• Title/Summary/Keyword: rock powder

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An experimental study on early strength of shotcrete (숏크리트의 조기강도에 대한 실험적 연구)

  • Song, Yong-Su;Ryu, Jong-Hyun;Lim, Heui-Dae
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.12 no.4
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    • pp.285-294
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    • 2010
  • As there are increasing number of tunneling works these days, shotcrete is used as primary supports in order to secure the stability of tunnels. The quality of shotcrete has a direct influence on tunnels, because it is a primary support which secures the stability of completed tunnels as well as the stability of tunnels under excavation. Especially in case that ordinary shotcrete is used under weak rock conditions or at water gushing sections, more shotcrete is needed and rebound ratio increases. As a result, it is hard to keep economic feasibility. In addition to it, in subway construction, there are cases of separated excavation and it may have a bad influence on construction period or quality. Therefore, in this study, we are going to evaluate the early strength of powder type accelerator.

A Study on Particle and Crystal Size Analysis of Lithium Lanthanum Titanate Powder Depending on Synthesis Methods (Sol-Gel & Solid-State reaction) (분말 합성법(Sol-Gel & Solid-State reaction)에 따른 Lithium Lanthanum Titanate 분말의 입자 및 결정 크기 비교 분석에 관한 연구)

  • Jeungjai Yun;Seung-Hwan Lee;So Hyun Baek;Yongbum Kwon;Yoseb Song;Bum Sung Kim;Bin Lee;Rhokyun Kwak;Da-Woon Jeong
    • Journal of Powder Materials
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    • v.30 no.4
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    • pp.324-331
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    • 2023
  • Lithium (Li) is a key resource driving the rapid growth of the electric vehicle industry globally, with demand and prices continually on the rise. To address the limited reserves of major lithium sources such as rock and brine, research is underway on seawater Li extraction using electrodialysis and Li-ion selective membranes. Lithium lanthanum titanate (LLTO), an oxide solid electrolyte for all-solid-state batteries, is a promising Li-ion selective membrane. An important factor in enhancing its performance is employing the powder synthesis process. In this study, the LLTO powder is prepared using two synthesis methods: sol-gel reaction (SGR) and solid-state reaction (SSR). Additionally, the powder size and uniformity are compared, which are indices related to membrane performance. X-ray diffraction and scanning electron microscopy are employed for determining characterization, with crystallite size analysis through the full width at half maximum parameter for the powders prepared using the two synthetic methods. The findings reveal that the powder SGR-synthesized powder exhibits smaller and more uniform characteristics (0.68 times smaller crystal size) than its SSR counterpart. This discovery lays the groundwork for optimizing the powder manufacturing process of LLTO membranes, making them more suitable for various applications, including manufacturing high-performance membranes or mass production of membranes.

Evaluation of Engineering Characteristics and Utilization of Nonmetal Mining Waste Powder as Geo-Materials (비금속 광산 폐분의 공학적 특성 및 활용 가능성 분석)

  • Cho, Jinwoo;Lee, Yongsoo
    • Journal of the Korean GEO-environmental Society
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    • v.12 no.12
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    • pp.71-78
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    • 2011
  • This paper aims to present the evaluation of engineering characteristics and reusing possibility of waste powders produced in dolomite and limestone nonmetal mining by physical and mechanical experiments on compaction, uniaxial compressive strength, permeability, chemical composition, and so on. Granite soil, 2 types of limestone waste powder, and 1 type of dolomite waste powder were used for main materials, and cement and bentonite were used for admixed materials in this experiments. The findings based on the experimental results are the severe difference of chemical composition of the dolomite & limestone waste powder and the crushed rock waste powder, and the outstanding of engineering characteristics of the dolomite waste powder with high content of MgO compared with the limestone waste powder. The engineering properties on compaction, uniaxial compressive strength, and permeability are enhanced with increase of admixed ratio of waste powder on granite soil. From the experimental results, it can be suggested that the dolomite waste powder admixed with in-situ granite soil is useful as geo-materials with considering of distribution costs.

Extraction of Pyrophyllite Mineralized Zone using Characteristics of Spectral Reflectance of Rock Samples (암석분광반사율 특성을 이용한 납석 광화대 추출)

  • Chi, Kwang-Hoon;Lee, Hong-Jin
    • Korean Journal of Remote Sensing
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    • v.23 no.6
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    • pp.493-500
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    • 2007
  • In general, it accomplished a spectral reflectance analysis to be, the measurement results appear differently by targets, methods and condition. This paper presents a standard methodology for preprocessing mineral/rock samples and setting the distance from a target to the sensor, and then examines closely the spectral features for pyrophyllite. The size of mineral/rock samples is various according to the condition and scale of outcrop, so it is important to maintain the distance between the sensor and the sample. Before standardization for preprocessing samples and the sensor and sample distance, we prepare various rock samples (Quartz Porphyry) such as natural rock, pebble, powder and cutting rock. For a qualitative analysis to minimize the effect of surface condition of the sample and shadow, we maintains the distance from the sample to the sensor at 30cm and measures three times repeatedly for cutting the sample at $1{\sim}2cm$ thickness. To illustrate the proposed methodology, a case study for pyrophyllite was carried out. In this study, pyrophyllite showed an absorption pattern at wave length of 1.406nm, 1,868nm, 2.180nm and 2.309nm, and a higher grade represented strong absorption at 1.406nm and 2.180 nm. These absorption feature corresponds the band 7 of LANDSAT TM and band 8 of ASTER imageries. So, using these results, pyrophyllite deposits were extracted from other features (such as barren area, concrete area, bed of river, stone pit area etc.).

Studies on Mineral Composition of Fault Clay in Quaternary Ipsil Fault: High Resolution Powder Diffraction Analysis (제4기 입실 단층 파쇄대에서 나타나는 단층점토의 산출상태에 따른 광물조성 연구: 고해상도분말회절 분석을 중심으로)

  • Park, Sung-Min;Kang, Han;Jang, Yun-Deuk;Im, Chang-Bock;Kim, Jeong-Jin
    • Journal of the Mineralogical Society of Korea
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    • v.20 no.2 s.52
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    • pp.83-89
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    • 2007
  • XRD, HRPD and SEM were used for mineralogical characterization of fault clay in fracture zone from Ipsil. Variations of color in fault clay exhibit significant mineral composition difference. Fault clays from Ipsil are composed mainly of smectite, laumontite, and quartz. Laumontite, a distinct fault clay in Ipsil fault, might be resulted from alteration of bed rock in fracture zone based on the result that no laumontite was found near fault rock. Fault clays from Ipsil are composed mainly of smectite.

Experimental and Numerical Studies on Application of Industrial Explosives to Explosive Welding, Explosive Forming, Shock Powder Consolidation (산업용 폭약을 이용한 폭발용접, 폭발성형과 충격분말고화에 관한 실험 및 수치해석적 연구)

  • Kim, Young-Kook;Kang, Seong-Seung;Cho, Sang-Ho
    • Tunnel and Underground Space
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    • v.22 no.1
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    • pp.69-76
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    • 2012
  • Theoretical backgrounds on the experimental methods of explosive welding, explosive forming and shock consolidation of powders are introduced. Explosive welding experiments of titanium (Ti) and stainless steel (SUS 304) plate were carried out. It was revealed that a series of waves of metal jet are generated in the contact surface between both materials; and that the optimal collision velocity and collision angle is about 2,100~2,800 m/s and $15{\sim}20^{\circ}$, respectively. Also, explosive forming experiments of Al plate were performed and compared to a conventional press forming method. The results confirmed that the shock-loaded Al plate has a larger curvature deformation than those made using conventional press forming. For shock consolidation of powders, the propagation behaviors of a detonation wave and underwater shock wave generated by explosion of an explosive are investigated by means of numerical calculation. The results revealed that the generation and convergence of reflected waves occur at the wall and center position of water column, and also the peak pressure of the converged reflected waves was 20 GPa which exceeds the detonation pressure. As results from the consolidation experiments of metal/ceramic powders ($Fe_{11.2}La_2O_3Co_{0.7}Si_{1.1}$), shock-consolidated $Fe_{11.2}La_2O_3Co_{0.7}Si_{1.1}$ bulk without cracks was successfully obtained by adapting the suggested water container and strong bonding between powder particles was confirmed through microscopic observations.

Current Status of X-ray CT Based Non Destructive Characterization of Bentonite as an Engineered Barrier Material (공학적방벽재로서 벤토나이트 거동의 X선 단층촬영 기반 비파괴 특성화 현황)

  • Diaz, Melvin B.;Kim, Joo Yeon;Kim, Kwang Yeom;Lee, Changsoo;Kim, Jin-Seop
    • Tunnel and Underground Space
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    • v.31 no.6
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    • pp.400-414
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    • 2021
  • Under high-level radioactive waste repository conditions, bentonite as an engineered barrier material undergoes thermal, hydrological, mechanical, and chemical processes. We report the applications of X-ray Computed Tomography (CT) imaging technique on the characterization and analysis of bentonite over the past decade to provide a reference of the utilization of this technique and the recent research trends. This overview of the X-ray CT technique applications includes the characterization of the bentonite either in pellets or powder form. X-ray imaging has provided a means to extract grain information at the microscale and identify crack networks responsible for the pellets' heterogeneity. Regarding samples of pellets-powder mixtures under hydration, X-ray CT allowed the identification and monitoring of heterogeneous zones throughout the test. Some results showed how zones with pellets only swell faster compared to others composed of pellets and powder. Moreover, the behavior of fissures between grains and bentonite matrix was observed to change under drying and hydrating conditions, tending to close during the former and open during the latter. The development of specializing software has allowed obtaining strain fields from a sequence of images. In more recent works, X-ray CT technique has served to estimate the dry density, water content, and particle displacement at different testing times. Also, when temperature was added to the hydration process of a sample, CT technology offered a way to observe localized and global density changes over time.

Quantitative Analysis of 1-Deoxynojirimycin Content Using Silkworm Genetic Resources

  • Ju, Wan-Taek;Kim, Kee-Young;Sung, Gyoo-Byung;Kim, Yong-Soon
    • International Journal of Industrial Entomology and Biomaterials
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    • v.29 no.2
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    • pp.162-168
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    • 2014
  • 1-Deoxynojirimycin(1-DNJ or DNJ), a component in silkworm powder, prevents glucose from being absorbed into the bloodstream from the small intestine by inhibiting ${\alpha}$-glucosidase activity. This study compared the functional components of 1-DNJ from various silkworm species using a gene database with those of 1-DNJ produced by silkworms bred through cross-combinations. We utilized comparisons of geographical origins and species of silkworms using a gene database and discovered that 1-DNJ activity was ranked in the following order by species, Japanese (SK-1) > Chinese (C48) > European (Rock191). 1-DNJ constituted varying percentages of silkworm organs in the following order, blood > epithelial tissue > body fat > silk glands. With regard to sex, 1-DNJ, levels were higher in males than females. However, 1-DNJ levels with respect to various genetic traits (blood color, silk color, and egg color) were consistent. In order to study 1-DNJ changes that occurred during cross breeding of the silkworm gene, we bred cross-combinations utilizing SK-1 and C48 silkworms. In conclusion, in order to provide information about the constituents of functional materials contained in silkworm powder, it is imperative that silkworm cross breeding occurs so that the database of functional materials extracted from silkworms will expand.

Development of Reinforcement Grout Materials Using Blast Furnace Slag Powder and Aramid Fiber (고로슬래그 미분말과 아라미드 섬유를 이용한 보강그라우트재 개발)

  • Seo, Hyeok;Park, Kyung-Ho;Kim, Chan-Jung;Kim, Ho-Chul;Kim, Daehyeon
    • Journal of the Korean Geosynthetics Society
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    • v.18 no.1
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    • pp.67-77
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    • 2019
  • The grouting method is utilized to reinforce and waterproof poor grounds, enhance the bearing capacity of structures damaged resulting from settlement due to elevation and vibration or differential settlement, and for cutoff. The purpose of this research is to enhance the compressive strength of grout materials by using aramid fiber and develop a high-strength ground improvement method by using blast furnace slag powder. In this regard, this study has conducted a uniaxial compression test after checking the high charge (higher than 50%) of the ratio of blast furnace slag powder and cement at 100:0, 70:30 and 40:60%, adding the aramid mixture based on 0, 0.5 and 1.0% of the cement and furnace slag powder weight and creating sand gels based on surface oiling rate of 0.7 and 1.2%. For the environmental review evaluation, a heavy metal exudation test and a pH test measurement have been conducted. The experiment results showed that 1% increase of aramid fiber led to 1.3 times greater uniaxial compression intensity. As for the hexavalent chrome, a 30% increase in blast furnace slag powder led to approximately 50% decrease in heavy metal exudation. However, the pH test revealed that a 30% increase in blast furnace slag powder resulted in approximately 0.5 increase in pH. Further research on the pH part is needed in the future.

Blast Coefficient for Bench Blasting (벤치발파 설계에서 발파계수 설정에 관한 연구)

  • Kim, Hee-Do;Kim, Jung-Kyu;Ko, Young-Hun;Noh, You-Song;Shin, Myeong-Jin;Yang, Hyung-Sik
    • Explosives and Blasting
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    • v.33 no.1
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    • pp.1-12
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    • 2015
  • In this study, the domestic bench blasting sites were researched to set the blast coefficient C according to the type of rock and type of industry. With the use of the experimental data on the representative industrial explosives and the data of the manufacturers'data on explosives, powder coefficient e was set up. The blast coefficient C was 0.21~0.30 when the average value for 5 representative kinds of rocks including granite was searched. The blast coefficient C for quarrying, mining and construction sites were 0.22, 0.13 and 0.26 respectively. On the other hand, powder coefficient e was obtained in four elements such as reactive energy, ballistic mortar test, VOD, Langefors'strength per unit weight. e value for emulsion which is one of the representative explosives was found to be 1 while those of high performance emulsion and ANFO were found to be 0.9 and 1, respectively.