• Korean Journal of Food Science and Technology
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• v.37 no.3
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• pp.339-344
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• 2005

Volatile compounds, isolated from Elsholtzia splendens using simultaneous steam distillation extraction (SDE) and headspace solid phase microextraction (HS-SPME), were analyzed by gas chromatography/mass spectrometry(GC-MS). Twenty-nine compounds, comprising 3 aldehydes, 7 alcohols, 11 hydrocarbons, 5 ketones, and 3 miscellaneous ones, were tentatively identified from volatile compounds of Elsholtzia splendens flowers. From leaves, 30 compounds, comprising 3 aldehydes, 6 alcohols, 11 hydrocarbons, 6 ketones, and 11 miscellaneous ones, were tentatively identified. Volatile compounds extracted by HS-SPME in E. splendens flowers were 3 alcohols, 18 hydrocarbons, 3 ketones, and 2 miscellaneous ones. In leaves, 31 compounds, comprising 7 alcohols, 15 hydrocarbons, 7 ketones, and 2 miscellaneous ones, were tentatively identified. Major volatile compounds identified by SDE and HS-SPME were naginataketone and elsholtziaketone, which were identified as aroma-active compounds, representing characteristic aroma of E. splendens.

• Analytical Science and Technology
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• v.21 no.2
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• pp.93-101
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• 2008

The application of solid phase microextraction (SPME) is generally conducted by directly immersing the fiber into the liquid sample or by exposing the fiber in the head space (HS). The extraction temperature, the time of incubation, and application of stirring are often designated to be the most important parameters for achieving the best extraction efficiencies of HS-SPME analysis. In this study, relative importance of these three analytical parameters involved in the HS-SPME method is evaluated using a polydimethylsiloxane/carboxen (PDMS/CAR) fiber. To optimize its operation conditions the competing relationships between different parameters were investigated by comparing the extraction efficiency based on the combination of three parameters and two contracting conditions: (1) heating the sample at 30 vs. 50 C, (2) exposing samples at two durations of 10 vs. 30 min, and (3) application of stirring vs. no stirring. According to our analysis among 8 combination types of HS-SPME method, an extraction condition termed as S50-30 condition ((1) 1200 rpm stirring, (2) $50^{\circ}C$ exposure temp, and (3) 30 min exposure duration) showed maximum recovery rate of 45.5~68.5% relative to an arbitrary reference of direct GC injection. According to this study, the employment of stirring is the most crucial factor to improve extraction efficiency in the application of HS-SPME.

• Proceedings of the KSME Conference
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• 2002.08a
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• pp.479-482
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• 2002

Riblets with longitudinal grooves along the streamwise direction have been used as an effective flow control technique for drag reduction. A flexible micro-riblet with v-grooves of peak-to-peak spacing of $300{\mu}m$ was made using a MEMS fabrication process of PDMS replica. The flexible micro-riblet was attached on the whole surface of a NACA0012 airfoil with which grooves are aligned with the streamwise direction. The riblet surface reduces drag coefficient about $7.9{\%}\;at\;U_o=3.3m/s$, however, it increases drag about $8{\%}\;at\;U_o=7.0m/s$, compared with the smooth airfoil without riblets. The near wake has been investigated experimentally far the cases of drag reduction ($U_o\;=\;3.3 m/s$) and drag increase ($U_o\;=\;7 m/s$). Five hundred instantaneous velocity fields were measured for each experimental condition using the cross-correlation PIV velocity field measurement technique. The instantaneous velocity fields were ensemble averaged to get spatial distribution of turbulent statistics such as turbulent kinetic energy. The experimental results were compared with those of a smooth airfoil under the same flow condition. The micro-riblet surface influences the near wake flow structure largely, especially in the region near the body surface

• Transactions of the Korean Society of Mechanical Engineers A
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• v.33 no.5
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• pp.489-495
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• 2009

A novel technique to measuret of viscoelastic properties of polymers is proposed to investigate complex Poisson's ratio as a function of frequency. The forced vibration responses for the samples under the normal and the shear deformation are to be measured with varying load masses. The measured data were used to obtain the viscoelastic properties of the material based on an accurate 2D numerical deformation model of the sample. The 2D model enabled us to exclude data correction by the empirical form factor used in 1D model. Comprehensive measurements of viscoelastic properties of two slightly varied silicone RTV rubber ($Silastic^{(R)}$ S2) compositions were performed. Standard composition (90% PDMS polymer + 10% catalyst) and modified composition (92.5% polymer + 7.5% catalyst) were tested in temperature range from $30^{\circ}C$ to $70^{\circ}C$. Shear modulus, modulus of elasticity, loss factor, and both the real and the imaginary parts of the Poisson's ratio were determined for frequencies from 50 to 400Hz in the linear deformation regime (at relative deformations $10^{-4}{\sim}10^{-3}$).

• Proceedings of the KIEE Conference
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• 2004.07c
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• pp.2093-2095
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• 2004

본 논문은 압전소자를 구동장치로 사용한 마이크로 펌프의 제작과 실험에 관한 논문이다. 마이크로 펌프의 상부기판은 polydimethyl siloxane(PDMS)을 소재로 미세유로에 상시 닫힌 밸브가 일체화된 구조로 제작되었고, 하부기판은 polymethyl methacrylate(PMMA)를 소재로 3개의 압전 디스크가 구동기로 부착되었다. 최종적으로 상, 하부 기판은 액상 PUMS로 접합하여 제작했다. 구동기의 입력신호는 6상으로 구형파를 인가하여 연동구동하며 주파수와 전압을 가변하면서 유량을 측정하였다. 구동 주파수가 0.167 Hz이고 전압이 20 V일 때, 마이크로펌프의 1회 토출량은 104 nl이고, 유량은 1.04${\mu}{\el}$/min이다.

• Bulletin of the Korean Chemical Society
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• v.25 no.4
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• pp.560-562
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• 2004

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.06a
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• pp.1168-1170
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• 2005

Nanoimprint Lithography(NIL) has increasingly been recognized as a key manufacturing technology for nanosized feature. One of the most important task for nanoimprint lithography is to provide the imprinting stamp with low price. The Stamp fabricated with Si based material by e-beam lithography, RIE is extremely expensive and its throughput is very limited and PDMS replica is too soft to hold high imprinting pressure.(>5atm) In this study, we present the imprinting stamp which can be easily replicated from original mold and is based on PVC film. Replication of original Si mold to PVC film was done by Hot embossing technique, ($120^{\circ}C$ of Temperature, 20 atm applied) As small as 100nm patterns were successfully transferred into PVC film. The size of stamp was up to 100mm in diameter.

• Journal of the Korean Society of Visualization
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• v.8 no.3
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• pp.22-28
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• 2010

In the present study, we performed the velocity field measurement in a microchannel using a focal length variable micro liquid lens. The liquid lens is used as a beam expander in a micro-PIV system to acquire the scatter image of the seeded particle. A thin film-type micro liquid lens was made of PDMS material and it was attached on top of the 700-micron-wide working fluid supply channel trench. As a result, the focal length and contact angle of the liquid lens changed with variations in applied pressure.

• Proceedings of the KIEE Conference
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• 2011.07a
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• pp.59-60
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• 2011

본 논문에서는 기존의 PCR 장비가 가지고 있는 낮은 경제성, 장비의 대형화, 긴 분석 시간 등과 같은 단점을 해결하기 위하여 ATMEGA128 마이크로 칩을 사용 continuous-flow PCR 칩의 온도를 제어 하였다. Polydimethylsiloxane (PDMS)와 산화 인듐-주석(Indium tin-oxide, ITO) 유리 기판을 사용하여 continuous-flow PCR 칩을 제작하였고 PDMS를 주조 하여 마이크로 채널을 형성하였다. 또한 유리 기판위에 ITO 전극을 패터닝하여 마이크로 히터를 제작하였다. 이 결과 continuous-flow PCR 칩에서 빠르고 정확한 온도 제어를 통한 DNA 중합 효소 연쇄반응 결과를 얻을 수 있었다.

• Journal of the Korean Graphic Arts Communication Society
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• v.21 no.1
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• pp.45-58
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• 2003

The entanglement effects were described by means of holes through which the network chain must pass. Inhomogeneous entanglement effects were related to the hole distributions on the surface and in the center of spheres in the network chains. It was assumed that holes were subjected to the affiance deformation and the network chains were gaussian distribution. The results of this model calculation was compared with the compression- extension experimental data of PDMS (polydimethyl siloxane) rubber, and then hole's relative position was known to be in the center of two adjacent holes.