below 40$^{\circ}C$ and above 70$^{\circ}C$. For the polyurethane foams formulated with two blowing gases, the adhesion was higher by 0.03 kN in the samples with HCFC-l4lb than that with HFC-245fa. When the these samples were exposed at water vapor soaking, the reduction of the bond strength for the HFC-245fa blown sample was negligible due to smaller area fraction of void area filled with gas at interfacial area. Consequently, it was found that adhesion of polyurethane foam to metal substrate was determined by variation of microstructural features with substrate preheating, surface treatment type of blowing agent.

Quality Characteristics of Rice Noodles in Korean Market (시판 쌀국수의 품질 특성)

  • Yang, Hee-Seon;Kim, Chang-Soon
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.39 no.5
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    • pp.737-744
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    • 2010
  • In order to provide fundamental data on development of rice noodles, the quality characteristics of 10 kinds of commercial rice noodles were evaluated. Rice noodles were categorized into 3 groups for examination: 100% rice noodles with different shapes; round shape noodles with different rice contents; and noodles with different rice contents but smilar cooking method. Cooking properties, texture measurement, and sensory characteristics were evaluated. Frozen rice noodles and instant type of noodles made from composite flour of rice and wheat flour exhibited higher scores in overall acceptance. As for the form of noodle, round-shaped noodles seemed to be preferred in comparison to flat-shaped noodles. Generally, noodles with high texture scores of cohesiveness, adhesiveness, chewiness, resilience but not high score of hardness having smooth surface were preferred affecting overall acceptance scores. It appears that cooking methods and cooking time recommended by manufactures, noodle thickness and shape, packaging types such as frozen, refrigerated, and dried noodles were more influential than rice contents in aspects to the quality characteristics of the commercial rice noodle products in this study.

A Study on the Seismic Response of a Non-earthquake Resistant RC Frame Using Inelastic Dynamic Analyses (비선형 동적 해석을 이용한 비내진 상세 RC 골조의 지진거동 특성 분석)

  • Jeong, Seong-Hoon;Lee, Kwang-Ho;Lee, Soo-Kueon
    • Journal of the Korea Concrete Institute
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    • v.22 no.3
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    • pp.381-388
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    • 2010
  • In this study, characteristics of the seismic response of the non-earthquake resistant reinforced concrete (RC) frame were identified. The test building is designed to withstand only gravity loads and not in compliance with modern seismic codes. Smooth bars were utilized for the reinforcement. Members are provided with minimal amount of stirrups to withstand low levels of shear forces and the core concrete is virtually not confined. Columns are slender and more flexible than beams, and beam-column connections were built without stirrups. Through the modeling of an example RC frame, the feasibility of the fiber elementbased 3D nonlinear analysis method was investigated. Since the torsion is governed by the fundamental mode shape of the structure under dynamic loading, pushover analysis cannot predict torsional response accurately. Hence, dynamic response history analysis is a more appropriate analysis method to estimate the response of an asymmetric building. The latter method was shown to be accurate in representing global responses by the comparison of the analytical and experimental results. Analytical models without rigid links provided a good estimation of reduced stiffness and strength of the test structure due to bond-slip, by forming plastic hinges closer to the column ends. However, the absence of a proper model to represent the bond-slip poased the limitations on the current inelastic analysis schemes for the seismic analysis of buildings especially for those with round steel reinforcements. Thus, development of the appropriate bond-slip model is in need to achieve more accurate analysis.

Effects of Yukmijihwangtang, Herbal Formula, on the Liver of Aged Senescence Accelerated Mouse (SAM) P8 (육미지황탕가미방이 노화된 Senescence Accelerated Mouse(SAM) P8의 간에 미치는 영향)

  • Kim, Jeong-Sang;Sheen, Yeong-Il;Kim, Hee-Chul;Park, Min-Hee;Na, Chang-Su
    • Applied Microscopy
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    • v.30 no.4
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    • pp.327-335
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    • 2000
  • The aim of this study was to discover whether Yukmijihwangtang which was added Plygalae Radix, Acori graminei Rhizoma, has antioxidant effects on aged senescence-accelerated mouse (SAM) P8. The control group used 12 months old SAM P8 and the experimental group was treated with Yukmijihwangtang extracts from 8 to 12 months old. In the liver, the MnSOD of the control group were approximately 11% higher than that of the experimental group treated with herbal extracts, but CuZnSOD activities of the experimental group were approximately 20% higher than that of the control group. The catalase activities of the experimental group was approximately 67% higher than that of the control group. The hepatocytes, in the control group compared with the experimental group, contained the dilated cisternae of rough endoplasmic reticulum and the abnormal mitochondira which had electron-dense matrix and indistinguishable cristae. The inner cavity of the smooth endoplasmic reticulum were slightly dilated, and a number of vacuoles and transitional vesicles occured in of the hepatocytes of the control group. These results suggest that the herbal extract has an antioxidant effects on the liver of SAM P8.

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Study on Surface Morphology Control of Electroless Ni-P for Reliability Improvement of Solder Joints (솔더 조인트 신뢰성 향상을 위한 무전해 니켈-도금의 표면형상 제어)

  • Lee, Dong-Jun;Choi, Jin-Won;Cho, Seung-Hyun
    • Journal of the Microelectronics and Packaging Society
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    • v.15 no.3
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    • pp.27-33
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    • 2008
  • With increasing use of portable appliances such as PDA and cellular phone, changing environment of applications requires higher solder joint reliability. The ENIG (Electroless Nickel Immersion Gold) process has been widely used for fine pitch SMT (Surface Mount Technology) and BGA (Ball Grid Array) packaged devices due to its benefits including excellent solderability, high uniformity and substantial legibility throughout the packaging process. Its brittle fracture of solder, however, has received increasingly attentions. It was Down that fracture brittleness is mainly related with black pad resulting from galvanic nickel corrosion and P-enriched layer formation between the IMC (Intermetallic Compounds) and electroless nickel layer. Theoretically, smooth electroless Ni layer was blown to have a advantages in minimizing the black pad phenomenon by uniform solution exchange during immersion gold plating. Nevertheless, how to control the surface morphology of electroless Ni layer has been hardly blown. This study investigates an effect of surface morphology of Cu underlayer on surface morphology of electroless Ni layer. To obtain various kinds of surface morphology of Cu layer, two types of Cu etching chemical and a number of Cu etching treatment were applied.

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Vascular Responses to Vasoactive Drugs in Propylthiouracil-Treated Rat Aorta (PTU-처치가 흰쥐대동맥의 수축 및 이완 반응에 미치는 영향)

  • Shim, Il-Chung;Kim, In-Kyeom;Kim, Choong-Young
    • The Korean Journal of Pharmacology
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    • v.26 no.2
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    • pp.135-144
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    • 1990
  • The vascular responses to the vasoactive drugs were evaluated using aortic ring preparations obtained from propylthiouracil (PTU)-treated rats. The body weights and the levels of serum thyroxine $(T{_4})$ and triiodothyronine $(T{_3})$ were significantly decreased in propylthiouracil-treated rats as compared with those in age-matched control rats. The contractile responses to norepinephrine and potassium and calcium ions were significantly attenuated in aortic rings of PTU-treated rats 4 weeks after when compared with those from age-matched control animals. By the PTU treatment, however, the sensitivity to norepinephrine but not to calcium was decreased while the maximal responses to norepinephrine and calcium were reduced together. The attenuated contractile responses to the vasoconstrictors in PTU-treated rats are ascribed to the decreased ability of the muscle cells to contract. On the other hand, the relaxation responses induced by acetylcholine and histamine (endothelium-dependent relaxants) and isoproterenol and sodium nitroprusside (endothelium-independent relaxants) had tendencies to be augmented in aortic rings of PTU-treated rats when compared with those of age-matched control animals. However, the sensitivities to the endothelium-independent relaxants were different between PTU-treated and control rats whereas those to the endothelium-dependent relaxants were not. These results suggest that the altered vascular responsiveness in the PTU-treated rats seems to be due to the alteration of smooth muslce cells rather than the Influence of endothelium, and that this change is slowly progressive after hypothyroidism is evident.

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Banding Artifacts Reduction Method in Multitoning Based on Threshold Modulation of MJBNM (MJBNM의 임계값 변조를 이용한 멀티토닝에서의 띠 결점 감소 방법)

  • Park Tae-Yong;Lee Myong-Young;Son Chang-Hwan;Ha Yeong-Ho
    • Journal of the Institute of Electronics Engineers of Korea SP
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    • v.43 no.2 s.308
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    • pp.40-47
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    • 2006
  • This paper proposes a multitoning method using threshold modulation of MJBNM(Modified Jointly Blue Noise Mask) for banding artifacts reduction. As banding artifacts in multitoning appear as uniform dot distributions around the intermediate output levels, such multitone output results in discontinuity and visually unpleasing patterns in smooth transition regions. Therefore, to reduce these banding artifacts, the proposed method rearranges the dot distribution by introducing pixels in the neighborhood of output levels that occurs banding artifacts. First of all principal cause of banding artifacts are analyzed using mathematical description. Based on this analytical result, a threshold modulation technique of MJBNM which takes account of chrominance error and correlation between channels is applied. The original threshold range of MJBNM is first scaled linearly sot that the minimum and maximum of the scaled range include two pixel more than adjacent two output levels that cover an input value. In an input value is inside the vicinity of any intermediate output levels produce banding artifacts, the output is set to one of neighboring output levels based on the pointwise comparison result according to threshold modulation parameter that determines the dot density and distribution. In this case, adjacent pixels are introduced at the position where the scaled threshold values are located between two output levels and the minimum and maximum threshold values. Otherwise, a conventional multitoning method is applied. As a result, the proposed method effectively decreased the appearance of banding artifacts around the intermediate output levels. To evaluate the quality of the multitone result, HVS-WRMSE according to gray level for gray ramp image and S-CIELAB color difference for color ramp image are compared with other methods.

Effects of Prostaglandin $F_2\alpha$ on the Hormone Concentration in Blood Plasma and Morphological Changes of Corpus Luteum in Female Rats II. The Effects of Prostaglandin $F_2\alpha$ on the Structure of the Corpups Luterum of the Pregnant Rat (Prostaglandin $F_2\alpha$의 투여에 따른 자성 Rat의 혈중 Hormone 함량과 황체의 형태학적 변화 II. Prostaglandin$F_2\alpha$의 투여가 임신 Rat의 황체 구조에 미치는 영향)

  • 변명대;조유정;성태수
    • Korean Journal of Animal Reproduction
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    • v.16 no.1
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    • pp.21-38
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    • 1992
  • The present study was carried out to investigate morphologic changes in the corpus luteum of the pregnant rat by electron microscope after administration of prostaglandin F2$\alpha$(PGF2$\alpha$). Pregnant rates were treated with PGF2$\alpha$(1,500$\mu\textrm{g}$/rat) and their corpura lutea were observed morphologically. The results obtained in this study were summarized as follows ; 1. The weight of the ovaries and corpura lutea were decreased slightly at 8~24 hours after PGF2$\alpha$ administratin but no significant differences were observed. 2. The number of corpora lutea and luteal cells decreased slightly at 12~48 hours and 18~24 hours after PGF2$\alpha$ tretment but there were no signifciant differences between control and treatment. 3. The weight of uterus and the unmber of embryo decreased slightly at 96 hours and at 18~96 hours after PGF2$\alpha$ administration but no significant differences were obtained. 4. In the electron microscopic observatons, lipid droplets which are electron dense and appear in the cytoplasm moderately increased in number after PGF2$\alpha$ treatment. The lipid droplets were surrounded by mitochodria and appeared in the autophagic vacuoles. 5. Moderated and high electron dense mitochondria which are round or elongated in shape showed pleomorphism from 3 hours after PGF2$\alpha$ treatment. Destruction of tubular of vesicular cristae was observed at 6 hours after the treatment. Dense body and myelin figures in matrix of mitochondria were also appeared. 6. Well-developed smooth endoplasmic reticulum(sER) showed tubular or vesicular cisternae. A number of whorl membranes containing ribosomes, mitochondria and lipid droplets were observed at 1.5 hour after treatment. sER was abundant in luteal cells at 12 hours were treatment. 7. Well-developed Golgi pparatus appeared obviously 6 hours and more prominently at 12 hours. Those Golgi vesicles were remarkably dilated. 8. Generally, a few rough endoplasmic reticulum (rER) were appeared after treatment and cisternae showed slight dilatation. No differences among the treatments were observed. However, slight dilation of cisternae was observed at 1.5 hours after treatment. 9. Ribosomes composed of free and polyribosomes were abundant before treatment but polyribosomes were appeared at 12 to 24 hours after treatment. 10. Intercellular space were slightly extended at 3 hours and markedly extended at 12 hours. Numerous microvillous protrusions were observed at these times. Membranous multivesicular structures and autophagic vacuoles were also appeared in the intercellular space. 11. At 3 hours after the treatment, autophagic vacuoles appeared in the cytoplasm of the cell. They increased in number with time and were observed to transfer to the intercellular space. Lysosomal dense body appeared in the cytoplasm and the inclusion body was also observed in nucleus at 12 to 24 hours after treatment.

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Measurement of picosecond laser pulsewidth and pulseshape by two-photon fluorescence and noncolloinear type I second harmonic generation method (이광자 형광법과 비공선 일종 이차고조파법에 의한 피코초 레이저 펄스폭과 펄스형 측정)

  • 한기호;박종락;이재용;김현수;엄기영;변재오;공흥진
    • Korean Journal of Optics and Photonics
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    • v.7 no.3
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    • pp.251-259
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    • 1996
  • Two-Photon Fluorescence (TPF) experiment measures temporal width of an amplified short laser pulse which has passed through a four-pass Nd: glass amplifier, after selecting a single pulse from pulse train Q-switched and mode-locked(QSML) in Nd:YLF master oscillator. Determination of pulsewidth and pulseshape was also made with detection of autocorrelation trace of CW mode-locked pulse train by using noncollinear type I Second Harmonic Generation (SHG) method. The observed TPF track showed various patterns, depending on pulse-selecting position in QSML pulse train. That is, autocorrelation of a pulse extracted at front of the train displayed smooth pulse shape, while one from the trailing part of the train created many sharp spikes and substructure in the pulse. By TPF method, pulsewidth was measured to be 44.4 ps with contrast ratio of 2.86 which enabled us to find out energy fraction of a pulse to total energy, (sum of pulse and background); we obtain the value of 0.62. Pulsewidth of 46.6ps was also acquired in another SHG experiment with the help of only mode-locked pulse train. On the other hand, we confirmed that shape of the pulse is close to $sech^2$ one as a result of fitting the SHG autocorrelation signal with various functions. With simulation using this $sech^2$ type of pulse, pulsewidth reduction of the beam, having passed through four-pass amplifier, was also verified.

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Properties of Rice Extrudates Added with the Sea Tangle Powder (다시마 분말을 첨가한 쌀 압출팽화물의 특성)

  • Kim Eui Hyeong;Kook Seung Wook;Jung Soon Teck;Park Yang Kyun
    • Food Science and Preservation
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    • v.12 no.3
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    • pp.241-246
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    • 2005
  • This study showed the optimum conditions for producing rice extrudate added with the sea tangle powder, and presented the effects of moisture content, barrel temperature and the amount of sea tangle powder. From the results, the more the amount of sea tangle powder was added, the less the water absorption ratio was showed, while the more the texture became smooth, the more the expansion ratio increased. From the sensory evaluation, the best preference was obtained when the moisture content was $18\%$, and the barrel temperature was at $100^{\circ}C$. Between control and $10\%$ sea tangle, there was no significant difference in all observed parameters. But if more than $20\%$ sea tangle was added, low sensory evaluation scores were obtained due to the peculiar smell from sea tangle. From these results, addition of sea tangle below $10\%$(w/w) did not affect the quality of products.