• Journal of Korean Society for Atmospheric Environment
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• v.9 no.E
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• pp.373-381
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• 1993

To understand the human exposure levels of volatile halogenated hydrocar-bons in ambient air, a new rapid and convenient analytical method for determination of the compounds in gaseous phase was evaluated and established. The method is based upon passsive diffusion to personal sampler containing adsorbent and solvent extraction followed by purge trap/ on-column cryof-ocusing method. A new method needs no special instrumentation for gas collection because it is based upon the passive diffusion principle. The typical chromatogram obtained in this study proved that rapid and simultaneous determination of target analytes was possible with good resolution. The developed method was successfully applied to determine the volatile halogenated hydrocarbons in indoor air and the values obtained by this new method were compared with those by direct suction method. The concentration of carbon tetrachloride, 1,1,2-trichloroethylene, chloroform showed the values below 400$\mug/m^3$ except the maximum of 1,513$\mug/m^3$ of chloroform. 1,1,1-Trichloroethane showed approximately 1,000 to 5,000$\mug/m^3$ range of diurnal fluctuation in indoor air.

• Journal of the Korean Society of Safety
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• v.27 no.6
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• pp.48-53
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• 2012

This paper is purposed to develop portable electric instrument to select NI-9223(National instrument comp.) and clamp meter(HIOKI comp.), which can be used in developing electric instrument, to detect leakage current(ZCT) and current(CT) signals. In this paper, The electric instrument that can interface with current and leakage current instrument(HIOKI 9283), is developed by NI-9223 of NI comp.. HIOKI clamp meter can measure current signals certainly by high-sensitivity of 10 ${\mu}A$ resolution(leakage current : at 10 mA range) and current 1~200A range. The NI-9223 use four 16-bit analog-to-digital converters(ADCs) for true simultaneous sampling at up to 1 MS/s per channel. NI-9223 can synchronize all analog input modules installed in the same chassis to share the same start clock and/or sample clocks. The monitoring program is developed by SignalExpress of LabVIEW. The monitoring program are developed to analyze at simultaneous sampling on electrical signals such as leakage current(ZCT) and current(CT). The developed system verification tests were conducted, and portable electric instrument can be used in place which requires analysis of the actual electrical signal.

• Korean Journal of Optics and Photonics
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• v.12 no.5
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• pp.371-375
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• 2001

We have implemented a sensor head which consists of erbium doped fiber pumped by 1480 nm LD and single fiber Bragg grating for simultaneous measurement of strain and temperature. The measurement precision and speed are improved by using Mach-Zehnder interferometer instead of optical spectrum analyzer (OSA) as a demodulator. The measurement precision of temperature measured by the amplitude variation of output signal is 0.05$^{\circ}C$ and that of strain measured by the phase variation of output signal is 0.1$\mu$strain. The measurement precision of temperature and strain are improved nearly 140 times and 700 times, respectively, compared to those using an OSA with wavelength resolution of 0.97 nm as d demodulator.

• Journal of the Korean Chemical Society
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• v.37 no.5
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• pp.513-522
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• 1993

The purpose of this study is to optimize the selectivity of mobile phase solvents for separation of 25 phenols in reversed phase liquid chromatography and to accomplish the simultaneous preconcentration and separation of trace phenols from water samples. Phenols used in this study were classified into three groups, chloro-, methyl-, and nitrophenols. Quaternary solvent mobile phases were employed to improve the selectivity. Overlapping resolution maps(ORM) as a statistical simplex techniques was used to predict the optimum solvent system. Additional criterion such as pH and temperature were also investigated. In order to improve the resolution and decrease the analysis time, isoselective multisolvent gradient elution system was employed with ORM-Prism method. The simultaneous preconcentration and separation of trace phenols from water samples were performed by using XAD-2/Dowex 1-X8 tandem column. When the extraction efficiency was evaluated by sampling up to 1 L of distilled water, recovery of the phenols, except phenol, was above 90% and the limit of detection of the phenols was 5 ppb. The XAD-2/Dowex 1-X8 method was superior to C18 cartridge in terms of recovery and selectivity.

• Geophysics and Geophysical Exploration
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• v.21 no.1
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• pp.15-25
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• 2018

Seismic inversion is a high-resolution tool to delineate the subsurface structures which may contain oil or gas. On the other hand, marine controlled-source electromagnetic (mCSEM) inversion can be a direct tool to indicate hydrocarbon. Thus, the joint inversion using both EM and seismic data together not only reduces the uncertainties but also takes advantage of both data simultaneously. In this paper, we have developed a simultaneous joint inversion approach for the direct estimation of reservoir petrophysical parameters, by linking electromagnetic and seismic data through rock physics model. A cross-gradient constraint is used to enhance the resolution of the inversion image and the maximum likelihood principle is applied to the relative weighting factor which controls the balance between two disparate data. By applying the developed algorithm to the synthetic model simulating the simplified gas field, we could confirm that the high-resolution images of petrophysical parameters can be obtained. However, from the other test using the synthetic model simulating an anticline reservoir, we noticed that the joint inversion produced different images depending on the model constraint used. Therefore, we modified the algorithm which has different model weighting matrix depending on the type of model parameters. Smoothness constraint and Marquardt-Levenberg constraint were applied to the water-saturation and porosity, respectively. When the improved algorithm is applied to the anticline model again, reliable porosity and water-saturation of reservoir were obtained. The inversion results indicate that the developed joint inversion algorithm can be contributed to the calculation of the accurate oil and gas reserves directly.

• Journal of Information Technology Application
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• v.1
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• pp.99-127
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• 1999

Under the concept of global economy, the enterprises are assigning design and production environments around the world in different areas. A serious problem of information exchange emerges as companies use traditional hardware and very distinct softwares appropriate to their field of expertise. To overcome the decreased productivity due to the interruption of information, the concept of simultaneous engineering and concurrent design becomes very significant. In this article, an agent-based ship design system is developed in order to support a cooperation in distributed ship design environments. Above all, the conflicts that occur in the middle of knowledge sharing in the system must be resolved. An approach to do this is the case-based conflict resolution strategy formulated to resolve current conflict on the basis of previous resolved similar cases in agent-based collaborative design system environments. To do this conflict cases that occur in initial ship design stage are extracted. On the basis of the extracted cases, case-base is constructed. In addition conflict resolution handler located in the facilitator is developed to treat conflict problems effectively by reasoning of the case-base and thus presenting an appropriate solution. The validation of developed case-based conflict resolution strategy is evaluated by applying to collaborative design process in initial ship design stage, especially the machinery outfitting design, the preliminary design, the hullform design, and the structural design. Through the help of the cooperation of the design agents, the facilitator, the conflict resolution handler, and the case-based system, a designer can be supported effectively in his/her decision-making based on the previous cases resolved similarly.

• Journal of the Korean Chemical Society
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• v.31 no.3
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• pp.236-243
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• 1987

The optimum resolution condition of 11 organophosphorus pesticides by gas-liquid chromatography was studied using a capillary column. The injection modes and types of vaporization tubes were evaluated in relation to pesticide analysis. The best reproducibility of peak heights of pesticides was obtained by the split mode with the vaporization tube packed with quartz wool. A 25m SE-30 capillary column provided better resolution than SE-54 column for their optimum resolution. The column at $200^{\circ}C$ initially was heated by $5^{\circ}C/min\;to\;230^{\circ}C$ followed by $10^{\circ}C/min\;to\;270^{\circ}C$ and the temperatures were held constant for 5 minutes at $230^{\circ}C\;and\;270^{\circ}C$, respectively. The relative standard deviations of their retention times were less than 0.19%.

• The Journal of the Convergence on Culture Technology
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• v.10 no.5
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• pp.775-780
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• 2024

In this study, a simultaneous analysis method was developed using reversed-phase high-performance liquid chromatography(RP-HPLC) for the main components of motion sickness medication: Dimenhydrinate, Caffeine, Methyl Paraben, and Propyl Paraben. The analysis was conducted after pretreating the four components, utilizing a C18 column with Acetonitrile and H₂O as the mobile phase. UV detection was carried out at a wavelength of 254nm. As a result of the experiment, the values of Resolution(Rs) was well over Rs > 1.5, which indicates that the separation of the four components was efficient. Additionally, the symmetry factor of the components was 0.989, 1.120, 1.256, and 1.280, respectively, showing their symmetrical stability. In the stability assessment, the calibration curves for the four components showed excellent linearity with R² > 0.9991 to 0.9998. Furthermore, the limit of detection(LOD) ranged between 0.017 to 3.060㎍/ml, while the limit of quantification(LOQ) ranged between 0.050 to 9.180 ㎍/ml. The recovery rates range from 98.28% to 101.71%, and repeatability showed precision within the range of 0.447 to 0.550, and robustness confirmed values with %RSD < 2. The quantitative analysis results of this study demonstrated the effectiveness of a simultaneous analysis method for motion sickness medication components.

• Analytical Science and Technology
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• v.7 no.1
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• pp.125-132
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• 1994

Flavours in kimchee are the result of unique combination of various sugars, organic acids and amino acids as well as various volatile organic compounds including sulfur-containing compounds, terpenes, alcohols, and some volatile organic acids. In the experiment for the flavour extracting methods, dynamic headspace(DHS) is more effective for collection of volatile flavour than simultaneous distillation extraction(SDE). The best polarity available at the moment is 5% phenyl methyl poly-siloxane which will separate non-polar, intermediate and polar components with good resolution.

• Journal of Korean Vacuum Science & Technology
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• v.5 no.1
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• pp.1-6
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• 2001

We measured the simultaneous, time-resolved spectra of photon emission, electron emission, and frictional force during the abrasion single crystal MgO with a diamond stylus in vacuum. phE and EE signal can be detected with millisecond resolution during the wear of a single crystal MgO substrate with a diamond stylus. The emissions and wear behavior are strong function of surface condition, load and stylus velocity. Measurement on annealed vs as-received material show that the luminescence is primarily due to deformation, and the electron emission is primarily due to fracture. These emissions provide insight into the processes responsible for catastrophic failure of ceramics in wear applications.