• Title/Summary/Keyword: rock sample

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Silver Coating on the Porous Pellets from Porphyry Rock and Application to an Antibacterial Media (반암(맥반석)으로 제조한 다공성 펠렛의 Ag 담지 및 항균 메디아로서의 적용)

  • Han, Yo-Sep;Kim, Hyun-Jung;Shin, Young-Seop;Park, Jai-Koo;Ko, Jae-Churl
    • Journal of the Korean Ceramic Society
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    • v.46 no.1
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    • pp.16-23
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    • 2009
  • The porous pellets were prepared from porphyry by slurry foaming method. The effect of sintering temperatures on pore structure of porous porphyry pellets with different extension ratio ($E_R$) was investigated by specific surface area, water absorption and porosity, which changed with sintering temperatures. When the sintering temperatures increased from $975^{\circ}C$ to $1075^{\circ}C$, specific surface area and water absorption of the all samples decreased. In case of the sample with an equal sintering temperature, $E_R=3.0$ pellets had little influence on pore structure compared to the $E_R=2.0$ pellets. As a results, it was shown by SEM that facilitated formation of micro pores at $E_R=2.0$ pellets shrunk increasingly after sintering process. At $E_R=3.0$ and sintering temperature at $1025^{\circ}C$, optimum conditions of the porous porphyry porous pellets was found. Also, Escherichia coli removal efficiency of the silver-containing porphoyry porous pellets was measured for the feasibility as a antibacterial media. The antibacterial activity of prepared silver-containing sample was maintained above 90% for 40 days.

Metamorphism of the Meta-Sedimentary Rocks in the Osu-Jinan Area, Cheonrapuk-Do, Korea (전라북도 오수-진안 지역에 분포하는 변성퇴적암류에 대한 변성작용)

  • Ahn, Kun Sang;Kim, Yong Jun;Shin, In Hyun
    • Economic and Environmental Geology
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    • v.30 no.2
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    • pp.163-174
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    • 1997
  • Precambrian metapelites and metapsammites of the Jinan-Osu area (so-called Seologri and Yongamsan Formation) consist of black slate, phyllite, mica schist, quartzite and rarely calc schist. They are intruded by Sunkagsan granite gneiss, Foliated granodiorite, Amphibolite, Sunchang foliated granite and Namwon granite. Mylonite texture, crenulation cleavage and minor shear zone are common. The meta-sedimentary rocks include various rock-fragments xenoliths in size (up to 3 cm) and rock-type. They have various porphyroblastic spots in size (up to 1 cm) and their mineral composition is different. The xenoliths are schists, granite and quartzite, which are rectangular or lens form and recrystallized muscovite, chlorite and quartz. Spots are andalusite and biotite aggregates extensively replaced by chlorite. The metamorphic terrain is divided into three zones of progressive metamorphism on the basis of mineral assemblage. They are chlorite zone, chloite-biotite zone and andalusite-biotite zone ascending order, from west to east approximately. Isograd reactions are phengitic muscovite + chlorite = less phengitic muscovite + biotite + quartz + $H_2O$ and muscovite + chlorite + quartz = andalusite + biotite + $H_2O$ between the chlorite zone and chlorite-biotite zone, and between the chloritebiotite zone and andalusite-biotite zone, respectively. Sample B6 (exposed near the Obong-ri) includes staurolites and greenish biotites, that is different in mineral assemblage and chemical composition from the meta-sedimentary rocks. Sample A12 (exposed near the Shinam-ri) has greenish white spots (up to 1 cm in diameter) mainly composed of Kfeldspar, quartz and sillimanite replaced by muscovite.

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Status of Manganese Nodule Samples in the Library of Marine Samples (해양시료도서관에 입고된 심해저 망간단괴 시료 현황)

  • Lee, Hyun-Bok;Kim, Wonnyon;Ko, Young-Tak;Oh, Jae-Ryong;Chi, Sang-Bum
    • Ocean and Polar Research
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    • v.36 no.4
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    • pp.515-524
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    • 2014
  • The Korea Institute of Ocean Science and Technology has acquired detailed biological, chemicophysical, and geological data in the northeastern Pacific through a manganese nodule program since 1983. Plenty of manganese nodules were collected to estimate the amount of resources by free-fall grab and box corer. The collected manganese nodules have been archived systematically in the rock and mineral storage section of the Library of Marine Samples (LIMS) since 2012. The LIMS provides essencial information on the stored samples including sample name, nodule type, sampling location, depth, and equipment. Although a high quality database of the information system is under construction, the samples have tagged information for manganese nodules like chemical composition, morphology, weight, size, abundance, and photograph. In this study, we attempted to provide information on the well-organized and easily accessible archived manganese nodule samples for future studies and to introduce the usefulness of the LIMS.

Evaluation of Compressibility of Rock Fill Materials by Large-Scale Oedometer Tests (대형 오이도미터 시험을 통한 Rockfill 재료의 압축성 평가)

  • Kim, Bum-Joo;Shin, Dong-Hoon;Jeon, Je-Sung;Lim, Jeong-Yeul
    • Proceedings of the Korean Geotechical Society Conference
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    • 2005.03a
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    • pp.627-632
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    • 2005
  • In this study, a series of large-scale oedometer tests was performed to investigate the compressibility of rock fill materials. The testing samples were prepared to have three different grain size distributions and for each distribution, exist in two different states(dried and saturated). The test results indicated that particle breakages occurred mainly for the particles larger than 4.75mm in size and increased with increasing grain sizes. Also, it was found that, for a dry sample as it became well-graged, its compressibility decreased and accordingly, its tangent constrained modulus increased. A comparion between the samples in dry and saturated states revealed that compressibility of the materials increases with increasing water content. The values of tangent constrained modulus calculated for the tested dry samples were larger by about 10 to 20%, on average, than those for the saturated samples.

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An Analysis of Poisson's Ratio Behaviors by Uniaxial Compressive Loading-reloading Test - On the Sedimentary Rocks of Kyungsang Basin - (일축압축 하에서 반복재하에 따른 포아송비의 거동분석 - 경상분지 퇴적암을 대상으로 -)

  • Lee, Jong-Suok;Moon, Jong-Kyu;Choi, Woong-Eui
    • Tunnel and Underground Space
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    • v.23 no.1
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    • pp.66-77
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    • 2013
  • This paper deals with Poisson's ratio and volumetric strain behavior on loading-reloading terms under uniaxial condition targeting 404 individual rocks, which include sedimentary rocks as sandstone, shale, mudstone, conglomerate and tuff on Kyungsang basin. Poisson' ratio demonstrates increase, convergence and decrease behavior according to the increase in load, which results in preponderance of increase behavior. Volumetric strain demonstrates normal, positive and negative behavior according to the increase in load, which results in preponderance of normal behavior. On practice, Poisson's ratio can be indicative of high or low values with low values of design load. Consequently, a careful selection of results in in-situ sample experiment should be made and varying design conditions should be considered.

Mineralogical and Chemical Variation in Weathering Profile on Ultramafic Rocks During Vermiculitization (질석화가 진행된 풍화단면에서의 광물조성과 주원소의 변화)

  • Moon, Hi-Soo;Song, Yungoo;Sin, Sang Eun
    • Economic and Environmental Geology
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    • v.26 no.1
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    • pp.29-40
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    • 1993
  • Several vermiculite deposits occur as the alteration product from phlogopite in ultramafic rock, in the Hongseong and Cheongyang area, South Korea. Some quarries show well-defined weathering profile. Samples collected from those quarries were examined by XRD and chemistry to define a vertical variations in mineralogy and chemistry of the weathering profile developed on ultramafic rocks. The analysis by X-ray diffractometry showed that mineral compositions changed continuously as depth of profile increasing, the vermiculite-the phlogopite/vermiculite interstratified-the phlogopite. Chemical analysis of bulk samples in altered zone revealed that regardless of composition and kinds of mineral in the rock, there are significant increase of MgO, CaO and $H_2O$, and decrease of K as depth of profile decrease reflecting the characteristics in vermiculitization. Also, there was a tendency that weathering indicies of each sample horizon change gradually with increasing depth. This tendency can be explained as variations of degree of vermiculitization. The regular changes of mineralogical and chemical composition in vertical profile suggest that weathering is the most important process in vermiculitization in this area.

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Effect of rock mineralogy on mortar expansion

  • Karaman, Kadir;Bakhytzhan, Aknur
    • Geomechanics and Engineering
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    • v.20 no.3
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    • pp.233-241
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    • 2020
  • Alkali-silica reaction (ASR) is among one of the most important damaging mechanisms in concrete, depending primarily on aggregates which contain reactive minerals. However, expansion in concrete may not directly relate to the reactive minerals. This study aims to investigate the influence of ASR and the expansion of mortar bars depending on aggregate type containing various components such as quartz, clay minerals (montmorillonite and kaolinite) and micas (muscovite and biotite). In this study, the accelerated mortar bar tests (AMBT) were performed in two conditions (mortar bars in the same and sole NaOH solutions). Petrographic thin section studies, X-ray diffraction (XRD) analysis (Rietveld method), scanning electron microscopy (SEM) and chemical analyses were carried out. This study showed that quartzite bars led to increase in expansion values of mortar bars in diabase-1 and andesite when these were in the same NaOH solution. However, three samples (basalt, quartzite and claystone) were found having ASR expansion based on the AMBT when the special molds were used for each sample. SEM study revealed that samples which exhibit highest expansions according to AMBT had a generally rough surface and acicular microstructures in or around the micro-cracks. Basalt and quartzite showed more variable in major oxides than those of other samples based on the chemical analyses, SEM studies and AMBT. This study revealed that the highest expansions were observed to source not only from reactive aggregates but also from alteration products (silicification, chloritization, sericitization and argillisation), phyllosilicates (muscovite, biotite and vermiculite) and clays (montmorillonite and kaolinite).

A Study on the Estimation of Diameter Distribution and Volumetric Frequency of Joint Discs Using the Least Square Method (최소자승법을 이용한 원판형 절리의 직경분포와 체적빈도 추정에 관한 연구)

  • Song Jae-Joon
    • Tunnel and Underground Space
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    • v.15 no.2 s.55
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    • pp.137-144
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    • 2005
  • An estimation technique of the joint diameter distribution using the least square method is suggested. When utilizing the technique by Song and Lee, the diameter distribution would be obtained only from the trace length distribution defined in an infinite window after the trace length distribution is estimated from the contained trace length distribution. With the new technique, however, the diameter distribution can be directly obtained from the sample histogram of the contained trace lengths. Compared with the previous technique, it shows a more accurate result for small sizes of joint samples and provides the joint geometry parameter of volumetric frequency. Verification of this new technique was completed by using Monte Carlo simulations.

Experimental and numerical investigation of the effect of sample shapes on point load index

  • Haeri, Hadi;Sarfarazi, Vahab;Shemirani, Alireza Bagher;Hosseini, Seyed Shahin
    • Geomechanics and Engineering
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    • v.13 no.6
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    • pp.1045-1055
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    • 2017
  • Tensile strength is considered key properties for characterizing rock material in engineering project. It is determined by direct and indirect methods. Point load test is a useful testing method to estimate the tensile strengths of rocks. In this paper, the effects of rock shape on the point load index of gypsum are investigated by PFC2D simulation. For PFC simulating, initially calibration of PFC was performed with respect to the Brazilian experimental data to ensure the conformity of the simulated numerical models response. In second step, nineteen models with different shape were prepared and tested under point load test. According to the obtained results, as the size of the models increases, the point load strength index increases. It is also found that the shape of particles has no major effect on its tensile strength. Our findings show that the dominant failure pattern for numerical models is breaking the model into two pieces. Also a criterion was rendered numerically for determination of tensile strength of gypsum. The proposed criteria were cross checked with the results of experimental point load test.

Effects of interface angles on properties of rock-cemented coal gangue-fly ash backfill bi-materials

  • Yin, Da W.;Chen, Shao J.;Sun, Xi Z.;Jiang, Ning
    • Geomechanics and Engineering
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    • v.24 no.1
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    • pp.81-89
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    • 2021
  • Uniaxial compression tests were conducted on sandstone-CGFB composite samples with different interface angles, and their strength, acoustic emission (AE), and failure characteristics were investigated. Three macro-failure patterns were identified: the splitting failure accompanied by local spalling failure in CGFB (Type-I), the mixed failure with small sliding failure along with the interface and Type-I failure (Type-II), and the sliding failure along with the interface (Type-III). With an increase of interface angle β measured horizontally, the macro-failure pattern changed from Type-I to Type-II, and then to Type-III, and the uniaxial compressive strength and elastic modulus generally decreased. Due to the small sliding failure along with the interface in the composite sample with β of 45°, AE events underwent fluctuations in peak values at the later post-peak failure stage. The composite samples with β of 60° occurred Type-III failure before the completion of initial compaction stage, and the post-peak stress-time curve initially exhibited a slow decrease, followed by a steep linear drop with peaks in AE events.