• 비파괴검사학회지
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• 제26권6호
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• pp.390-402
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• 2006

The elastic properties and thickness of mullite environmental barrier coatings grown through chemical vapor deposition (CVD) on silicon carbide substrates were measured using frequency domain photoacoustic microscopy. In this technique, extremely narrow bandwidth surface acoustic waves are generated with an amplitude modulated laser source. A photorefractive crystal based interferometer is used to detect the resulting surface displacement. The complex displacement field is mapped as a function of source-to-receiver distance in order to extract the wavelength of the surface acoustic wave at a given excitation frequency, and the phase velocity is determined. The coatings tested exhibited spatial variations in thickness and mechanical properties. The measured surface wave dispersion curves were used to extract an effective value for the elastic modulus and the coating thickness. Nanoindentation was used to validate the measurements of the effective elastic modulus. The average elastic modulus measured through the coating thickness using nanoindentation is compared to the effective modulus found using the photoacoustic system. Optical microscopy is used to validate the thickness measurements. The results indicate that the photoacoustic microscopy technique can be used to estimate the effective elastic properties in coatings exhibiting spatial inhomogeneities, potentially providing valuable feedback for the optimization of the CVD growth process.

• 한국해양공학회지
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• 제25권6호
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• pp.72-79
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• 2011

In this paper, the fatigue characteristics of shot peened A7075-T651 alloy were compared with those of the specimens without the shot peening. The multi-spindle and single-spindle rotating bending fatigue testing machines were employed for the evaluation. Shot peening (SP) with various pressure (5 psi, 10 psi, 15 psi, 25 psi and 35 psi) were used in this test. In order to investigate the effect of the applied pressure during the SP, we carried out the surface roughness test, compressive residual stress test, hardness test, tensile test, VHCF (Very high cycle fatigue) test and SEM observation. SP induced the formation of remarkable compressive residual stress from the surface to certain depth of sample by means of the plastic deformation. The surface hardness and the fatigue characteristics of the specimens were also modified by the SP. According to the S-N curves, fatigue lives of shot peended sample with 25 psi measures 50 times higher than that of the untreated sample. The fatigue lives of shot peened sample with 15 psi and 35 psi measure approximately 10 times higher than that of the untreated ones.

• 한국식품위생안전성학회지
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• 제18권2호
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• pp.43-50
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• 2003

A liquid chromatographic method, using matrix solid-phase dispersion (MSPD) is developed for the extraction of residual furazolidone in chicken eggs. Blank or fortified egg samples (0.5 g) were blended with Octadecylsilyl (Bulk $C_{18}$, 40${\mu}{\textrm}{m}$, 18%. load, endcapped. 2 g) derivatized silica. After homogenization, $C_{18}$/egg and Na$_2$S $O_4$matrix were transferred to a column made of 10 ml glass syringe and filter paper and compressed 4.0∼4.5 ml volume. The column was washed with 8 ml of hexane and dried under $N_2$ gas. Furazolidone was eluted with acetonitrile (8 ml) under gravity. The eluate containing furazolidone was free from interfering compounds when analyzed by HPLC with UV detection (365 nm, photodiode array). Calibration curves were linear (r = 0.99985) and inter- (1.47%) and intra-assay (5.29%) variabilities for the concentration range examined (7.8∼497 ng/g of eggs, 20 ${mu}ell$ injection volume) were indicative of an acceptable methodology for the analysis of furazolidone. Average recovery of furazolidone added to egg was 96.2%. The limit of detection for the proposed method was 1 ng/g for furazolidone. The method using MSPD is proposed as an alternative assay to the classical method which involves the use of large volumes of a harmful solvent and requires a long tedious separation and clean-up processes prior to its determination.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2008년도 Techno-Fair 및 추계학술대회 논문집 전기물성,응용부문
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• pp.165-166
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• 2008

We investigate characteristics of J-aggregation as take advantage of LB technic. In order to confirm the applications possible for the molecular electronic device, the morphological properties of merocyanine dye were investigated by AFM. ${\pi}-A$ curves investigated the surface pressure of the LB film from a liquid to a solid state ranged between 90 and 100 mN/m. We observed aggregation and it's characteristics by using visible reflection spectroscopy. We have observed morphology of merocyanine dye on gold surface by STM. focuses on results obtained in mercocyanide dye of J-aggregation. When LB films of merocyanine dye are mixed with arachidic acid, J-aggregate formation is exhibited. J-aggregate formation has been serving as typical systems in revealing the physical and structural aspects of nano-sized molecular aggregates constructed as muiltilayers.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2004년도 추계학술대회 논문집 Vol.17
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• pp.345-348
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• 2004

For practical applications, the evaluation of reliability or endurance of HTS conductors is necessary. The mechanical properties and the critical current, $I_c$, of multifilamentary Bi-2223 superconducting tapes, externally reinforced with stainless steel foils, subjected to high cycle fatigue loading in the longitudinal direction were investigated at 77K. The S-N curves were obtained and its transport property was evaluated with the increase of repeated cycles at different stress amplitudes. The effect of the stress ratio, R, on the $I_c$ degradation behavior under fatigue loading was also examined considering the practical application situation of HTS tapes. Microstructure observation was conducted in order to understand the L degradation mechanism in fatigued Bi-2223 tapes.

• International Journal of Concrete Structures and Materials
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• 제9권1호
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• pp.55-60
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• 2015

In this study, influence of different stone powders (SP), including limestone powders (LP), quartzite powders (QP), and granitic powders (GP), on the hydration behaviors of portland cement, for example, setting time, hydration heat, and hydration products, were discussed. The initial and the final setting time both shorten when the content of LP is 5 %, however, they are slightly delayed by the other two SPs. The LP has no obvious influence on the arrival time of the first peak in the exothermal curves, and it makes the peak value decrease; the other two SPs postpone the appearance of the first peak, and they also make the peak value decrease. For the second peak, LP shifts the peak position to the left, QP has no effect on this peak position, and GP makes the appearance of this peak delayed by 143 min. Similarly, three kinds of SPs have different influence on the hydration products of portland cement. The LP precipitates the formation of hydrated calcium carbo aluminate, the QP the formation of hydrated garnet, and the GP makes the amount of Tobermorite increase.

• 한국전산유체공학회지
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• 제20권4호
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• pp.1-6
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• 2015

Centrifugal pumps consume considerable amount of energy in various industrial applications. Therefore, improvement of the efficiency of these machines has become a major challenge. Cavitation is a phenomenon which decreases the pump efficiency and even causes structural demage. Hence, the goal of this paper is to investigate the cavitation problem in the single-stage and double-stage centrifugal pumps. The Volume of Fraction (VOF) method has been used for the numerical simulations together with Rayliegh-Plesset model for the gas-liquid two-phase flow inside the pump. In order to capture the turbulent phenomena, the standard k-${\varepsilon}$ turbulence model has been adopted, and the simulations have been done as unsteady cases. In addition, the motion of the rotating parts has been simulated using Multi Reference Frame(MRF) method. The results are presented and compared in terms of hydraulic head and NPSH for both the single-stage and double-stage pumps. The H-Q curves show the effects of cavitation on decreasing the pumps performances.

• Progress in Superconductivity
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• 제1권2호
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• pp.110-114
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• 2000

We have investigated the Josephson vortex dynamics in $Bi_2Sr_2CaCu_2O{8+\delta}$ intrinsic Josephson junctions subjected to a magnetic field parallel to $CuO_2$ planes. We investigated mesas with $40\times40{\mu}m^2$ in size and containing 6 and 20. intrinsic junctions. The zero field I-V characteristics exhibited a typical hysteretic, multi-branched nature of the intrinsic Josephson effect. At high magnetic fields (H>1.5 T), I-V characteristics showed flux flow steps. The Swihart velocity obtained from this observation was about $4.2\times10^5$ m/s, which was the lowest mode electromagnetic wave velocity of N coupled stack. The experimental I-V curves fitted well into the simple model of Cherenkov radiation including Ohmic and non-linear dissipation terms. This suggests that the dissipation mechanism of Josephson vortex be due to both Cherenkov radiation and quasiparticle tunneling current.

• International Journal of Fluid Machinery and Systems
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• 제8권4호
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• pp.254-263
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• 2015

The failure of hydraulic turbine runners is a rare event. So in order to assess the reliability of these components one cannot rely solely on the number of observed failures in a given population. However, as there is a limited number of degradation mechanisms involved, it is possible to use physically-based reliability models. Such models are often more complicated but are able to account for physical parameters in the degradation process. They can therefore help provide solutions to improve reliability. With such models, the effect of materials properties on runner reliability can be highlighted. This paper presents a brief review of the Kitagawa-Takahashi diagram which links the damage tolerance approach, based on fracture mechanics, to the stress or strain-life approaches. Using simplified response spectra based on runner stress measurements, we will show how fatigue reliability is sensitive to materials fatigue properties, namely fatigue crack propagation behaviour and fatigue limit obtained on S-N curves. Furthermore, we will review the influence of the main microstructural features observed in 13%Cr-4%Ni stainless steels commonly used for runner manufacturing. The goal is ultimately to identify the most influential microstructural features and to quantify their effect on fatigue reliability of runners.

• Steel and Composite Structures
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• 제25권1호
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• pp.57-65
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• 2017

The fatigue fracture of studs is the main reason for failure of composite beams based on massive engineering practices. Hence, studying the laws of cracks initiation and propagation are of great directive significance. eXtended Finite Element Method (XFEM) is an effective method in solving moving discontinuous problems in recent years. This paper extends our recent work on the fatigue damage analysis of stud shear connectors in the steel and crumble rubber concrete (RRFC) composite beams based on XFEM. The process of crack initiation to failure of the stud is simulated and an effective calculation criteria for the fatigue life of the composite beams is put forward. After the reliability of the numerical analysis is verified based on tests results, the extensive parametric study is conducted concerning effects of different rubber contents, shear connection degrees and the stress amplitudes. Results show that with the increasing rubber contents and shear connection degrees, the fatigue lives of composite beams increase obviously. Furthermore, the relationship between the fatigue life of the stud at the edge of the shear span and the whole composite beams is studied. Finally, the S-N curves of the single stud and the whole composite beams are put forward based on XFEM.