• 제목/요약/키워드: scanning microscopy

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Effects of a Compatibilizer on the Tensile Properties of Low-Density Polyethylene/Modified Starch Blends

  • Park, Jin-Woo;Kim, Gue-Hyun;Moon, Jin-Bok
    • 한국환경과학회지
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    • 제22권10호
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    • pp.1287-1294
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    • 2013
  • In this study, thermoplastic starch (TPS), cross-linked starch (CS), and cross-linked starch modified with glycerol (CTPS) were prepared, and the mechanical properties of the compatibilized low-density polyethylene (LDPE) blends (LDPE/TPS, LDPE/CS, and LDPE/CTPS) were investigated and compared with those of uncompatibilized LDPE/TPS, LDPE/CS, and LDPE/CTPS blends. Maleic-anhydride-grafted polyethylene was used as the compatibilizer. The enhanced tensile strength and elongation at break for the compatibilized LDPE/modified starch blends are a result of the improved compatibility between LDPE and the modified starch, which was confirmed by torque measurements and scanning electron microscopy.

Confocal Microscopy Measurement of the Fiber Orientation in Short Fiber Reinforced Plastics

  • Lee, Kwang Seok;Lee, Seok Won;Youn, Jae Ryoun;Kang, Tae Jin;Chung, Kwansoo
    • Fibers and Polymers
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    • 제2권1호
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    • pp.163-172
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    • 2001
  • To determine three-dimensional fiber orientation states in injection-molded short fiber composites a CLSM (Confocal Laser Scanning Microscope) is used. Since the CLSM optically sections the composites, more than two cross-sections either on or below the surface of the composite can be obtained. Three dimensional fiber orientation states can be determined with geometric parameters of fibers on two parallel cross-sections. For experiment, carbon fiber reinforced polystyrene is examined by the CLSM. Geometric parameters of fibers are measured by image analysis. In order to compactly describe fiber orientation states, orientation tensors are used. Orientation tensors are determined at different positions of the prepared specimen. Three dimensional orientation states are obtained without the difficulty in determining the out-of-plane angles by utilizing images on two parallel planes acquired by the CLSM. Orientation states are different at different positions and show the shell-core structure along the thickness of the specimen.

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방전가공된 공구강표면의 연마재 유동가공에 관한 연구 (A Study of Abrasive Flow Machining on EDMed Surfacs of Tool Steel)

  • 최재찬;김창호;허관도
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 1996년도 춘계학술대회 논문집
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    • pp.8-13
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    • 1996
  • A relatively new non-traditional finishing process called Abrasive Flow Machining(AFM) is being used to deburr, polish and radius workpiece or produce compressive residual stresses by flowing an abrasive-laden viscoelastic compound across the surface to be machined. This paper presents the effects of AFM on surfaces of tool steel produced by EDM and W-EDM. Using AFM, white layer produced by EDM is erased almost equally and the amount of metal removal is significantly affected the initally machined surface condition of workpiece. The dimension of workiece is enlarged and its surface roughness is improved as AFM time is increased. The optimal AFM time can be established from the experimental results. It is considered that the grinding method lide AFM is useful to grind complex or slim geometry of workpiece even. Scanning Electron Microscopy(SEM) was used to study the surface characteristics of the workpiece before and after AFM.

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주사 전자현미경의 이미지 해상도 향상을 위한 방안 및 실험적 검증 (Methodologies and Verifications for Enhancing Resolution of a Scanning Electron Microscopy)

  • 김동환;김영대;박만진;장동영;박근
    • 한국공작기계학회논문집
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    • 제16권5호
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    • pp.122-128
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    • 2007
  • The electric part of thermal SEM(Scanning Electron Microscopy) consists of high voltage generation, lens control, and image processing. Several methodologies for enhancing SEM image are addressed and those results are verified through analyses and experiments. The controller employes a DSP(Digital Signal Processing), making the system more flexible and convenient than the classical analogue based controller. In some parts based the analog circuit, there are inevitable sources of noise and image distortion. The experimental investigation is provided along with analytical proof to enhance the SEM image.

압입 표면형상의 구현과 체적계산법 (Indented Surface Configuration and its Volume Calculation)

  • 양재용;윤문철
    • 한국생산제조학회지
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    • 제21권5호
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    • pp.708-713
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    • 2012
  • The indented geometry for rockwell hardness indenter has been configured by using Confocal Laser Scanning Microscopy (CLSM). For this purpose, the CLSM can be well suited to construct the three-dimensional indented volume from the indented surface by rockwell hardness tester. Furthermore, the height data of HEI(height encoded image) by CLSM must be acquired at first and converted to indented surface later. And the indented surface patterns enable us to predict the indenter shape and volume. This volume can be used to study the rockwell hardness model as a volume parameter. As a result, the technique performed in this study by combining the CLSM with compensation technique is an excellent one to obtain the geometries of indented surfaces over a wide range of surface resolution in a micro scale. And it can be used for micro volume calculation.

전자현미경 수준에서의 목재부후균의 미세구조학적 고찰 (Ultrastructural Description of Some Wood Degrading Fungi at Light Microscopic and Scanning Electron Microscopic Levels)

  • 이양수
    • Applied Microscopy
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    • 제34권4호
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    • pp.271-276
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    • 2004
  • Biscogniauxia속에 속한 대다수의 종들은 목재를 분해균으로 알려져 있으며, 목질내지는 탄소질이며 암갈색의 자좌를 가진 Xylariales에 속하여 있다. Daldinia concentrica와 Biscogniauxia에 속한 목재부후균이 심하게 부후된 활엽수에서 분리되었으며 이는 광학현미경 및 전자현미경을 이용하여 고찰하였다. Daldinia concentrica는 국내 최초의 전자현미경을 이용한 미세구조학적 고찰이다. 또한, Biscogniauxia속 미동정 부후균은 $11.4\;15.6{\times}9.6\;12.0{\mu}m$ 크기의 자낭포자를 가지고 있으며, 국내에서 발견된 비슷한 종들과 비교 분석하였다.

Bimorph PZT를 이용한 고밀도 광학헤드의 정밀위치 및 간극제어 (Precision Position and Gap Control for High Density Optical Head Using Bimorph PZT)

  • 권영기;홍어진;박태욱;박노철;양현석;박영필
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 2004년도 춘계학술대회논문집
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    • pp.888-893
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    • 2004
  • This paper proposed a dual actuator using bimorph PZT for information storage device based on prove array NSOM(Near-field Scanning Optical Microscopy). The gap between the media and the optical head should be maintained within the optical tolerance. Therefore, a new actuator having high sensitivity is required. Bimorph PZT, which has fast access time and high sensitivity characteristic, is suitable for this precise actuating system. This paper is focused on derivation of mathematical model of dual bimorph PZT actuator and control algorithm. Hamilton's principle was used for mathematical model. The model is verified by FEA(Finite Element Analysis), and compared with experimental results. Different control algorithms were used f3r two bimorph PZT actuating same direction and opposite direction. The gap between recording media and optical head was controlled within 20nm in experiment.

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한국재래산양의 태아 및 신생아의 식도 발달에 관하여 (Development on the esophagus of fetuses and neonates in Korean native goats)

  • 정순희;김종섭;허찬권
    • 대한수의학회지
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    • 제34권4호
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    • pp.679-686
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    • 1994
  • The development of esophagus in fetuses between 60, 90, 120 days of gestation and neonates of Korean native goats was investigated by light, scanning electron microscopy. The results were summarized as follows; 1. The esophageal wall appeared to be differentiated into the epithelium, lamina propria, tunica muscularis and tunica adventitia at 60 days of gestation. The esophageal epithelium was stratified cuboidal at 60 days, being transformed into stratified squamous epithelium at 90 days, and completely transformed into squamous epithelium an 120 days. 2. In scanning electron microscopy, the longitudinal furrows and ridges appeared on the epithelium of the esophagus of the fetuses at 60 days of gestation. The longitudinal furrow became deeper and microplicae appeared in 90-day-old fetuses. The transverse and longitudinal folds appeared on the epithelial surface of esophagus and the esophageal epithelium started to be keratinized in the neonates.

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Dimensions of Structural Elements in Fusiform Ray of Sitka Spruce (Picea sitchensis (Bong.) Carr.) Affecting Radial Permeability

  • Usta, Ilker
    • Journal of the Korean Wood Science and Technology
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    • 제33권5호통권133호
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    • pp.1-6
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    • 2005
  • The anatomical structure of fusiform ray was examined by scanning electron microscopy (and microscopic images were analysed by image analyser) to explain the differences in radial fluid uptake between the extremes in the radial treatment data, i.e. between the selected trees of QCI (Queen Charlotte Islands in Rhondda, South Wales) and SO (South Oregon in Dalby, North-East England) planted in the UK. The ray structure of these two seed origins was examined microscopically and different patterns of ray composition were observed. The most important anatomical features influencing radial permeability were the nature of fusiform ray, and the condition of the resin canals, epithelial cells and intercellular spaces in particular.

Two-dimensional Chiral Honeycomb Structures of Unnatural Amino Acids on Au(111)

  • Yang, Sena;Jeon, Aram;Lee, Hee-Seung;Kim, Sehun
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2014년도 제46회 동계 정기학술대회 초록집
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    • pp.191.1-191.1
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    • 2014
  • Crystallization has become the most popular technique for the separation of enantiomers since the Pasteur's discovery. To investigate mechanism of crystallization of chiral molecules, it is necessary to study self-assembled structures on two-dimensional surface. Here, we have studied two-dimensional self-assembled structures of an unnatural amino acid, (S)-${\beta}$-methyl naphthalen-1-${\gamma}$-aminobutyric acid (${\gamma}^2$-1-naphthylalanine) on Au(111) surface at 150 K using scanning tunneling microscopy (STM). At initial stage, we found two chiral honeycomb structures which are counter-clockwise and clockwise configurations in one domain. The molecules are arranged around molecular vacancies, dark hole. By further increasing the amounts of adsorbed ${\gamma}^2$-1-naphthylalanine, a well-ordered square packed structure was observed. In addition, we found the other structure that molecules were trapped in the pore of the hexagonal molecular assembly.

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