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Quantitative Analysis of Silicone Oil in Antifoaming Agent (소포제중 실리콘 오일의 함량에 대한 분석)

  • Kim, Kyeong Sook;Yang, Seug Ran;LIm, Chun Sik;Park, Hyun Joo
    • Journal of the Korean Chemical Society
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    • v.44 no.4
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    • pp.337-342
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    • 2000
  • Many kinds of experiments were performed for the quality control of antifoaming agents used in thermal power pIants of KEPCO. We tried to establish more convenient ans more accurate quantitative analytical method to determine the amount of silicone oil in silicone oil type antifoaming agent regardless of the amount and/or the type of involved surface active agents. First, the amount of silicone oil was measured by gravimetric method or centrifugal method using very simple apparatus, and then was compared to the results of FT-lR spectroscopy. The centrifugal method was turned out a poor method depending upon the recovery test and virtual experiments. Some antifoaming agents showed very similar results between gravimetric method and spectroscopic methods, and the others gave very different results. We concluded that FT-lR spectroscopy is the most convenient and reliable methodto determine the amounts of silicone oil in the antifoaming agents.

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Microwave Sintering of Silver Thick Film on Glass Substrate (유리기판 위에 Ag 후막의 마이크로웨이브 소결)

  • Hwang, Seong-Jin;Veronesi, Paolo;Leonelli, Cristina;Kim, Hyung-Sun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.22-22
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    • 2009
  • The silver thick film has been used in many industries such as display, chip, solar cell, automobile, and decoration with conventional heating. The silver thick film is fired with optimal time and temperature. However, decreasing the fabrication time is required due to high production power. Furthermore, there is a problem that silver in electrode is diffused throughout any substrates. For inhibiting the Ag diffusion and long fabrication time we considered a microwave heating. We investigated firing of silver thick film with conventional and microwave heating. The temperature of substrate was measured by thermal paper and the temperature of substrate was under $100\;^{\circ}C$ The shrinkage of electrode was measured with optical microscopy and optical profilometry. The shrinkage of electrode heat treated with microwave for 5min was similar to the that fired by the conventional heating for several hours. After firing by two types of heating, the diffusion of silver was determined using a optical microscope. The microstructure of sintered silver thick film was observed by SEM. Based on our results, the microwave heating should be a candidate heating source for the fabrication electronic devices in terms of saving the tact time and preventing the contamination of substrate.

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Thermo-Mechanical Reliability of Lead-Free Surface Mount Assemblies for Auto-Mobile Application (무연 솔더가 적용된 자동차 전장부품 접합부의 열적.기계적 신뢰성 평가)

  • Ha, Sang-Su;Kim, Jong-Woong;Chae, Jong-Hyuck;Moon, Won-Chul;Hong, Tae-Hwan;Yoo, Choong-Sik;Moon, Jeong-Hoon;Jung, Seung-Boo
    • Journal of Welding and Joining
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    • v.24 no.6
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    • pp.21-27
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    • 2006
  • This study was focused on the evaluation of the thermo-mechanical board-level reliability of Pb-bearing and Pb-free surface mount assemblies. The composition of Pb-bearing solder was a typical Sn-37Pb and that of Pb-free solder used in this study was a representative Sn-3.0Ag-0.5Cu in mass %. Thermal shock test was chosen for the reliability evaluation of the solder joints. Typical $Cu_6Sn_5$ intermetallic compound (IMC) layer was formed between both solders and Cu lead frame at the as-reflowed state, while a layer of $Cu_3Sn$ was additionally formed between the $Cu_6Sn_5$ and Cu lead frame during the thermal shock testing. Thickness of the IMC layers increased with increasing thermal shock cycles, and this is very similar result with that of isothermal aging study of solder joints. Shear test of the multi layer ceramic capacitor(MLCC) joints was also performed to investigate the degradation of mechanical bonding strength of solder joints during the thermal shock testing. Failure mode of the joints after shear testing revealed that the degradation was mainly due to the excessive growth of the IMC layers during the thermal shock testing.

Text Mining Techniques for Adaptable Learning (적응적인 학습을 위한 텍스트 마이닝 기술)

  • Kim, Cheon-Shik;Jung, Myung-Hee;Hong, You-Sik
    • Journal of the Institute of Electronics Engineers of Korea CI
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    • v.45 no.3
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    • pp.31-39
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    • 2008
  • Until now, there are many technologies to improve studying ability using e-learning system. In most of e-learning system, learners are studying through the lecture materials and studying problems. The studying ability and intention, however, can be improved through the shared materials and discussion. In this case, learning materials are shared by the learners' discussion and shared materials through the board Internet and MSN. Such data was not classified by learners; it was not easy for the learners to search related valuable information. Therefore, it was not helping to learning. The technologies of most text mining extract summary data from the collection of document or classify into similar document from the complex document. In this paper, we implemented e-learning system for learners to improve learning abilities and especially, applied text mining technology to classify learning material for helping learners.

CLPP of Biofilm on Different Pipe Materials in Drinking Water Distribution System (수돗물속에서 관재질에 따른 생물막의 CLPP)

  • Lee Dong-Geun;Lee Jae-Hwa;Lee Sang-Hyeon;Ha Bae-Jin;Ha Jong-Myung
    • Journal of Life Science
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    • v.14 no.6 s.67
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    • pp.891-894
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    • 2004
  • The effect of pipe materials on biofilm communities were investigated by CLPP (community level physiology profile) using Biolog GN plates. Heterotrophic bacterial concentrations were $10^4\;-\;10^6\;CFU/cm^2$ and there was no differences between galvanized iron and carbon steel. Average optical density of Biolog plate was similar between two pipe materials. However, CLPP was different according to the type of pipe materials and exposed times to tap water, and CLPP was independent of bacterial concentration. This represents the differences of bacterial communities with pipes and water contact times.

Analysis of Diesel Nano-particle Number Distribution Characteristics for Three Different Particle Measurement Systems (3개 입자측정스시템별 디젤 극미세입자의 수량분포 특성 비교)

  • Lee, Jin-Wook;Kim, Hong-Suk;Cho, Gyu-Baek;Jeong, Young-Il
    • Transactions of the Korean Society of Automotive Engineers
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    • v.15 no.6
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    • pp.144-150
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    • 2007
  • In recent years, the particle number emissions rather than particulate mass emissions in automotive engine have become the subject of controversial discussions. Recent results from the health effects studies imply that it is possible that particulate mass does not properly correlated with the variety of health effects attributed to diesel exhaust. So, the concern is instead now focusing on nano-sized particles emitted from I. C. engine. This study has been performed for the better understanding about the engine nano-particle for 3-measurement systems with different measuring principle. Firstly, EEPS is a newly introduced instrument for size distribution measurement of engine exhaust particles. It can measure nano-particles with an adequate resolution and in real time. In this study, the characteristics of EEPS were compared with ELPI and SMPS. As a research results, EEPS showed a same effect of engine load on the size distribution with ELPI and SMPS. But the quantitative results of EEPS were more similar to SMPS than ELPI, because the EEPS and SMPS use a same principle for classifying particles by size. The capability for transient measurement of EEPS was equivalent to that of ELPI.

Fishing performance of a coastal drift net in accordance with materials of the environmentally-friendly biodegradable net twine (친환경 생분해성 그물실의 재질에 따른 연안 유자망의 어획성능 특성)

  • KIM, Seonghun;KIM, Pyungkwan;JEONG, Seongjae;BAE, Jaehyun;LIM, Jihyun;OH, Wooseok
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.54 no.2
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    • pp.97-106
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    • 2018
  • The objective of this study was to estimate physical properties and fishing performances of net twine with improved PBS copolymer resin (Bio-new), the existing PBS/PBAT blending resin (Bio-old) and commercial Nylon (Nylon). The tensile strength of Bio-new monofilament was equal to Bio-old and the elongation of Bio-new was about 6 % higher than that of Bio-old in wet condition. The physical properties tests were carried out to estimate breaking load and stiffness in dry and wet conditions, respectively. In the results, the breaking load of Nylon netting was the highest whereas the elongation of Bio-new was 1.4 times higher than that of Nylon netting in wet condition. The breaking load of Bio-old netting was about 9.2 % higher than that of Bio-new netting. However, the elongation of the Bio-new netting was about 3% higher than that of Bio-old. The stiffness of the Bio-new compared to Bio-old was improved about 34 % in dry condition and about 32 % in wet condition. The filed experiments of the fishing performance were conducted with three kinds of drift nets with different netting materials in the coastal sea of Jeju. The each experimental drift net made of different materials showed the similar fishing performance. Bio-old drift net yielded less catches of small sized yellow croaker than other drift nets. The netting materials affected the fishing performance and length distribution of catches in the drift nets.

Construction of a Novel Recombinant Baculovirus Producing Polyhedra with a Bacillus thuringiensis Cry1Ac Crystal Protein

  • Je, Yeon-Ho;Jin, Byung-Rae;Roh, Jong-Yul;Chang, Jin-Hee;Kang, Seok-Kwon
    • The Journal of Korean Society of Virology
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    • v.29 no.3
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    • pp.145-153
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    • 1999
  • We have now constructed a novel recombinant baculovirus Autographa californica nuclear polyhedrosis virus (AcNPV) producing polyhedra with Bacillus thuringiensis (Bt) CryIAc crystal protein. The recombinant polyhedra produced by the recombinant baculovirus, Btrus, in insect cells was characterized. The recombinant baculovirus has two independent transcription units in opposite orientations with two promoters, p10 or polyhedrin gene promoter each initiating transcription of either native polyhedrin or fusion protein with polyhedrin and Bt Cry1Ac crystal protein. Surprisingly, this recombinant baculovirus stably produced recombinant polyhedra which were nearly similar to those of wild-type AcNPV. The immunogold staining experiment showed that the recombinant polyhedra were assembled with polyhedrin and Bt Cry1Ac crystal protein, and contained virus particles. Insecticidal toxicity of recombinant polyhedra of Btrus to the fall webworm, Hyphantria cunea, was strikingly improved in comparison with the wild-type AcNPV.

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A comparative study of constant current control and adaptive control on electrode life time for resistance spot welding of galvanized steels (용융아연도금 강판 저항 점 용접 시 정전류 및 적응제어 적용에 따른 연속타점 특성 평가 및 고찰)

  • Seo, Jeong-Chul;Choi, Il-Dong;Son, Hong-Rea;Ji, Changwook;Kim, Chiho;Suh, Sung-Bu;Seo, Jinseok;Park, Yeong-Do
    • Journal of Welding and Joining
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    • v.33 no.2
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    • pp.47-55
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    • 2015
  • With using adaptive control of the resistance spot welding machine, the advantage on electrode life time for galvanized steels has been addressed. This study was aimed to evaluate the electrode life time of galvanized steels with applying the constant current control and the adaptive control resistance spot welding process for a comparison purpose. The growth in diameter of electrode face was similar for both the constant current and the adaptive control up to 2000 welds. The button diameter was decreased with weld numbers, however, sudden increase in button diameter with use of the adaptive control after 1500 welds was observed. The peak load was continuously decreased with increasing number of welds for both the constant current and the adaptive control. The current compensation during a weld was observed with using the adaptive control after 1800 welds since the ${\beta}$-peak on dynamic resistance curve was detected at later weld time. The current compensation with adaptive control during resistance spot welding enhanced the nugget diameter at the faying interface of steel sheets and improved the penetration to thinner steel sheet.

Phase Transformation and Microstructural Change of Alumina Membrane (알루미나 여과막의 상전이와 미세구조 변화)

  • Cheong, Hun;Choi, Duck-Kyun;Cheong, Deck-Soo
    • Korean Journal of Materials Research
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    • v.10 no.9
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    • pp.619-623
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    • 2000
  • Alumina membrane was prepared by sol-gel coating method using boehmite powder(${\Upsilon}-AlOOH$). The supported and the unsupported alumina membrane were fabricated to investigate the phase transformation and change of microstructure. It is important to control the homogeneous pore size and distribution in application of filtering process. The ${\theta}-to\;{\alpha}-AL_2O_3$ phase transformation (XRD) and the change of microstructure was investigated using scanning electron microscopy(SEM). XRD patterns showed that the supported membrane had $100^{\circ}C$ higher ${\theta}-to\;{\alpha}-AL_2O_3$ transformation temperature compared to the unsupported membrane. The similar effect was also observed for microstructural change of the membrane.

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