• Progress in Superconductivity and Cryogenics
• /
• v.16 no.3
• /
• pp.7-9
• /
• 2014

Single-crystal like $MgB_2$ thin film was grown on (000l) $Al_2O_3$ substrate by using hybrid physical-chemical vapor deposition (HPCVD) system. Single crystal properties were studied by X-ray diffraction (XRD) and the full width at half maximum (FWHM) of the (0001) $MgB_2$ peak is $15^{\circ}$, which is very close to that has been reported for $MgB_2$ single-crystal. It indicates that the crystalline quality of thin film is good. Temperature dependence on resistivity was investigated by physical property measurement system (PPMS) in various applied fields from 0 to 9 T. The upper critical field ($H_{c2}$) and irreversibility field ($H_{irr}$) were determined from PPMS data, and the estimated values are comparable with that of $MgB_2$ single-crystals. The thin film shows a high critical temperature ($T_c$) of 40.4 K with a sharp superconducting transition width of 0.2 K, and a high residual resistivity ratio (RRR=21), it reflects that $MgB_2$ thin film has a pure phase structure.

• Journal of the Korean Ceramic Society
• /
• v.33 no.1
• /
• pp.56-64
• /
• 1996

A large amount of papers about the cubic-to-tetragonal phase transition the ferroelectric domain structures of the BaTiO3 were already reported but there exist still some needs to observe the domain behaviors directly. In this study the domain structures of the tinned plates prepared from ta single crystal grown by the TSSG technique were observed using a polarizing microscope TE and X-ray topography. The spatial relation be-tween the orientation states of domains was investigated and the effects of external stresses and electric fields on the behaviors of ferroelectric and ferroelastic domains were studied. All the 90$^{\circ}$walls cut off in the crystal are the wedge shaped lamellar domains and all the straight boundaries in the observed domain patte군 can be interpreted as the head-to-tail 90$^{\circ}$walls. The irregular overlapped boundaries commonly observed by using a polarizing microscope and X-ray topography are complex combinations of well-known 90$^{\circ}$walls and are domain walls were predominant and were stabilized after surface polishing. In the paraelectric phase region the domain walls vanished but the residual surface strain patterns could be seen at the same positions of the stabilized 90$^{\circ}$a-a walls in the tetragonal phase region, These stabilized walls resulted from the surface strain had a memory effect in domain formation during the repeated phase transitions and could notr be affected by an external electtric field.

• Journal of Sensor Science and Technology
• /
• v.16 no.6
• /
• pp.462-466
• /
• 2007

Aluminum nitride (AlN) thin films were deposited on Si substrates by using polycrystalline (poly) 3C-SiC buffer layers, in which the AlN film was grown by pulsed reactive magnetron sputtering. Characteristics of grown AlN films were investigated experimentally by means of FE-SEM, X-ray diffraction, and FT-IR, respectively. The columnar structure of AlN thin films was observed by FE-SEM. X-ray diffraction pattern proved that the grown AlN film on 3C-SiC layers had highly (002) orientation with low value of FWHM (${\Theta}=1.3^{\circ}$) in the rocking curve around (002) reflections. These results were shown that almost free residual stress existed in the grown AlN film on 3C-SiC buffer layers from the infrared absorbance spectrum. Therefore, the presented results showed that AlN thin films grown on 3C-SiC buffer layers can be used for various piezoelectric fields and M/NEMS applications.

• Journal of the Society of Naval Architects of Korea
• /
• v.28 no.1
• /
• pp.139-149
• /
• 1991

In this paper, an efficient method for the ultimate longitudinal strength analysis of the double skin hull girder is presented by using idealized structural unit method. Idealized plate element subjected to biaxial load is developed taking account of initial deflection and welding residual stress. Interaction effect between local and global buckling in the whole structure is also taken into consideration. The reserve strength factor and reliability index for the example 40K double skin product oil carrier are evacuated against the ultimate longitudinal strength. It is concluded that the prudent method seems to be useful in the sense that the computing time required is very short while giving the reasonable solution.

• Transactions of Materials Processing
• /
• v.18 no.1
• /
• pp.45-51
• /
• 2009

Shape memory alloy has been used to improve the tensile strength of composite by the occurrence of compressive residual stress in matrix using its shape memory effect. In order to fabricate shape memory alloy composite, TiNi alloy fiber and Al2024 sheets were used as reinforcing material and matrix, respectively. In this study, TiNi/Al2024 shape memory alloy composite was made by using hot press method. In order to investigate bonding condition between TiNi reinforcement and Al matrix, the micro-structure of interface was observed by using optical microscope and diffusion layer of interface was measured by using Electron Probe Micro Analyser. And the mechanical properties of composite with three parameters(volume fraction of fiber, cold rolling amount and test temperature) were obtained by tensile test. The most optimum bonding condition for fabrication the TiNi/Al2024 composite material was obtained as holding for 30min. under the pressure of 60MPa at 793K. The strength of composite material increased considerably with the volume fraction of fiber up to 7.0%. And the tensile strength of this composite increased with the reduction ratio and it also depends on the volume fraction of fiber.

• Microbiology and Biotechnology Letters
• /
• v.19 no.5
• /
• pp.514-520
• /
• 1991

Direct synthesis of cyclodextrin (CD) from extruded insoluble corn starch without liquefaction procedure using cyclodextrin glucanotransferase (CGTase) was carried out. Increased CD production rate and yield were achieved in heterogeneous enzyme reaction system containing extruded corn starch compared with those of conventional system employing liquefied or partially cyclized starch. At extruded starch concentration of 100 g/l the CD concentration and conversion yield were reached up to 54 g/l and 0.54, respectively. High purity of $\alpha \beta \gamma$-CDs without accumulation of undesirable malto-oligosaccharides was produced, furthermore, the residual extruded starch was easily separated by centrifugation from reaction mixture, whlch will facilitate the purification procedure. Granular structure of extruded starch was observed by SEM to investigate enzyme reaction mechanism. Supplemental addition of $\alpha$-amylase enhanced slightly the initial CD production rate, but it decomposed produced CD at the late stage. Various! extruded raw starches, such as, corn, rice, and barley were also suitable substrates for CD production.

• Journal of Environmental Health Sciences
• /
• v.30 no.3
• /
• pp.264-271
• /
• 2004

An aquatic food chain was constructed to provide information of bioaccumulation of DEHP as followed: phytoplankton(Scenedesmus subspicatus) ${\rightarrow}$ zooplankton(Daphnia magna) ${\rightarrow}$ fish(Oryzias latipes). After 10 days of exposure to DEHP, the fish and culture water were analyzed for residual concentration of DEHP and BAF(Bioaccumulation Factor) was determined. In addition, BCF(Bioconcentration Factor) was calculated in exposure tank in which fish were only exposed DEHP by culture water. These experiments provide the relative importance between BAF and BCF. In this study, BCF and BAF did not show any significant difference. Another work in this study was model construction and application to investigate the effect of food chain structure to BAF in higher organism (fish). The model constructed in this study considered the biological characteristics of DEHP such as metabolic parameters, as well as the chemical characteristics such as solubility. This model could be used in prediction of bioaccumulation level in dependent of various food chain structures, when the target organisms or chemicals would be changed.

• The Transactions of The Korean Institute of Electrical Engineers
• /
• v.56 no.11
• /
• pp.1998-2003
• /
• 2007

A flexible but implantable polyimide-based neural implant was fabricated for reliable and stable long-term monitoring of neural activities from brain. The developed neural implant provides 3-dimensional (3D) $3{\times}3$ structure, avoids any hand handling, and makes the insertion more efficient and reliable. Any film curvature caused by residual stress was not observed in the electrode. The 3D flexible polyimide electrode penetrated a dense gel whose stiffness is close to live brain tissue, because a ${\sim}1{\mu}m$ thick nickel was electroplated along the edge of the shank in order to improve the stiffness. The recording sites were positioned at both side of the shank to increase the probability of recording neural signals from a target volume of tissue. Impedance remained stable over 72 hours because of extremely low moisture uptake in the polyimide dielectric layers. At electrical recording test in vitro, the fabricated electrode showed excellent recording performance, suggesting that this electrode has the potential for great recording from neuron firing and long-term implant performance.

• Proceedings of the Korean Society For Composite Materials Conference
• /
• 2000.11a
• /
• pp.245-248
• /
• 2000

Modern aircraft composite structures are designed using a damage tolerance philosophy. This design philosophy envisions sufficient strength and structural integrity of the aircraft to sustain major damage and to avoid catastrophic failure. The only reasonable way to treat on the same basis all the conditions and uncertainties participating in the design of damage tolerant composite aircraft structures is to use the probability-based approach. Therefore, the model has been developed to assess the probability of structural failure (POSF) and associated risk taking into account the random mechanical loads, random temperature-humidity conditions, conditions causing damages, as well as structural strength variations due to intrinsic strength scatter, manufacturing defects, operational damages, temperature-humidity conditions. The model enables engineers to establish the relationship between static/residual strength safety margins, production quality control requirements, in-service inspection resolution and criteria, and POSF. This make possible to estimate the cost associated with the mentioned factors and to use this cost as overall criterion. The methodology has been programmed into software.

• Earthquakes and Structures
• /
• v.3 no.5
• /
• pp.767-781
• /
• 2012

The residual capacity against collapse of a main shock-damaged bridge can be coupled with the aftershock ground motion hazard to make an objective decision on its probability of collapse in aftershocks. In this paper, a steel tower suspension bridge with a main span of 2000 m is adopted for a case-study. Seismic responses of the bridge in longitudinal and transversal directions are analyzed using dynamic elasto-plastic finite displacement theory. The analysis is conducted in two stages: main shock and aftershocks. The ability of the main shock-damaged bridge to resist aftershocks is discussed. Results show that the damage caused by accumulated plastic strain can be ignored in the long-span suspension bridge. And under longitudinal and transversal seismic excitations, the damage is prone to occur at higher positions of the tower and the shaft-beam junctions. When aftershocks are not large enough to cause plastic strain in the structure, the aftershock excitation can be ignored in the seismic damage analysis of the bridge. It is also found that the assessment of seismic damage can be determined by superposition of damage under independent action of seismic excitations.