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Evaluation of the repair capacities and color stabilities of a resin nanoceramic and hybrid CAD/CAM blocks

  • Bahadir, Hasibe Sevilay;Bayraktar, Yusuf
    • The Journal of Advanced Prosthodontics
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    • v.12 no.3
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    • pp.140-149
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    • 2020
  • PURPOSE. This study evaluated the color stabilities of two computer-aided design and computer-aided manufacturing (CAD/CAM) blocks and a nanofill composite resin and the microtensile bond strength (µTBS) between the materials. MATERIALS AND METHODS. Twelve specimens of 4 mm height were prepared for both Lava Ultimate (L) and Vita Enamic (E) CAD/CAM blocks. Half of the specimens were thermocycled (10,000 cycle, 5° to 55℃) for each material. Both thermocycled and non-thermocycled specimens were surface treated with one of the three different methods (Er,Cr:YSGG laser, bur, or control). For each surface treatment group, one of the thermocycled and one of non-thermocycled specimens were restored using silane (Ceramic Primer II), universal adhesive (Single Bond Universal), and nanofill composite resin of 4-mm height (Filtek Ultimate). The other specimens were restored with the same procedure without using silane. For each group, 1 × 1 × 8 mm bar specimens were prepared using a microcutting device. Bar specimens were thermocycled (10,000 cycle, 5° to 55℃) and microtensile tests were performed. Staining of the materials in coffee solution was also compared using a spectrophotometer. Data were analyzed using one-way ANOVA, t-test and post-hoc Scheffe tests. RESULTS. µTBS were found similar between the thermocycled and non-thermocycled groups (P>.05). The highest µTBS (20.818 MPa) was found in the non-thermocycled, bur-ground, silane-applied E group. Silane increased µTBS at some E groups (P<.05). Composite resin specimens showed more staining than CAD/CAM blocks (P<.05). CONCLUSION. CAD/CAM blocks can be repaired with composite resins after proper surface treatments. Using silane is recommended in repair process. Color differences may be shown between CAD/CAM blocks and the nanofill composite after a certain time period.

Physical Properties of Cement Blended Finex-Slag Powder (파이넥스 슬래그 미분말을 혼합한 시멘트의 물성)

  • Lee, Keun-Jae;Byun, Seung-Ho;Choi, Hyun-Kook;Song, Jong-Taek
    • Journal of the Korea Concrete Institute
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    • v.22 no.3
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    • pp.375-380
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    • 2010
  • In this study, physical properties of cement blended with Finex-slag powder(OPC-FS) were investigated by the measurement of flowability, compressive strength, hydration heat, and $Ca(OH)_2$ content. In addition, those properties of the cement blended with blast furnace slag(OPC-BFS) were also measured for comparison. It was found that OPC-FS and OPC-BFS showed similar trend in the rheological properties. In the blended cement pastes with the $4,000\;cm^2/g$ Blaine value the flowability of OPCFS was better than that of OPC-BFS. The initial 3 day mortar compressive strength and the hydration heat of paste of OPC-FS was a bit higher, compared with OPC-BFS. Accordingly $Ca(OH)_2$ produced in the cement hydration was decreased very rapidly.

Fatigue resistance, debonding force, and failure type of fiber-reinforced composite, polyethylene ribbon-reinforced, and braided stainless steel wire lingual retainers in vitro

  • Foek, Dave Lie Sam;Yetkiner, Enver;Ozcan, Mutlu
    • The korean journal of orthodontics
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    • v.43 no.4
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    • pp.186-192
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    • 2013
  • Objective: To analyze the fatigue resistance, debonding force, and failure type of fiber-reinforced composite, polyethylene ribbon-reinforced, and braided stainless steel wire lingual retainers in vitro. Methods: Roots of human mandibular central incisors were covered with silicone, mimicking the periodontal ligament, and embedded in polymethylmethacrylate. The specimens (N = 50), with two teeth each, were randomly divided into five groups (n = 10/group) according to the retainer materials: (1) Interlig (E-glass), (2) everStick Ortho (E-glass), (3) DentaPreg Splint (S2-glass), (4) Ribbond (polyethylene), and (5) Quad Cat wire (stainless steel). After the recommended adhesive procedures, the retainers were bonded to the teeth by using flowable composite resin (Tetric Flow). The teeth were subjected to 10,00,000 cyclic loads (8 Hz, 3 - 100 N, $45^{\circ}$ angle, under $37{\pm}3^{\circ}C$ water) at their incisoproximal contact, and debonding forces were measured with a universal testing machine (1 mm/min crosshead speed). Failure sites were examined under a stereomicroscope (${\times}40$ magnification). Data were analyzed by one-way analysis of variance. Results: All the specimens survived the cyclic loading. Their mean debonding forces were not significantly different (p > 0.05). The DentaPreg Splint group (80%) showed the highest incidence of complete adhesive debonding, followed by the Interlig group (60%). The everStick Ortho group (80%) presented predominantly partial adhesive debonding. The Quad Cat wire group (50%) presented overlying composite detachment. Conclusions: Cyclic loading did not cause debonding. The retainers presented similar debonding forces but different failure types. Braided stainless steel wire retainers presented the most repairable failure type.

A COMPARATIVE STUDY ON THE ACCURACY OF IMPRESSION METHOD USING ADDITION SILICONE PUTTY IMPRESSION MATERIAL (부가중합형 Silicone putty 인상재를 이용한 인상채득 방법의 정확성에 관한 연구)

  • Je, Hong-Ji;Jeong, Chang-Mo;Jeon, Young-Chan;Hwang, Hie-Seong
    • The Journal of Korean Academy of Prosthodontics
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    • v.34 no.2
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    • pp.373-383
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    • 1996
  • In order to compare the accuracy of impression method using addition silicone putty impression material, metal master die was fabricated with 4 cylindrical abutments that were similar in shape to mandibular arch. Among the 4 abutments, two(A, D) with 8mm width and 7mm height were formed in the 2nd molar regions and the other two(B, C) with 6mm width and 7mm height were on the canine regions. Impressions were taken using one-step putty wash impression technique and two-step putty wash impression technique by three different types of impression materials(Perfect, Express, Exaflex). Upon measuring the distance between the abutments on the model by three dimensional measuring machine, the percent of devitaion of the materials were obtained, rendering the following results. The results obtained are as follows : 1. There was no significant difference in accuracy in regard with the impression method between one-step putty wash impression technique and two-step putty wash impression technique using addition silicone putty impression material. 2. There were no difference in accuracy among with three different addition silicone putty impression materials. 3. All the distances between abutments on improved stone models increased in comparison with those on the metal master model.

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Monostatic RCS Reduction by Gap-Fill with Epoxy/MWCNT in Groove Pattern

  • Choi, Won-Ho;Jang, Hong-Kyu;Shin, Jae-Hwan;Song, Tae-Hoon;Kim, Jin-Kyu;Kim, Chun-Gon
    • Journal of electromagnetic engineering and science
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    • v.12 no.1
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    • pp.101-106
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    • 2012
  • In this study, we investigated the effect of groove pattern and gap-fill with lossy materials at 15 GHz frequency of Ku-band. We used Epoxy/MWCNT composite materials as gap-fill materials. Although epoxy does not have an absorbance capability, epoxy added conductive fillers, which are multi-walled carbon nanotubes (MWCNT), can function as radar absorbing material. Specimens were fabricated with different MWCNT mass fractions (0, 0.5, 1.0, 2.0 wt%) and their permittivity in the Ku-band was measured using the waveguide technique. We investigated the effect of gap-fill on monostatic RCS by calculating RCS with and without gap-fill. For arbitrarily chosen thickness and experimentally obtained relative permittivity, we chose the relative permittivity of MWCNT at 2 wt% (${\varepsilon}_r$=8.8-j2.4), which was the lowest reflection coefficient for given thickness of 3.3 mm at V-pol. and $80^{\circ}$ incident angle. We also checked the monostatic RCS and the field intensity inside the groove channel. In the case of H-pol, gap-fill was not affected by the monostatic RCS and magnitude was similar with or without gap-fill. However, in the case of V-pol, gap-fill effectively reduced the monostatic RCS. The field intensity inside the groove channel reveals that different RCS behaviors depend on the wave polarizations.

Study of Cure Behavior of the External and Internal of Composite Parts (경화공정에 따른 복합재 부품 외부와 내부의 경화 거동 차이에 대한 연구)

  • Hyun, Dong Keun;Lee, Dong Seung;Shin, Do Hoon;Kim, Ji Hoon
    • Composites Research
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    • v.33 no.5
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    • pp.302-308
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    • 2020
  • We measured the thermal conductivity of composite materials manufactured by the autoclave and vacuum bag only processes and predicted the cure behavior of the external and internal of composite parts with a cure kinetics model. The temperature difference between the external and internal depends on the processes because of the change of thermal conductivity. In the autoclave process, the temperature and cure behavior of the internal were similar to those of the external because of the high thermal conductivity. However, the temperature of the internal of the vacuum bag only process was different from that of the external. The difference can influence the part quality and evacuation of air. Compression tests were performed to find the mechanical property using 0° unidirectional specimens. The composite of the vacuum bag only process was found to have a lower compressive strength than that of the autoclave process.

The Selection Proper Materials to Develop Specialized Root Substrate for Working with Bulb Onion Transplanter (양파 정식기용 전용 상토에 적합한 상토 재료 선발)

  • Min, Byeonggyu;ha, Injong;Lee, Jongtae;Choi, Silim;Lee, Sangdae
    • Journal of Bio-Environment Control
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    • v.25 no.2
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    • pp.100-105
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    • 2016
  • In this study we investigated the suitability of horticultural main organic root substrate materials (peatmoss, coir) for the development proper root substrate for working with bulb onion transplanter. We investigated seedling sprout ratio, growth and characteristics (bulk density, root substrate cohesion) those are suitable for mechanical transplanting by mixing with inorganic materials(red clay etc.). Although both seedling growth and root substrate bulk density were similar in peatmoss and coir based root substrates, we found that peatmoss mixing had higher root substrate cohesion compared to coir mixing. We assume that higher cohesion properties of peatmoss based root substrate will give more weight of root part during mechanical transplanting of young onion seedlings in the field. Because of this, we suggest that peatmoss is the appropriate ingredient for developing root substrates for working with bulb onion transplanter.

Physicochemical Properties of Extruded Rice Flour and Gelatinization Popped Rice Flour (제조 방법이 다른 팽화미 분말의 이화학적 특성)

  • Lee, Jung-Eun;Kim, Yu-Jin;Cho, Mun-Gyeong;Park, Shin-Young;Kim, Eun-Mi;Cho, Yong-Sik;Choi, Yoon-Hee
    • The Korean Journal of Food And Nutrition
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    • v.25 no.4
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    • pp.850-854
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    • 2012
  • This study is carried out in order to develop food materials for the promotion of rice consumption. In this study, we researched the physicochemical properties of extruded rice flour (ER) and gelatinization popped rice flour (GPR) by the extrusion process and by the popped method with milled rice and brown rice. The extrusion process used a couple of screw extruders. The extrusion parameter was kept constant at a feed moisture content of 25%, barrel temperature of $120^{\circ}C$ and screw speed of 400 rpm. GPR was prepared by batch popping machine after gelatinization of rice. In order to evaluate the physicochemical properties of ER and GPR, as well as the gelatinization rate, water soluble index (WSI), water adsorption index (WAI), DPPH radical scavenging activity and total dietary fiber content, the color value was carried out. The gelatinization rate was similar to 71.1~73.8%. Further, the results of WSI and WAI were increased at ER and GPR compared to the raw materials; ER was also higher than GPR. DPPH radical scavenging activity and total dietary fiber content showed a tendency to reduce after extrution and popping. As a result of the color value, the L value of ER decreased more than the raw materials, whereas GPR increased at a and b values.

Microstructural and Mechanical Analysis of a Friction Stir Welded Joint of Dissimilar Advanced High-Strength Steels (초고강도 합금강의 이종마찰교반 접합부에서의 미세조직 특성 및 기계적 물성 연구)

  • Lee, J.W.;Cho, H.H.;Mondal, Mounarik;Das, Hrishikesh;Hong, S.T.
    • Transactions of Materials Processing
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    • v.29 no.1
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    • pp.11-19
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    • 2020
  • For microstructural analysis of a friction stir welded (FSWed) joint of advanced high-strength steels, dual phase (DP) and complex phase (CP) steels, are studied. FSWed joints are successfully fabricated in the following four cases: (i) DP/DP; (ii) CP/CP; (iii) DP/CP, where the advancing side is DP and the retreating side is CP; (iv) CP/DP, where the advancing side is CP and the retreating side is DP. The stir zone (SZ) of (i) the DP/DP joint mainly consists of lath martensite, while the stir zone of (ii) the CP/CP joint consists not only of lath martensite but also of bainite. In the case of (iii) DP/CP and (iv) CP/DP, they exhibit a similar microstructure including acicular-shaped phases in the joints; however, cross-sections of the joints show differences in material mixing in each case. In (iv) the CP/DP joint, temperature towards the CP steel is sufficient to cause softening, thus leading to better mixing than that in (iii) DP/CP. The phases of the SZ in each of the four cases are formed by phase transformation during the FSWed process; however, the transformed phase volume fraction of CP steel is lower than that of DP steel, indicating that dynamic recrystallization occurs mainly in CP steel. The hardness values of the SZ are significantly higher than those of the base materials, especially, the SZ of (iii) the DP/CP joint has the highest value due to highest fraction of lath martensite.

Evaluation of Defiberation by Organosolv Ethanolamine Pulping for Integral Utilization of Oil Palm EFB (오일팜 바이오매스 EFB 고도 활용을 위한 Organosolv 에탄올아민 펄핑에 따른 섬유화 특성평가)

  • Kim, Chul-Hwan;Kim, Dong-Seop;Sung, Yong Joo;Hong, Hae-Eun;Kim, Se-Bin
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.1
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    • pp.67-74
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    • 2013
  • Organosolv ethanolamine pulping for oil palm empty fruit bunches(EFB) were evaluated in this study. The screen yield by the ethanolamine pulping were higher than that by the soda pulping at the same operation conditions. The higher concentration of ethanolamine solvent resulted in the higher yield and the lower contents of residual lignin. The EFB pulp fibers were the narrower in fiber width but the higher in coarseness than those of the hardwood pulp fiber, while the fiber length of the EFB pulp fiber were similar to that of the hardwood fiber. The intrinsic zero span tensile testing showed the EFB pulp fiber by the 80% ethanolamine pulping were the stronger than the fiber by the soda pulping. The results of this study supported that the ethanolamine pulping could be used as an alternative pulping method for the EFB.