• Journal of the Korean Ceramic Society
• /
• v.50 no.6
• /
• pp.402-409
• /
• 2013

The objective of this study was to develop a synthesis process for ${\beta}$-SiC powders to reduce the synthesis temperature and to control the particle size and to prevent particle agglomeration of the synthesized ${\beta}$-SiC powders. A phenol resin and TEOS were used as the starting materials for the carbon and Si sources, respectively. $SiO_2$-C hybrid precursors with various C/Si mole ratios were fabricated using a conventional sol-gel process. ${\beta}$-SiC powders were synthesized by a carbothermal reduction process using $SiO_2$-C hybrid precursors with various C/Si mole ratios (1.6 ~ 2.5) fabricated using a sol-gel process. In this study, the effects of excess carbon and the addition of Si powders to the $SiO_2$-C hybrid precursor on the synthesis temperature and particle size of ${\beta}$-SiC were examined. It was found that the addition of metallic Si powders to the $SiO_2$/C hybrid precursor with excess carbon reduced the synthesis temperature of the ${\beta}$-SiC powders to as low as $1300^{\circ}C$. The synthesis temperature for ${\beta}$-SiC appeared to be reduced with an increase of the C/Si mole ratio in the $SiO_2$-C hybrid precursor by a direct carburization reaction between Si and excess carbon.

• Journal of Hydrogen and New Energy
• /
• v.25 no.4
• /
• pp.436-442
• /
• 2014

$LaCoO_3$ powders synthesized by Pechini process were pulverized by planetary ball-milling to decrease particle size and characterized as a catalyst in alkaline solution for oxygen reduction and evolution reaction (ORR & OER). The changes of physical properties, such as particle size distribution, surface area and electric conductivity, were analyzed as a function of ball-milling time. Also, the variations of the crystal structure and surface morphology of ball-milled powders were examined by X-ray diffraction (XRD) and scanning electron microscopy (SEM), respectively. The electrochemically catalytic activities of the intrinsic $LaCoO_3$ powders decreased with increasing ball-milling time, but their electrochemical performance as an electrode improved by the increase of the surface area of the powder.

• Environmental Engineering Research
• /
• v.24 no.3
• /
• pp.463-473
• /
• 2019

Nanoscale zero-valent iron (nZVI) has proved to be an effective tool in applied environmental nanotechnology, where the decreased particle diameter provides a drastic change in the properties and efficiency of nanomaterials used in water purification. However, the agglomeration and colloidal instability represent a problematic and a remarkable reduction in nZVI reactivity. In view of that, this study reports a simple and cost-effective new strategy for ultra-small (< 7.5%) distributed functionalized nZVI-EG (1-9 nm), with high colloidal stability and reduction capacity. These were obtained without inert conditions, using a simple, economical synthesis methodology employing two stabilization mechanisms based on the use of non-aqueous solvent (methanol) and ethylene glycol (EG) as a stabilizer. The information from UV-Vis absorption spectroscopy and Fourier transform infrared spectroscopy suggests iron ion coordination by interaction with methanol molecules. Subsequently, after nZVI formation, particle-surface modification occurs by the addition of the EG. Size distribution analysis shows an average diameter of 4.23 nm and the predominance (> 90%) of particles with sizes < 6.10 nm. Evaluation of the stability of functionalized nZVI by sedimentation test and a dynamic light-scattering technique, demonstrated very high colloidal stability. The ultra-small particles displayed a rapid and high nitrate removal capacity from water.

• Journal of the Microelectronics and Packaging Society
• /
• v.15 no.3
• /
• pp.1-8
• /
• 2008

Effects of annealing process in a reduction ambient on thermoelectric properties of the $(Bi,Sb)_{2}Te_3$ thin films prepared by thermal evaporation have been investigated. With annealing at $300^{\circ}C$ for 2 hrs in a reduction ambient(50% $H_2$+50% Ar), the crystallinity of the $(Bi,Sb)_{2}Te_3$ thin films were substantially improved with remarkable increase in the grain size. Seebeck coefficients of the $(Bi,Sb)_{2}Te_3$ thin films increased from$\sim90{\mu}V/K$ to $\sim180{\mu}V/K$ with annealing in the reduction ambient due to decrease in the hole concentration. Power factors of the $(Bi,Sb)_{2}Te_3$ thin films were remarkably improved for $5\sim16$ times with annealing in the reduction atmosphere. After annealing in the reduction ambient, a $(Bi,Sb)_{2}Te_3$ evaporated film exhibited a maximum power factor of $18.6\times10^{-4}W/K^{2}-m$.

• The Korean Journal of Food And Nutrition
• /
• v.19 no.1
• /
• pp.91-102
• /
• 2006

The goal of this study was to find the way of reduction on food wastes in the university cafeteria. Four hundred and two students from three universities in Daejeon city were surveyed. The data were analyzed by SAS program. The results were summarized as followings: 24.95% of the total users use the university cafeteria everyday. Reasons for the utilization were listed as time saving 31.40%, near place 26.73%, low price 23.16% and no other place to eat 17.82%. Recommendations for the improvements of university cafeteria were listed as menu variation 38.26%, taste 37.83%, price decrease 10.43%. Female students left more food wastes than male students and most leaving food was side dish than Bab, Guk and Kimchi. The major reason of leaving foods was shown to be influenced by the taste and amount of foods supplied in university cafeteria. And they preferred kimchibock-kumbab to other kinds of bab. But they disliked Flounderjolim, pickled anchovies, Ggonchigui, Ginger, Burdock, Lotus root and Crown daisy. The perception of users on the reduction of food waste was 84.10% of total students. The students who know on the method of food wastes treatment were 58.26%. Improvement for reduction of food wastes of university cafeteria can be summarized to emphasize on taste, menu variation, adequate of serving size, also that should be conduct studies for systematic administration method and standard education for reduction of food waste.

• Journal of the Korea Institute of Information Security & Cryptology
• /
• v.23 no.2
• /
• pp.231-242
• /
• 2013

Recently, automated software testing methods such as fuzzing have been researched to find software vulnerabilities. The purpose of fuzzing is to disclose software vulnerabilities by providing a software with malformed data. In order to increase the probability of vulnerability discovery by fuzzing, we must solve the test suite reduction problem because the probability depends on the test case quality. In this paper, we propose a new method to solve the test suite reduction problem which is suitable for the long test case such as file. First, we suggested the length of test case as a measure in addition to old measures such as coverage and redundancy. Next we designed a test suite reduction algorithm using the new measure. In the experimental results, the proposed algorithm showed better performance in the size and length reduction ratio of the test suite than previous studies. Finally, results from an empirical study suggested the viability of our proposed measure and algorithm for file fuzzing.

• Resources Recycling
• /
• v.18 no.5
• /
• pp.12-18
• /
• 2009

The 20% Pt/C catalysts were synthesized using the chemical reduction method for polymer electrolyte fuel cell cathode and were heat-treated in the temperature range from 300 to $600^{\circ}C$. The oxygen reduction reaction of the catalysts was evaluated using the electrochemical measurement. The oxygen reduction reaction of the heat-treated Pt/C at $300^{\circ}C$ had high catalytic activity and the oxygen reduction reaction current of that was 2 times than that of non-heat treatment catalyst. It is considered that the change of the crystallinity and particle size by heat treatment could increase the catalytic activity.

• Journal of the Institute of Electronics Engineers of Korea TC
• /
• v.46 no.5
• /
• pp.88-94
• /
• 2009

We propose a scheme which reduce the computational complexity of the lattice reduction (LR) aided detector in MIMO system. The performance of the ML detection algorithm is good but the computational complexity grows exponentially with the number of antenna elements and constellation points. LR aided detector shows the same diversity with the ML scheme with relatively less complexity. But the LR scheme still requires many computations since it involves several iterations of size reduction and column vector exchange. We notice that the LR process depends not on the received signal but only on the channel matrix so we can apply LR process offline and store the results in Look-Up Table (LUT). In this paper we propose an algorithm to generate the LUT which require less memory requirement and we evaluate the performance and complexity of the proposed system. We show that the proposed system requires less computational complexity with similar detection performance compared with the conventional LR aided detector.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2009.05a
• /
• pp.355-356
• /
• 2009

The change of thermal expansion and mechanical behaviors by cold working has been investigated in Fe-29%Ni-17%Co low thermal expansion Kovar alloy. Fe-29%Ni-17%Co alloy was cold rolled gradually and prepared to plates having reduction ratio of 0%, 20%, 40%, 60%, and 80%. Annealing effect on the properties was also studied. Thermal expansion was measured from $25^{\circ}C$ to $600^{\circ}C$ with a heating rate of $5^{\circ}C$/min by using vacuum differential dilatometer. It was found that thermal expansion coefficient ($\alpha_{30{\sim}400}$) slightly decreased (reduction ration of 20%) and then remarkably increased (above reduction ration of 40%) with increasing reduction ratio of cold rolling. Thermal expansion coefficient ($\alpha_{30{\sim}400}$) was sharply decreased after annealing heat-treatment. Yield and tensile strengths were continuously increased and elongation was decreased by cold roiling. Microstructural observation and X-ray diffraction analysis results showed that the $\alpha$ phase significantly increased as the reduction ratio increased. The slight decrease of thermal expansion coefficient bellow reduction ration of 20% could be explained by the destroying short-range ordering and the decreasing of grain size. The significant increase of thermal expansion coefficient with cold rolling mainly attributed to the appearance of $\alpha$ phase. The correlation between the microstructural cause and invar phenomena for the low thermal expansion behavior was also discussed.

• The Journal of the Acoustical Society of Korea
• /
• v.35 no.6
• /
• pp.491-500
• /
• 2016

The present study describes the acoustical characteristics of the new noise barriers which can control not only noise but also wind pressure by allowing air flow through barriers. In order to investigate the sound reduction index of the air transparent noise barrier, 17 models in total were examined with various size of openings and the volume of the resonators. As a result, it was found that the sound reduction index varies with the volume of the resonator and the area of the openings. Also, it was revealed that double layer of units has more sound reduction index than the single layer of unit at the frequency band from 400 Hz to 1250 Hz. This denoted that physical features of openings and resonators affect the sound reduction index of the air transparent noise barrier.