• 제목/요약/키워드: sample environment

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국내 수질측정대행업에 대한 생태독성 숙련도시험 평가 (Evaluation of Whole Effluent Toxicity (WET) Proficiency Testing for Water Quality Measurement Agencies in Korea)

  • 박우상;김상훈
    • 한국물환경학회지
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    • 제29권4호
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    • pp.568-573
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    • 2013
  • In this study, we conducted whole effluent toxicity (WET) proficiency testing based on the results which $EC_{50}$ value of 3 types (A, B, C) unknown samples calculated from 32 water quality measurement agencies in Korea. WET proficiency testing was expected to their improve of analysis skill and ensure reliability of analysis results. Ultimately, it is intended to promote the reliable enforcement of WET. WET proficiency testing was evaluated using the z-score, robust z-score and the results showed that 30 participating agencies were "compliance". In addition, $EC_{50}$ values of "unknown sample A" were the normal distribution. Therefore, "unknown sample A" was considered as the most suitable standard toxicity substance.

분산환경을 위한 Sample Distributed Virtual Machine 설계 및 구현 (A Design and Implementation of Sample Distributed Virtual Machine for Distributed Environment)

  • 양일등;이석희;김성열
    • 정보처리학회논문지A
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    • 제11A권4호
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    • pp.251-256
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    • 2004
  • 고성능 컴퓨터들의 대량 보급으로 인해 다양한 종류의 분산 자원이 주위에 산재해 있다. 이러한 분산 자원을 이용하는데 각 분야별 시스템들의 개념, 모듈, 운영 및 관리를 배제하고 사용할 수 있다면 최소한의 비용으로 분산 자원을 사용할 수 있을 젓이다. 이에 '분산환경에 적용될수 있는 DVM 및 DESPL의 제안'을 통해 제안된 내용중 그 일부를 수용하여 SDVM을 설계 및 구현한다. SDVM을 이용하는 사용자는 분산 환경의 개념없이 최소한의 비용으로 분산된 자원을 사용할 수 있다.

인천항 고철 하역 작업시 발생하는 비산분진 억제를 위한 계면활성제의 적용 및 기초 성능 평가 (The Application of Surfactants to the Suppression of Fugitive Dust Generated from the Scrap Metal Loading Field in Inchon Port and Preliminary Evaluation on Their Wetting Capability)

  • 이보영;유용호;정용원;김진
    • 한국대기환경학회지
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    • 제17권1호
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    • pp.85-96
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    • 2001
  • The objective of this study is to develop the water spraying which can effectively by applied to the control or suppression of the fugitive dust generated from the scrap metal handling area at the Port of Inchon. As a first step toward this goal, we carried out some preliminary analyses on the chemical composition, physical shape, and particle size distribution of the sample dust. Next, to quantitatively investigate the effect of adding surfactants to the spraying water on the wettability of the sample dust, the Standard Sink Test was carried out for four different surfactants and at six different concentrations using the surfactants considered in this study. Results of from the preliminary analysis indicated that the main chemical component consisting of the sample dust is Goethite(FeO(OH)) and that the particles smaller than 10 ${\mu}{\textrm}{m}$ in geometric diameter occupy about 36% of the sample dust in mass. This result implies that the fugitive dust generated from the scrap metal handling area at the Port of Inchon should affect the environment nearby more than we have expected. This is because of relatively large mass percentage of the small metal particles less than 10${\mu}{\textrm}{m}$ in geometric diameter, what we may call respirable particles. As for the results of the Standard Sink Test, higher surfactant concentration tends to result in the higher wettability of the sample dust for the surfactants considered in this study, which in turn ensures the high particle collection efficiency of the droplets generated from the water spraying system. Based upon this preliminary results, studies to develop more sophisticated scaled model for dynamic test in underway and the effort to find the best surfactants as well as the optimum operating conditions are being made at the same time.

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QuEChERS 전처리법과 GC-TOF/MS, ECD, NPD를 이용한 잔류농약 다성분분석 (Multi-residue Analysis of Pesticides using GC-TOF/MS, ECD, NPD with QuEChERS Sample Preparation)

  • 박정욱;김애경;김종필;이향희;박덕웅;문수진;하동룡;김은선;서계원
    • 농약과학회지
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    • 제18권4호
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    • pp.278-295
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    • 2014
  • 농수산물검사소에서는 빠르고 정확한 잔류농약검사법이 필요하므로 QuEChERS 시료 전처리법과 GC-TOF/MS(가스크로마토그래피 비행시간질량분석기와 GC-ECD(전자포획검출기), GC-NPD(질소인검출기) 기기분석을 이용하여 잔류농약 동시다성분 분석의 가능성을 살펴보았다. GC-TOF/MS에서는 138종의 농약성분을 0.3, $0.5{\mu}g/g$수준으로 상추에 처리 후 회수율 측정을 하였다. 동시다성분 회수율기준 70~130% 범위에 들어오고 표준편차 20% 이내인 농약은 61종이었다. GC-ECD, NPD에서는 145종의 농약성분 중 71종이 적정한 회수율 범위 내에 들었다. 이러한 결과는 일부 농약성분에 대해 QuEChERS 시료 전처리법과 GC-TOF/MS, GC-ECD, NPD를을 이용한 잔류농약 동시다성분분석 방법 적용 가능성을 보여주었다.

온라인 자동화 시료 전처리 및 HR Orbitrap LC/ESI-MS를 이용한 환경시료 중 잔류 의약물질 분석방법 확립 (Establishment of the Analytical Method for Residual Pharmaceuticals in Raw Water Using Online Sample Preparation and High Resolution Orbitrap LC/ESI-MS)

  • 황윤정;신상희;박종숙
    • 한국물환경학회지
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    • 제29권3호
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    • pp.409-419
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    • 2013
  • In this study, the analytical method for 27 residual pharmaceuticals in raw water was developed. Online sample preconcentration/extraction and analysis with high resolution Orbitrap mass spectrometry (LC-ESI/Orbitrap MS) were performed. The calibration curves showed good linearities (above $r^2$ = 0.998) in the range of 5 ~ 1,000 ng/L. The method detection limit and the limit of quantification were 1.1 ~ 10.0 ng/L and 3.4 ~ 31.7 ng/L, respectively. Recoveries of the target compounds were between 70.1% and 115.8% (except cefadroxil, cefradine, vancomycin, and iopromide (50.2 ~ 67.0%)). The optimized analytical method can be useful to determine the residual pharmaceuticals in raw water.

대학도서관 서비스 품질의 측정 (Measuring Service Quality in Academic Libraries)

  • 박동진;윤동원
    • 한국도서관정보학회지
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    • 제30권4호
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    • pp.183-206
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    • 1999
  • The purpose of this research is to evaluate the service quality measure and service quality level between one sample library and the other. Most typically, service quality is defined in terms of reducing the gap between customer expectations and the actual service provided. This research also focuses on gap reduction. Service quality concept was originally discussed in a commercial environment and may require some adaptation to the non-commercial environment of the academic library. A revised service quality measure that developed by P. J. Calvert and P. Hernon(1996) was used for this research. Results showed that service quality measure of this research was reliable(99 service quality items scale's Cronbach Alpha coefficient was 0.983) and was validated by correlation and factor analysis. Therefore service quality measure of this research will be applied positively for academic libraries. And this research showed that the service quality level of sample academic library was inferior to that of the others. The service quality of sample academic library should be improved to meet the customer's needs and expectations immediately.

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폐광산의 AMD 오염영역탐지를 위한 지구물리탐사 (Geophysical Surveys for Mapping of the AMD Contaminant Channels at an Abandoned Mine)

  • 김지수;최상훈;한수형
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2000년도 추계학술대회
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    • pp.258-261
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    • 2000
  • Geophysical surveys (electrical resistivity, self-potential, and magnetic methods) and streamwater sample analysis have been carried out at a site of tailings of waste deposits in an abandoned mine, Jangpoong, which is situated in Kowesan-Gun, Chungbuk-Do. The research was aimed at investigating the suitability of the various geophysical methods for detection of AMD (acid mine drainage) paths, and ultimately mapping of preferred AMD flow channels by incorporating the water sample analysis. Electrical resistivity section from the dipole-dipole line represents the low-resistivity zone trending northwest toward the stream nearby. The positions of the resistivity anomalies for AMD channels are well correlated to the ones from the various geophysical surveys. In addition they correspond to the sites of the higher peaks for the pH, EC, heavy metal content for the water sample data.

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표준시료를 이용한 토양중 중금속 분석방법 비교

  • 윤정기;김태승;김동호;전성환;정일록;김혁
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2005년도 총회 및 춘계학술발표회
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    • pp.242-246
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    • 2005
  • The heavy metal analysis (Cd, Pb, Cu, Cr, Zn, Ni) with various extraction methods was performed using the certified sample and real soil sample. In case of the certified samples, $10.5{\sim}118%$ of recovery was showed with various ranges depend on the metal kinds and extraction methods. Also, the alkali-digestion method was showed the proper results by applying in hexavalent chromium. In case of real sample, compared to amounts of heavy metals extracted using 0.1N-HCl, those extracted using acid digestion are higher by $3{\sim}24$ times in Cu, $1.1{\sim}1.5$ times in Cd, $2{\sim}23$ times in Pb, $3{\sim}104$ times in Zn, $12{\sim}101$ times in Ni, $30{\sim}202$ times in Cr. There is no considerable difference between four acid digestion methods.

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사향소합원(麝香蘇合元)이 정서반응성(情緖反應性)과 Alzheimer's disease 모델 백서(白鼠)의 학습(學習)에 미치는 영향(影響) (The Effects of Sahyangsohapwon on the Affective Reactivity and the Acquisition of Two-way avoidance in AD Model Rats)

  • 홍대성;김종우;황의완
    • 동의신경정신과학회지
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    • 제10권1호
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    • pp.17-38
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    • 1999
  • The effects of Sahyangsohapwon on the affective reactivity of rats were studied with open-field behavior. Sample group was treated with the medicine for 8 weeks, whereas control group was treated with the vehicle. The effects of Sahyangsohapwon on the enhancement of learning and memory of AD model rats were studied with two-way avoidance task. Sample group electrically lesioned on nbM(nucleus basalis of Meynert) was treated with the medicine for 8 weeks, whereas control group with nbM lesion and sham group with the sham operation were treated with the vehicle. 1. In the open-field behavior task, the start latency from start box was measured $27.08{\pm}7.51sec$ in control group, $23.15{\pm}5.98sec$ in sample group. Rats in sample group showed a tendency of shortened latency going out to a strange place compared with those in control group, but with no statistical significance(p>0.05). 2. In the open-field behavior task, the number of locomotion crossing the grid lines was measured $84.54{\pm}3.55$ in control group, $116.93{\pm}6.41$ in sample group. There was an increased locomotion in sample group compared with control group with statistical significance(p<0.01). This can be interpreted as rats in sample group showed lowerd anxiety under a strange environment. 3. In the open-field behavior task, the rearing number was measured $7.46{\pm}0.57$ in control group, $10.13{\pm}0.95$ in sample group. There was an increased rearing in sample group compared with control group with statistical significance(p<0.05). This can also be interpreted as rats in sample group showed lowerd anxiety under a strange environment. 4. In the open-field behavior task, the number of crossing behavior was measured $5.54{\pm}1.50$ in control group, $9.20{\pm}1.67$ in sample group. There was a increasing tendency of crossing behavior in sample group compared with control group, but with no statistical significance(p<0.05). 5. In the open-field behavior task, the total activity was measured $97.54{\pm}4.70$ in control group, $136.27{\pm}792$ in sample group. There was an increased total activity in sample group compared with control group with statistical significance(p<0.01). This can also be interpreted as rats in sample group showed lowerd anxiety under a strange environment. 6. In the analysis of effects on the learning and memory in AD model rats with two-way avoidance task, the response latency was measured $6717{\pm}134msec$ in the 1st session, $5416{\pm}160msec$ in the 2nd session, $5252{\pm}148msec$ in the 3rd session in control group. It was measured $6724{\pm}155msec$ in the 1st session, $4642{\pm}139msec$ in the 2nd session, $4914{\pm}148msec$ in the 3rd session in sample group and $4357{\pm}144msec$ in the 1st session, $3125{\pm}115msec$ in the 2nd session, $3091{\pm}98msec$ in the 3rd session in sham group. There were differences between sham group and nbM lesioned groups with statistical significance in post hoc analysis(p<0.000). And in the 2nd session, there was a reduction of latency in sample group compared with control group with statistical significance (p<0.000). This showed that sample group had better learning capacity than control group. 7. In the analysis of effects on the learning and memory in AD model rats with two-way avoidance task, the number of avoidance response was measured $5.85{\pm}1.41$ in the 1st session, $14.23{\pm}2.89$ in the 2nd session, $15.69{\pm}2.56$ in the 3rd session in control group. It was measured $7.92{\pm}1.94$ in the 1st session, $16.83{\pm}2.29$ in the 2nd session, $15.42{\pm}2.81$ in the 3rd session in sample group and $14.38{\pm}1.62$ in the 1st session, $22.88{\pm}0.89$ in the 2nd session, $23.88{\pm}1.64$ in the 3rd session in sham group. There were differences between sham group and nbM lesioned groups with statistical significance in post hoc analysis(p<0.001). But between control and sample group, there was no significant difference. With the experimental results above, Sahyangsohapwon can be supposed to have the enhancing effects on the affect reactivity and learning with memory of AD model rats induced by electrolyte injury of nbM.

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열처리조건 변화에 따른 in-situ $MgB_2$ 초전도 특성 비교 (Comparison of in-situ $MgB_2$ Superconducting Properties Under Different Annealing Environment)

  • 정국채;;장세훈;김정호
    • Progress in Superconductivity
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    • 제14권2호
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    • pp.116-121
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    • 2012
  • Effect of mixed gas and additional Mg powder in an annealing process of the $MgB_2$ is investigated. Four different type of samples were prepared, each in different annealing environment of Ar, $Ar+4%H_2$, Ar with Mg powder and $Ar+4%H_2$ with Mg powder. Different annealing environment did not affect the electron-phonon interaction which is reflected from the same superconducting transition of 36.6 K for all samples. The reducing effect of hydrogen is clearly depicted from the presence of excess Mg in sample synthesized in $Ar+4%H_2$ gas implying the reduced rate of reaction between Mg and B. This has manifested itself in terms of slightly increased high-field critical current density of the sample. In contrast, the sample synthesized in $Ar+4%H_2$ with Mg powder, has shown overall enhancement in the superconducting properties as presented by higher diamagnetic saturation and critical current density.