• Title/Summary/Keyword: residual voids

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Study for polycrystalline 3C-SiC thin films growth by LPCVD (LPCVD에 의한 다결정 3C-SiC 결정성장에 관한 연구)

  • Kim, Kang-San;Chung, Gwiy-Sang
    • Proceedings of the KIEE Conference
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    • 2006.07c
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    • pp.1313-1314
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    • 2006
  • The polycrystalline 3C-SiC thin films heteroepitaxially grown by LPCVD method using single precursor 1,3-disilabutane at $850^{\circ}C$. The crystallinity of the 3C-SiC thin film was analyzed by XRD and FT-IR. Residual strain was investigated by Raman scattering. The surface morphology was also observed by AFM and voids or dislocations between SiC and $SiO_2$ were measured by SEM. The grown poly 3C-SiC thin film is very good crystalline quality, surface like mirror, and low defect and strain. Therefore, the polycrystalline 3C-SiC is suitable for harsh environment MEMS applications.

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Growing of polycrystalline 3C-SiC thin films for harsh environment MEMS applications. (극한 환경 MEMS용 다결정 3C-SiC 박막의 성장)

  • Kim, Kang-San;Chung, Gwiy-Sang
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.408-409
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    • 2006
  • The polycrystalline 3C-SiC thin films heteroepitaxially grown by LPCVD method using single precursor 1. 3-disilabutane at $850^{\circ}C$. The crystallinity of the 3C-SiC thin film. was analyzed by XPS. Residual strain was investigated by Raman scattering. The surface morphology and voids between SiC and $SiO_2$ were measured by SEM. The grown poly 3C-SiC thin film is very good crystalline quality, surface like mirror, and low defect and strain. Therefore, the polycrystalline 3C-SiC is suitable for harsh environment MEMS applications.

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Impact Property of S-2 Glass Woven Composites with Different Matrices and Stitching (S-2 유리섬유 평직복합재의 기지재료 및 스티칭에 따른 충격 특성 비교)

  • Byeon, Jun-Hyeong;Hwang, Byeong-Seon;Eom, Mun-Gwang;Lee, Jeong-Hun;Nam, Won-Sang;Song, Seung-Uk;Lee, Chang-Hun
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2005.11a
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    • pp.31-34
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    • 2005
  • For the damage tolerance improvement of conventional laminated composites, stitching process has been utilized for providing through-thickness reinforcements. 2D prefonl1S were stacked with S-2 glass plain weave, and 3D preforms were fabricated using the stitching process. For the matrix system, epoxy and phenol resins were considered. To examine the damage resistance performance the low velocity drop weight impact test has been carried out, and the impact damage was examined by scanning image. CAI (Compressive After Ih1paet) tests were also conducted to evaluate residual compressive strength. Compared with 2D epoxy composites, 2D phenol composites showed drastic reduction in the compressive strength prior to impact because of the higher contents of voids. The damage area of 2D phenol composites were also larger than that of 2D epoxy composites. However, by introducing the stitching, the damage area of 3D phenol composites was reduced by 60%, while the CAI strength improvement was negligible.

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Evaluation of wear chracteristics for $Al_{2}O_{3}-40%TiO_{2}$ sprayed on casting aluminum alloy (주조용 알루미늄합금의 $Al_{2}O_{3}-40%TiO_{2}$ 용사층에 대한 마멸특성 평가)

  • 채영훈;김석삼
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1997.10a
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    • pp.183-190
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    • 1997
  • The wear behaviors of $Al_2O_3-40%TiO_2$ deposited on casting aluminum alloy(ASTM A356) by plasma spray against SiC ball have been investigated experimentally. Friction and wear tests are carried out at room temperature. The friction coefficient of $Al_2O_3-40%TiO_2$ coating is lower than that of pure $Al_2O_3$ coating(APS). It is found that low friction correspond to low wear and high friction to high wear in the experimental result. The thickness of $Al_2O_3-40%TiO_2$ coatings indicated the existence of the optimal coating thickness. It is found that a voids and porosities of coating surface result in the crack generated. As the tensile stresses in coating increased with the increased friction coefficient. The columnar grain of coating will be fractured to achieve the critical stress. It is found that the cohesive of splats and the porosity of surface play a role in wear characteristics. It is suggested that the mismatch of thermal expansion of substrate and coating play an important role in wear performance. Tensile and compressire under thermo-mechanical stress may be occurred by the mismatch between thermal expansion of substrate and coating. This crack propagation above interface is observed in SEM.

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Evaluation of Wear Chracteristics for $Al_2O_3-40%TiO_2$Sprayed on Casted Aluminum Alloy (주조용 알루미늄 합금의 $Al_2O_3-40%TiO_2$ 용사층에 대한 마멸특성 평가)

  • 채영훈;김석삼
    • Tribology and Lubricants
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    • v.15 no.1
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    • pp.39-45
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    • 1999
  • The wear behavior of $Al_2$O$_3$-40%TiO$_2$deposited on casted aluminum alloy (ASTM A356) by APS (Air Plasma Spray) against SiC ball has been investigated in this work. Wear tests were carried out at room temperature. The friction coefficient of $Al_2$O$_3$-40%TiO$_2$coating is lower than that of pure $Al_2$O$_3$coating(APS). $Al_2$O$_3$-40%TiO$_2$coating indicated the existence of the optimal coating thickness. It is found that voids and pores of coating surface resulted in the generation of cracks, and the cohesive of splats and the porosity of surface play a role in wear characteristics. It is suggested that the mismatch of thermal expansion of substrate and coating play an important role in wear performance. Tension and compression under thermo-mechanical stress may be occurred by the mismatch between thermal expansion of substrate and coating. The crack propagation above interface is observed in SEM.

Physical Characteristics of Polycrystalline 3C-SiC Thin Films Grown by LPCVD (LPCVD로 성장된 다결정 3C-SiC 박막의 물리적 특성)

  • Chung Gwiy-Sang;Kim Kang-San
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.19 no.8
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    • pp.732-736
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    • 2006
  • This paper describes the physical characterizations of polycrystalline 3C-SiC thin films heteroepitaxially grown on Si wafers with thermal oxide, In this work, the 3C-SiC film was deposited by LPCVD (low pressure chemical vapor deposition) method using single precursor 1, 3-disilabutane $(DSB:\;H_3Si-CH_2-SiH_2-CH_3)\;at\;850^{\circ}C$. The crystallinity of the 3C-SiC thin film was analyzed by XPS (X-ray photoelectron spectroscopy), XRD (X-ray diffraction) and FT-IR (fourier transform-infrared spectometers), respectively. The surface morphology was also observed by AFM (atomic force microscopy) and voids or dislocations between SiC and $SiO_2$ were measured by SEM (scanning electron microscope). Finally, residual strain was investigated by Raman scattering and a peak of the energy level was less than other type SiC films, From these results, the grown poly 3C-SiC thin film is very good crystalline quality, surface like mirror, and low defect and strain. Therefore, the polycrystalline 3C-SiC is suitable for harsh environment MEMS (Micro-Electro-Mechanical-Systems) applications.

Influence of granite waste aggregate on properties of binary blend self-compacting concrete

  • Jain, Abhishek;Gupta, Rajesh;Chaudhary, Sandeep
    • Advances in concrete construction
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    • v.10 no.2
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    • pp.127-140
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    • 2020
  • This study explores the feasibility of granite waste aggregate (GWA) as a partial replacement of natural fine aggregate (NFA) in binary blend self-compacting concrete (SCC) prepared with fly ash. Total of nine SCC mixtures were prepared wherein one was Ordinary Portland cement (OPC) based control SCC mixture and remaining were fly ash based binary blend SCC mixtures which included the various percentages of GWA. Fresh properties tests such as slump flow, T500, V-funnel, J-ring, L-box, U-box, segregation resistance, bleeding, fresh density, and loss of slump flow (with time) were conducted. Compressive strength and percentage of permeable voids were evaluated in the hardened state. All the SCC mixtures exhibited sufficient flowability, passing ability, and resistance to segregation. Besides, all the binary blend SCC mixtures exhibited lower fresh density and bleeding, and better residual slump (up to 50% of GWA) compared to the OPC based control SCC mixture. Binary blend SCC mixture incorporating up to 40% GWA provided higher compressive strength than binary blend control SCC mixture. The findings of this study encourage the utilization of GWA in the development of binary blend SCC mixtures with satisfactory workability characteristics as a replacement of NFA.

Compressive and tensile strength enhancement of soft soils using nanocarbons

  • Taha, Mohd R.;Alsharef, Jamal M.A.;Khan, Tanveer A.;Aziz, Mubashir;Gaber, Maryam
    • Geomechanics and Engineering
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    • v.16 no.5
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    • pp.559-567
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    • 2018
  • Technological innovations in sustainable materials for soil improvement have attracted considerable interest due to energy crisis and environmental concerns in recent years. This study presents results of a comprehensive investigation on utilization of nanocarbons in reinforcement of a residual soil mixed with 0, 10 and 20% bentonite. Effects of adding proportionate quantities (0, 0.05, 0.075, 0.1 and 0.2%) of carbon nanotubes and carbon nanofibers to soil samples of different plasticities were evaluated. The investigation revealed that the inclusion of nanocarbons into the soil samples significantly improved unconfined compressive strength, Young's modulus and indirect tensile strength. It was observed that carbon nanofibers showed better performance as compared to carbon nanotubes. The nanosized diameter and high aspect ratio of nanocarbons make it possible to distribute the reinforcing materials on a much smaller scale and bridge the inter-particles voids. As a result, a better 'soil-reinforcing material' interaction is achieved and desired properties of the soil are improved at nanolevel.

Development of Environment-friendly Cushioning Materials by Pulping of Waste Residual Woods (폐잔재의 펄프화를 통한 환경친화적 완충소재의 개발)

  • Lee, Young-Min;Kim, Chul-Hwan;Kim, Jae-Ok;Kim, Gyeong-Yun;Shin, Tae-Gi;Song, Dae-Bin;Park, Chong-Yawl
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.38 no.2 s.115
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    • pp.61-71
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    • 2006
  • Environment-friendly shock-absorbing (cushioning) materials were made using a vacuum forming method from waste wood collected from local mountains in Korea. The waste wood was pulped by thermomechanical pulping. The TMP cushions showed superior shock-absorbing properties with lower elastic moduli compared to EPS(Expanded Polystyrene) and pulp mold. Even though the TMP cushions made using at different suction times had many free voids in their inner fiber structures, their apparent densities were a little higher than EPS and much lower than pulp mold. The addition of cationic starch improved elastic modulus of the TMP cushions without increasing the apparent density, which was different from surface sizing with starch. The porosity of the TMP cushions was a little greater than EPS and much less than pulp mold. Finally, the TMP cushions have great potential to endure external impacts occurring during goods distribution.

The Analysis of Wear Phenomena on Added Carbon Content Gas Atmosphere in Ion-Nitriding (이온질화에 있어서 가스중 첨가탄소량에 대한 마모현상 분석)

  • 조규식
    • Tribology and Lubricants
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    • v.13 no.2
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    • pp.96-104
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    • 1997
  • This paper was focused on the wear characteristics of ion-nitrided metal and with ion-nitride processing, which is basically concerned with the effects of carbon content in workpiece and added carbon content gas atmosphere on the best wear performance. Increased carbon content in workpiece increases compound layer thickness, but decreases diffusion layer thickness. On the other hand, a small optimal amount of carbon content in gas atmosphere increase compound layer thickness as well as diffusion layer thickness and hardness. Wear tests show that the compound layer of ion-nitrided metal reduces wear rate when the applied wear load is small. However, as the load becomes large, the existence of compound layer tends to increase wear rate. Compressive residual stress at the compound layer is the largest at the compound layer, and decreases as the depth from the surface increases. It is found in the analysis that under small applied load, the critical depth where voids and cracks may be created and propagated is located at the compound layer, so that the adhesive wear is created and the existence of compound layer reduces the amount of wear. When the load becomes large, the critical depth is located below the compound layer and delamination, which may explained by surface deformation, crack nucleation and propagation, is created and the existence of compound layer increases wear rate. For the compound layer, at added carbon contents of 0 percent and 0.5 at. percent, the $\varepsilon$ monophase is predominant. But at 0.7 at. percent added carbon, the $\varepsilon$ monophase formation tends to be severely inhibited and r' and $Fe_3C$ polyphase formation becomes dominant. This increased hard $\varepsilon$ phase layer was observed to be more beneficial in reducing friction and wear.