• Title/Summary/Keyword: scanning measurements

Search Result 741, Processing Time 0.026 seconds

Characteristics and Processing Effects of $ZrO_2$ Thin Films grown by Metal-Organic Molecular Beam Epitaxy (금속 유기 분자 빔 에피택시로 성장시킨 $ZrO_2$ 박막의 특성과 공정변수가 박막 성장률에 미치는 영향)

  • Kim, Myung-Suk;Go, Young-Don;Hong, Jang-Hyuk;Jeong, Min-Chang;Myoung, Jae-Min;Yun, Il-Gu
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2003.07a
    • /
    • pp.452-455
    • /
    • 2003
  • [ $ZrO_2$ ] dielectric layers were grown on the p-type Si (100) substrate by metalorganic molecular beam epitaxy(MOMBE). Zrconium t-butoxide, $Zr(O{\cdot}t-C_4H_9)_4$ was used as a Zr precursor and Argon gas was used as a carrier gas. The thickness of the layers was measured by scanning electron microscopy (SEM) and the properties of the $ZrO_2$ layers were evaluated by X-ray diffraction, high frequency capacitance-voltage measurement. and HF C-V measurements have shown that $ZrO_2$ layer grown by MOMBE has a high dielectric constant (k=18-19). The growth rate is affected by various process variables such as substrate temperature, bubbler temperature, Ar, and $O_2$ gas flows.

  • PDF

The Effect of Far Infrared Radiation of $\beta$-Spodumene Glass-Ceramics Flims Coated on Iron Substrate by Sol-Gel Technique (졸-겔법에 의한 금속기판상의 $\beta$-spodumene 결정성유리의 박영도포와 원적외선상세성)

  • 양중식;신현택;박종옥
    • Journal of Surface Science and Engineering
    • /
    • v.27 no.2
    • /
    • pp.99-108
    • /
    • 1994
  • Films of glass-ceramics $Li_2O-Al_2O_3-SiO_2$(LAS)system were prepared on substrate of an iron plate(SCP) by sol-gel technique using metal alkoxide such as Si$(OC_2H_5)_4$,Al$(OC_2H_9)_3$) and Ti$(OC_2H_6)_4$). Sol which was made by means of simple spray coating, on the substrate was hydrolyzed at 75~$80^{\circ}C$ in moisture cabinet (80~90 % humidity) to form the multicomponent gel. The films up to about 0.8~1.0$mu extrm{m}$ in thickness can be obtained by repeating operation, spraylongrightarrowhydrolysis and condensationlongrightarrowdryinglongrightarrowheating and crystallization at $700^{\circ}C$ for 3~5min. The far-infrared radiation spectra of the coated films on substrate were examined by FT-IR and of films was also observed by scanning electron micrograph technique. The thermal evaluation of the gel-film is followed by TG/DTA measurements. The structure evaluation is followedd X-ray diffraction. These results suggest that this process is applicable to far-infrared radiat at thin film technique.

  • PDF

Classification of Precipitation Type Using the Wind Profiler Observations and Analysis of the Associated Synoptic Conditions: Years 2003-2005 (윈드프로파일러 관측 자료를 이용한 장마철 강수 형태 분류와 관련된 종관장의 특성 분석: 2003년-2005년)

  • Won, Hye-Yeong;Jo, Cheon-Ho;Baek, Seon-Gyun
    • Atmosphere
    • /
    • v.16 no.3
    • /
    • pp.235-246
    • /
    • 2006
  • Remote sensing techniques using satellites or the scanning weather radars depend mostly on the presence of clouds or precipitation, and leave the extensive regions of clear air unobserved. But wind profilers provide the most direct measurements of mesoscale vertical air motion in the troposphere, even in the context of heavy precipitation. In this paper, the precipitation events during the Changma period was classified into 4 precipitation types - stratiform, mixed stratiform/ convective, deep convective, and shallow convective. The parameters for the classification of analysis are the vertical structure of reflectivity, Doppler velocity, and spectral width measured with the wind profiler at Haenam for a three-year period (2003-2005). In addition, the synoptic fields and total amount of precipitation were analyzed using the Global Final Analyses (FNL) data and the Global Precipitation Climatology Project (GPCP) data. During the Changma period, the results show that the stratiform type was dominant under the moist-neutral atmosphere in 2003, whereas the deep convective type was under the moist unstable condition in 2004. The stratiform type was no less popular than the deep convective type among four seasons because the moist neutral layer was formed by the convergence between the upper-level jet and the low-level jet, and by the moisture transport along the western rim of the North Pacific subtropical anticyclone.

Development of Infrared Telemeter for Autonomous Orchard Vehicle (과수원용 차량의 자율주행을 위한 적외선 측거 장치개발)

  • 장익주;김태한;이상민
    • Journal of Biosystems Engineering
    • /
    • v.25 no.2
    • /
    • pp.131-140
    • /
    • 2000
  • Spraying operation is one of the most essential in an orchard management and it is also hazardous to human body. for automatic and unmanned spraying , an autonomous travelling vehicle is demanded. In this study, a telemeter was developed using infrared beam which could detect trunks and obstacles measure distance and direction from the vehicle travelling in the orchard. The telemeter system was composed of two infrared LED transmitters and receivers, a beam scanning device for continuous object detection , two rotary encoders for angle detector, and a beam level controller for uneven soil surface. The detected distance and direction signal s were sent to personal computer which made for the system display the angular and distance measurements through I/O board. According to a field test in an apple farm, the system detected up to 10m distance under 12 V of transmitted beam intensity, however, it was recommended that the proper beam transmit intensity be 7 v at the 10 m distance, because of the negative effect to human body at 12 V. The error rate of this system was 0.92 % when the actual distance was compared to measured one. The system was feasible at the small error rate. The developed telemeter system was an important part for autonomous travelling vehicle provided the real time object recognition . A direction control system could be constructed suing the system. It is expected that the system could greatly contribute to the development of autonomous farm vehicle.

  • PDF

Thermal and Mechanical Properties of Biodegradable PBAT and MWCNT Composites (생분해성 PBAT와 MWCNT 복합재료의 제조 및 열적, 기계적 특성)

  • Cho, Yong-Kwang;Bae, Seong-Guk;Noh, Geon Ho;Park, Chan-Young;Lee, Won-Ki;Jang, Seong-Ho
    • Journal of Environmental Science International
    • /
    • v.26 no.1
    • /
    • pp.79-85
    • /
    • 2017
  • Multi-Walled Carbon Nanotubes (MWCNTs) were modified with epoxy and aminosilane diethanolamine (DEA), and nanocomposites of poly(butylene adipate-co-terephthalate) (PBAT) and the modified MWCNTs were prepared with the aim of improving the physical properties of biodegradable PBAT. The physical and the thermal properties of the PBAT/MWCNT nanocomposites were investigated using various techniques. Fourier transform infrared spectroscopy measurements revealed that the MWCNTs were efficiently modified with DEA. Scanning electron micrographs of the nanocomposites indicated that the modified MWCNTs were dispersed homogeneously in PBAT. The thermal stability of the nanocomposite decreased with increase in the content of epoxy-MWCNT-DEA due to the poor thermal stabilities of epoxy and amino silane DEA. However, the surface hydrophobicity of the nanocomposite increased. The highest stress (170% of PBAT) was observed when the content of epoxy-MWCNT-DEA in the nanocomposite was 2 wt%.

Effect of pH on the Size Distribution of Au Nanoparticles

  • Kang, Ae-Yeon;Park, Dae-Keun;Lee, Cho-Yeon;Yun, Wan-Soo
    • Proceedings of the Korean Vacuum Society Conference
    • /
    • 2011.08a
    • /
    • pp.390-390
    • /
    • 2011
  • The size distribution of gold nanoparticles (NPs) is an important factor in their application to various fields of nanotechnology such as nanodevice fabrication, nanobio measurements, medical diagnosis, and so on, since the properties of nanoparticles depend on the size. As the pH of the reaction mixture was increased, the size distribution of gold NPs synthesized via sodium citrate reduction method was getting narrower and it finally became quite mono-dispersive when the pH was higher than ca. 7. 0.1M NaOH solution was used in controlling the pH, while the ratio between sodium citrate and HAuCl4 was fixed to 3:1 whose initial pH was about 5. Scanning and tunneling electron microscopy and UV/Vis spectrometry were used to characterize the resulting Au NPs. The change of the size distribution of the NPs was discussed with the change of the reaction rate related to the change of hydroxyl ion concentration.

  • PDF

Bending Performance Evaluation of Reinforced Aluminum Square Tube Beams (보강 알루미늄 사각관 보의 굽힘 성능평가)

  • Lee Sung-Hyuk;Choi Nak-Sam
    • Transactions of the Korean Society of Automotive Engineers
    • /
    • v.13 no.5
    • /
    • pp.171-180
    • /
    • 2005
  • Bending performances of aluminum square tube beams reinforced by aluminum plates under three point bending loads have been evaluated using experimental tests combined with theoretical and finite element analyses. A finite element simulation for the three-point bending test was performed. Basic properties of aluminum materials used for initial input data of the finite element simulation were obtained from the true stress-true strain curves of specimens which had been extracted from the Al tube beams. True stresses were determined from applied loads and cross-sectional area records of a tensile specimen with a rectangular cross-section by real-time photographing, and true strains were obtained from in-situ local elongation measurements of the specimen gage portion by the multi-point scanning laser extensometer. Six kinds of aluminum tube beam specimens adhered by aluminum plates were employed fur the bending test. The bending deformation behaviors up to the maximum load described by the numerical simulation were in good agreement with experimental ones. After passing the maximum load, reinforcing plate was debonded from the aluminum tube beam. An aluminum tube beam strengthened by aluminum plate on the upper web showed an excellent bending capability.

Investigation of Ball Size Effect on Microstructure and Thermoelectric Properties of p-type BiSbTe by Mechanical Alloying

  • Lwin, May Likha;Yoon, Sang-min;Madavali, Babu;Lee, Chul-Hee;Hong, Soon-Jik
    • Journal of Powder Materials
    • /
    • v.23 no.2
    • /
    • pp.120-125
    • /
    • 2016
  • P-type ternary $Bi_{0.5}Sb_{1.5}Te_3$ alloys are fabricated via mechanical alloying (MA) and spark plasma sintering (SPS). Different ball sizes are used in the MA process, and their effect on the microstructure; hardness, and thermoelectric properties of the p-type BiSbTe alloys are investigated. The phases of milled powders and bulks are identified using an X-ray diffraction technique. The morphology of milled powders and fracture surface of compacted samples are examined using scanning electron microscopy. The morphology, phase, and grain structures of the samples are not altered by the use of different ball sizes in the MA process. Measurements of the thermoelectric (TE) transport properties including the electrical conductivity, Seebeck coefficient, and power factor are measured at temperatures of 300-400 K for samples treated by SPS. The TE properties do not depend on the ball size used in the MA process.

Synthesis and Physical Properties of Liquid-Crystalline Polyurethanes (液晶性 Polyurethane의 合成과 物性에 關한 硏究)

  • Lee, Jong Back;Song, Jin Cherl;Choi, Dae Woong
    • Textile Coloration and Finishing
    • /
    • v.8 no.1
    • /
    • pp.56-63
    • /
    • 1996
  • A number of thermotropic liquid crystalline polyurethanes with mesogenic unit were synthesized by polyaddition of a para-type diisocyanate such as 1, 4-phenylene diisocyanate(1,4-PDI) with 4, 4'-bis($\omega$-hydorxyalkoxy) biphenyls($BP{m}$) in DMF. The thermal and liquid crystab line properties were examined by differential scanning calorimetry(DSC), polarized optical microscopy, and wide-angle X-ray scattering(WAXS). Intrinsic viscosities of the polymers exbibited two endothermic peaks correspondinding to phase transitions of melting and isotropization. For example, polyurethane(1,4-PDI/($BP{11}$) ) was found to display a liquid crystalline phase between 177 to 205$^{\circ}C$. In order to know how the hydrogen bonding interaction affects the formation of mesophases in polyurethane 1, 4-PDI/($BP{8}$) / thermal processing FT-IR measurements were carried out. It was found that the stretches regarded as shift to higher frequency region with increasing temperature which showed grdually their liquid crystalline phase

  • PDF

Structural and Electrical Properties of Cu(In,Ga)Se2 Thin Films Prepared by RF Magnetron Sputtering without Selenization (셀렌화 공정을 제외한 RF 마그네트론 스퍼터링으로 제작된 Cu(In,Ga)Se2 박막의 구조 및 전기적 특성)

  • Choi, Jung-Kyu;Hwang, Dong-Hyun;Son, Young-Guk
    • Journal of Surface Science and Engineering
    • /
    • v.46 no.2
    • /
    • pp.75-79
    • /
    • 2013
  • A one-step route was developed to fabricate $Cu(In,Ga)Se_2$ (CIGS) thin films by radio frequency (RF) magnetron sputtering from a single quaternary $CuIn_{0.75}Ga_{0.25}Se_2$ target. The effects of the substrate temperatures on the structural and electrical properties of the CIGS layers were investigated by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive X-ray spectroscopy (EDS) and Hall effect measurements. All the deposited films showed a preferential orientation along the (112) direction. The films deposited at $300^{\circ}C$ and $400^{\circ}C$ revealed that chalcopyrite main (112) peak and weak prominent peaks of (220)/(204) and (312)/(116), indicating polycrystalline structures. The element ratio of the deposited film at $300^{\circ}C$ were almost the same as the near-optimum value. The carrier concentration of the films decreased with increasing substrate temperatures.