• 제목/요약/키워드: sample compositions

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Effects of the Gamma Irradiation on Composition of Free Amino Acid, Fatty Acid and Organic Acid of Soybean-Based Fermentation Food (감마선 조사가 장류제품의 유리 아미노산, 지방산 및 유기산 조성에 미치는 영향)

  • 김동호;김정옥;차보숙;이자영;변명우
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.30 no.5
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    • pp.777-781
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    • 2001
  • The effects of gamma-irradiation on the nutritional components of some Korean soybean-based fermentation foods were studied. Doenjang (soybean paste), kochujang (red pepper paste) and chungkukjang were prepared, irradiated at 0, 5, 10 and 20 kGy, and their compositions of free amino acid, free fatty acid and organic acid were determined. Compositions of free amino acid and free fatty acid in gamma irradiated sample were stable compared to non-irradiated control. Content of citric acid and succinic acid increased, while that of malic acid decreased in the gamma irradiated chungkookjang, but there were no significant changes in organic acid composition in organic and kochujang.

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INVESTIGATION OF EQUINE HEMATOLOGICAL CONSTITUENTS IN CENTRAL TAIWAN. I. DISTRIBUTION OF THE BLOOD CELL PARAMETERS AND THE BIOCHEMICAL COMPOSITIONS OF SERUM

  • Ju, J.C.;Cheng, S.P.;Fan, Y.K.;Hsu, J.C.;Chiang, S.K.;Chen, E.V.;Chang, S.H.;Chiou, S.C.
    • Asian-Australasian Journal of Animal Sciences
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    • v.6 no.1
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    • pp.147-153
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    • 1993
  • A total of 109 heads of horses and ponies from eight horseback riding clubs nearby Central Taiwan were investigated to evaluate the blood parameters and the biochemical compositions of serum for the documentation of clinical pathological diagnosis and exercise physiology. Blood samples were collected from the jugular vein of resting horses. The sex difference in the blood traits were compared both in horses and in ponies. Results shows that total plasma proteins (PP) and hematocrit (PCV) were found higher in male horses than in females (p < 0.05). The sexual effect also exertes a significant influence on the leucocyte (WBC) count, but not on the erythrocyte (RBC) concentration. According to the differential counts of leucocytes, the number of monocytes and lymphocytes was higher in the male pony than that of in male horse. A close relationship Between the erythrocyte sedimention rate (ESR) and the other blood parameters were found especially in PCV, RBC concentration, and plasma protein level. The average ESR observed at 60 minutes were $21.80{\pm}21.87mm$, $39.50{\pm}18.90mm$ and $43.73{\pm}17.89mm$ in stallions, geldings, and mares, respectively. Most of the biochemical components of horse serum detected were distributed in normal ranges, although some of the items show a great variation in such a large sample size.

Quality Characteristics of Sprouted Brown Rice Dasik with Yujacheong Added (유자청을 첨가한 발아현미다식의 품질 특성)

  • Lee, Young-Sook;Kim, Ae-Jung;Rho, Jeong-Ok
    • Korean journal of food and cookery science
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    • v.24 no.4
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    • pp.494-500
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    • 2008
  • The principal objective of this study was to assess the quality characteristics of Sprouted Brown Rice Dasik(SBRD) manufactured with various addition levels of honey and Yujacheong(Yuja syrup and Yuja sarcocarp) in accordance with the traditional method for the preparation of Korean Dasik(a kind of cookie). The nutritional components, color value, physical tests, volatile compounds, and sensory evaluation of SBRD to which Yujacheong was added were conducted. The results were summarized as follows. In SBRD to which Yujacheong had been added, the moisture contents and crude fat content did not differ significantly among the sample groups, and the contents of crude protein and crude ash increased with increasing additions of Yuja syrup and Yuja sarcocarp. The pH(p<0.001) and sweetness(p<0.001) were significantly higher in sample D1 than in samples D2 and D4. The L color value was highest in D2, the a value was highest in D3, and the b value was highest in sample D2. The texture property analysis showed that the cohesiveness, springiness, gumminess, and chewiness of SBRD to which Yujacheong was added were all significantly higher compared to sample D1. According to the results of our volatile analysis, the D1 and other experimental groups evidenced different flavors and antibacterial compositions. According to the results of our sensory evaluation, the appearance of the D1 sample was superior to the other samples. However, flavor, taste, texture, and overall preference were higher in the samples to which Yuja syrup and Yuja sarcocarp were added. These results indicate that SBRD to which Yujacheong was added, and particularly those to which Yuja syrup was added, is superior to Dasik prepared with honey in terms of flavor and taste, and this method will improve the flavor and preparation time, due to its lower pH.

Effect of Dry Grinding of Laterite on the Extraction of Nickel and Cobalt (라테라이트광의 건식분쇄가 니켈 및 코발트의 침출에 미치는 영향)

  • Kim, Wan-Tae;Choi, Do-Young;Kim, Sang-Bae
    • Journal of the Mineralogical Society of Korea
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    • v.23 no.3
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    • pp.227-234
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    • 2010
  • We investigated the effect of dry grinding of laterite on the extraction of nickel and cobalt. The major chemical compositions of the sample for this work were $SiO_2$, $Fe_2O_3$ and MgO. The sample contained 0.81% Ni and 0.02% Co. The major minerals of the sample were lizardite and quartz with minor amounts of forsterite and enstatite. The mean particle size, specific surface area and density of the ground sample decreased with increasing grinding time, while the amorphization of lizardite increased as identified by XRD analysis. The grinding enabled the extraction ratio of Ni and Co to increase by the breakdown of Mg-OH bonding in the lizardite structure. However, physical properties of quartz were not changed by grinding. The extraction ratio of Ni and Co increased with increasing grinding time. Approximately 80% of Ni and Co were extracted regardless of the kind of acid solutions when the sample was ground for 60 minutes.

Changes of Physicochemical and Sensory Characteristics in the Codonopsis lanceolata Saengsik, Uncooked Food by Different Drying Methods (건조방법 달리하여 제조한 더덕 생식의 이화학적 및 관능적 특성 변화)

  • Jin, Tie-Yan;Quan, Wu-Rong;Wang, Myeong-Hyeon
    • Korean Journal of Food Science and Technology
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    • v.40 no.6
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    • pp.721-725
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    • 2008
  • Changes in the physicochemical and sensory characteristics of the uncooked food, Codonopsis lanceolata saengsik, were investigated to determine an efficient drying method, one of the most important manufacturing processes in the preparation of C. lanceolata saengsik. No changes in the proximate compositions of all samples were observed during hot-air drying at 50 and $60^{\circ}C$ and freeze-drying. The L value in the freeze-dried sample was higher than that in the hot-air dried samples, whereas the b value in the freeze-dried sample was reduced. Dietary fiber content in the hotair dried samples were higher than that in the freeze-dried sample, whereas the total phenolic compounds and crude saponin contents were lower than those in the freeze-dried sample. The highest overall acceptability values in the sensory test for color, flavor, taste, and overall acceptability were 5.63, 5.45, 5.75, and 5.85, respectively. In conclusion, the freezedrying method was the most favorable of the tested method for the manufacture of C. lanceolata saengsik.

Study on Characterization of Contact Lens with Hydrophobic Monomers (소수성 모노머들을 포함한 콘택트렌즈의 특성에 관한 연구)

  • Ye, Ki-Hun;Kim, Tae-Hun;Sung, A-Young
    • Journal of Korean Ophthalmic Optics Society
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    • v.13 no.3
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    • pp.29-34
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    • 2008
  • Purpose: In this study, we compared the physical properties of the compositions that were mixed with basic materials of HEMA (2-Hydroxyethyl methacrylate)/Silicone and BMA (Butyl methacrylate), MMA (Methyl methacrylate) by making the silicone contact lens. Method: Each sample of contact lenses was fabricated by cast mould method. We analyzed results by using average values of physical property of each sample. Results: In the composition of HEMA/Silicone/BMA, water contents of samples showed the value from 24.69% to 29.26%. Ultimate strength of samples showed the value from 0.109 kgf to 0.263 kgf. In the composition of HEMA/Silicone/MMA, swelling ratio of samples showed the value from 13.56% to 14.83%. Water contents of samples showed the value from 25.61% to 29.33%. Ultimate strength of samples showed the value from 0.107 kgf to 0.286 kgf. Conclusions: The compositions of percents of silicone were ranged from 0.20% to 11.50% and the composition percent of BMA and MMA was 5.15% in total. Swelling ratio and water contents increased with decreasing of BMA (Butyl methacrylate) and MMA (Methyl methacrylate) percent. In the composition of HEMA/Silicone/MMA, the values of ultimate strength increased with increasing of silicone percent to 4-MMA sample. In the composition of HEMA/Silicone/BMA, the values of ultimate strength decreased with increasing of silicone percent.

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Superconductivty and Magnetic Properties of Tb-substituted $RuSr_2(Eu_{1.34}Ce_{0.66})Cu_2O_z$ (Tb이 치환된 $RuSr_2(Eu_{1.34}Ce_{0.66})Cu_2O_z$ 계의 초전도 및 자기적 특성)

  • Lee, H.K.;Lee, M.S.
    • Progress in Superconductivity
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    • v.14 no.2
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    • pp.110-115
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    • 2012
  • Samples with nominal compositions of $RuSr_2(Eu_{1.34-x}Tb_xCe_{0.66})Cu_2O_z$ (x = 0, 0.67) were prepared and their superconductivity and magnetic properties were compared to shed light on the effect of Tb substitution for Eu. X-ray diffraction measurements indicate that the Tb substitution resulted in a decrease in both a and c lattice parameters in consistent with ionic size difference between Eu and Tb. Contrary to the Tb-free sample, no superconducting transition behavior is observed in the Tb-sustituted sample. It is also found that the Tb substitution for Eu significantly increases the weak-ferromagnetic component of the field-cooled magnetic susceptibility as well as an increase in the magnetic ordering temperature. These results suggest that the magnetic state of the Ru sublattice is significantly affected by the Tb substitution for Eu.

Characterization of Thermal Degradation of Polytrimethylene Terephthalate by MALDI-TOF Mass Spectrometry

  • Jang, Sung-Woo;Yang, Eun-Kyung;Jin, Sung-Il;Cho, Young-Dal;Choe, Eun-Kyung;Park, Chan-Ryang
    • Bulletin of the Korean Chemical Society
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    • v.33 no.3
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    • pp.833-838
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    • 2012
  • The thermal degradation products of polytrimethylene terephthalate (PTT) obtained by heating the sample in the temperature range of $250-360^{\circ}C$ under non-oxidative conditions was characterized using MALDI-TOF (matrix assisted laser desorption/ionization) mass spectrometry. The structures of the degradation products were determined and the relative compositions were estimated. The MALDI-TOF mass spectra of the thermally degraded PTT sample showed three main series of oligomer products with different end groups, which were carboxyl/carboxyl, carboxyl/allyl, and allyl/allyl. In contrast to the thermal degradation of polyethylene terephthalate (PET), the oligomers containing terephthalic anhydrides were not detected, whereas the formation of oligomers containing the unsaturated allyl ester group was confirmed by mass assignment. From these results, it was concluded that the thermal degradation of PTT proceeds exclusively through the ${\beta}$-CH hydrogen transfer mechanism, which is in accordance with the proposed reaction mechanism for the thermal degradation of polybutylene terephthalate (PBT).

Analysis of Gases in Nuclear Fuel Rod by Quadrupole Mass Spectrometry (Quadrupole Mass Spectrometry를 이용한 핵연료봉내 기체분석)

  • Kim, Seung-Soo;Kang, Moon-Ja;Park, Soon-Dal;Park, Yong-Joon;Joe, Kih-Soo
    • Analytical Science and Technology
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    • v.12 no.2
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    • pp.94-98
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    • 1999
  • An analysis method of components and isotopic compositions of low pressure gases from nuclear fuel rod using quadrupole mass spectrometer was studied. The calibration curves of each gas in pure and mixtures of He, $N_2$, $O_2$, Ar, Kr and Xe were obtained as a function of pressure and concentration, respectively. Effect of molecular leak, located between sample chamber and analyser chamber, on the sensitivites was also studied. The results suggested that samples could be analysed accurately at the same analytical condition as that of synthetic gas mixture. The difference of sensitivities among isotopes of Kr and Xe was not observed in the range of measured pressure.

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Flocculation Behavior and properties of Montmorillonites Mixed with Organic Polymer Solutions (유기폴리머 용액에 혼합한 몬모릴로나이트의 응집 거동 및 특징)

  • 황진영
    • Economic and Environmental Geology
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    • v.32 no.3
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    • pp.307-315
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    • 1999
  • Four organic polymers were mixed with mothmorillonite. Two cationic polymers a hi로 molecular weight polyacrylamide (494C) and a low molecular weight polymer (587C).Two anionic polymers include a high molecular weight polymer (aerotil). Each clay supension series were allowed to stand for 24 hours and were centrifuged, and the clay plugs were washed and dried. The dried samples investigated by XRD, IR and CEC measurement. The suspended clay containing anionic polymers was not flocculated at any concentratuons of polymer. But the suspendions containing two cationic polymers were rapidly flocculated at almost all concentrations. the d(001) spacings of Na-montmorillonite after being with cationic polymer 587C show about 15$\AA$ suggesting the polymers may have entered the interlayer spaces. The polymer 494C-treated sample produced double peaks of about 12 and 15$\AA$ in XRD. It indicates that the high molecular weight polymer. And cationic polymer 494C may be adsorbed mainy on the outside surface of clay, and some polymers may peretrate into olny interlayers in the margin of montmorillonite particles because of its high molecular weught. CEC of polumer 587-treated sample was reduecd mmarkedly suggesting polymer blocks CEC sites. The d(001) spacings of Ca-montmorillonite after being treated with cationic polymers show about 15$\AA$ suggesting that the interlayer spaces have not been expanded. In the experiment using a dilute Ca-bearing solution, the suspended caly containinf anionic polymers was flocculated. The results indicate that the flocculation behavior of montmorillonite-polymer supension depends on not only polymer properties such as concentration, electric charge and molecular weight but also compositions of solvent.

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