• Title/Summary/Keyword: residual condition

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Sintering and Dielectric Properties in Cordierite/Glass Composite for LTCC Application (Cordierite/Glass Composite계 LTCC 소재의 소결 및 유전특성)

  • Hwang, Il-Sun;Yeo, Dong-Hun;Shin, Hyo-Soon;Kim, Jong-Hee
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.2
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    • pp.144-150
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    • 2008
  • Recently, there has been growing interest in low loss and low dielectric constant material for LTCC application, as the frequency range for electronic devices increases. This study was designed to evaluate the effect of cordierite filler for low dielectric constant LTCC material. From the previous experiments, two glass compositions of B-Si-Al-Zn-Ba-Ca-O and B-Si-Al-Sr-Ca-O system, were chosen. Each powder of two glass compositions was sintered respectively with commercial cordierite powder in temperature range from $800^{\circ}C\;to\;900^{\circ}C$. Crystalline cordierite and glass peaks were affected only with two factors of composition and sintering temperature among various factors. With the optimized condition of two cordierite/glass compositions, obtained dielectric constant was below 5.5 and quality factor was above 1,000. Closed pore of sintered body was controled by sintering temperature and sintering time. When cordierite/glass composite with ratio of 5.5:4.5 was sintered at $900^{\circ}C$, densification was sufficient with good dielectric characteristics of ${\epsilon}_r<5.1,\;Q{\ge}1,000$. Residual fine closed pores could be reduced with control of sintering temperature and time. 3 point bending strength and chemical durability were evaluated to obtain feasibility for substrate material.

Studies of Cyclosporin A Biosynthesis under the Conditions of Limited Dissolved Oxygen or Carbon Source in Fed-batch Culture (용존산소 제한 또는 탄소원 제한 조건의 유가식배양에서의 Cyclosporin A 생합성 연구)

  • 전계택;박성관;권호균;정연호;정용섭;장용근;이영행
    • KSBB Journal
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    • v.13 no.2
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    • pp.203-208
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    • 1998
  • We investigated the effects of dissolved oxygen (D.O.) and fructose (C-source) on cell growth and biosynthesis of cyclosporin A (CyA) produced as a secondary metabolite by a wild-type filamentous fungus, Tolypocladium inflatum. This was performed by controlling the level of D.O. and the residual C-source, as required, through adjustment of medium flow rate, medium concentration and agitation rate in fed-batch cultures. CyA production was furned out to be maximal, when D.O. level was controlled around 10% saturated D.O. and concentration of the C-source was maintained sufficiently low (below 2 g/L) not to cause carbon catabolite repression. Under this culture condition, we obtained the highest values of CyA concentration (507.14 mg/L), Qp (2.11 mg CyA/L/hr), $Y_x/s$ (0.49 g DCW/g fructose), $Y_p/s$<(22.56 mg CyA/g fructose), and YTEX>$_p/x$ (48.31 mg CyA/g DCW), but relatively lower values of cell concentration (11.98 g DCW/L) and cell productivity (0.043 g DCW/L/hr), in comparison with other parallel fed-batch fermentation conditions. These results implied that, in the carbon-limited culture with 10% saturated D.O. level, the producer microorganism utilized the C-source more efficiently for secondary metabolism.

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Cure Behavior of a DGEBF Epoxy using Asymmetric Cycloaliphatic Amine Curing Agent (비대칭 고리형 지방족 아민 경화제를 이용한 DGEBF 계열 에폭시의 경화 거동)

  • Kim, Hongkyeong
    • Korean Chemical Engineering Research
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    • v.46 no.1
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    • pp.200-204
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    • 2008
  • The curing kinetics of diglycidyl ether of bisphenol F (DGEBF) with an asymmetric cycloaliphatic amine curing agent were examined by thermal analysis in both isothermal and dynamic curing conditions. From the residual curing of the samples partially cured in isothermal condition and from the dynamic curing with various heating rates, it was found that there exist two kinds of reactions such as at low temperature and at high temperature regions. It was thus also found that the cure parameters obtained from the isothermal curing kinetic model hardly estimate experimental results for a degree of cure larger than 0.6. The activation energies and frequency factors of these two kinds of reactions were obtained from the dynamic curing experiments with various heating rates. From the curing analysis, it was verified that the total cure kinetics for low degrees of cure is dominated by the cure reaction in the low temperature region.

Characteristics of Machined Surface Roughness and Surface Layers of WC-Co Tools with Plasma Source Ion Implantation (WC-Co 공구의 이온 주입에 따른 표면층 및 가공된 표면거칠기 특성)

  • Kang, Seong-Ki;Kim, Yung-Kyu;Wang, Duck-Hyun;Chun, Young-Rok;Kim, Won-Il
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.9 no.1
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    • pp.106-113
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    • 2010
  • The most suitable condition for plasma source ion implantation(PSII) was found based on the study of the characteristics of PSIIed tool and machined surfaces. The depth analysis according to the chemical bonding state of elements and surface component elements through the XPS and SIMS, was conducted to find the improved property of the PSIIed surface. Due to the diffusion of PSII, the nitrogen was found up to a depth of about 150nm according to the supplied voltage and ion implanted time. The deep diffusion by nitrogen caused the surface modification, but the formation of oxide component was found due to the residual gas contamination on the surface. Statistical method of ANOVA was conducted to find the effects of spindle speed and feed rate in interaction for machined surface roughness with PSIIed tools. The surface modification was found largely occurred by the nitrogen implanted surface with 2 hours for 27kV, 35kV and 43kV.

Characteristics of Friction Welding of Bulk Metallic Glass Rods and Tubes (벌크 비정질 금속 봉재 및 튜브재의 마찰접합 특성)

  • Shin, Hyung-Seop;Park, Jung-Soo;Jung, Yoon-Chul
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.33 no.7
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    • pp.687-692
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    • 2009
  • The friction welding of Zr-based bulk metallic glass (BMG) rods and tubes to similar BMGs, and to crystalline metals were performed. An infrared thermal imager (FLIR-Thermal Cam SC-2000) was used to measure the temperature distribution at joining interface of the specimens during friction welding. All BMGs adopted in this study showed a successful friction joining to similar BMG. The shape of the protrusion formed at the weld interface were examined. In order to characterize the friction weld interface, the micrographic observation and the X-ray diffraction analysis on the weld cross-section were carried out. The obtained results were discussed based on the temperature distribution measured at the weld interface A successful joining of the BMGs to crystalline metals could be obtained for certain pairs of the material combination through the precise control of the friction condition. The residual strength after dissimilar friction welding of BMG was evaluated by the four-point bending test and compared with the cases of friction welding to similar materials.

A Study on the Investigation of Optimal Peening Intensity for Shot Peened Spur Gear (쇼트피닝가공한 평기어의 최적 피닝강도 탐색에 관한 연구)

  • Cheong Seong-Kyun;Lee Dong-Sun;Lee Kook-Jin;Kim Tae-Hyung
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2005.05a
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    • pp.185-190
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    • 2005
  • The shot peening process is often used to improve fatigue properties of metal parts. Among them, It is the most use in an auto-component. In order to achieve optimum, repeatable and reliable fatigue enhancement from the shot peening process, the important shot peening parameters must be controlled. In this paper, the optimum peening intensity (Almen intensity) condition is investigated by experiment. The Spur Gear steel was used to investigate shot peening effects. The fatigue life at $\sigma_a=1,050$ and $\sigma_a=1,250MPa$ first gently increases, then drops gently as peening intensity increases compared with unpeened specimen. Experimental results show that the optimum peening intensity range is $0.391\~0.434mmA$..So the fatigue strength and fatigue life have been tremendously increased by optimum-peening treatment. However, the fatigue strength and fatigue life have been decreased by over peeing.

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The Versatility of Cervical Vertebral Segmentation in Detection of Positional Changes in Patient with Long Standing Congenital Torticollis

  • Hussein, Mohammed Ahmed;Kim, Yong Oock
    • Journal of International Society for Simulation Surgery
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    • v.3 no.1
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    • pp.28-32
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    • 2016
  • Background Congenital muscular torticollis (CMT) is a benign condition. With early diagnosis and appropriate management, it can be cured completely, leaving no residual deformity. However, long-standing, untreated CMT can lead to permanent craniofacial deformities and asymmetry.Methods Nineteen patients presented to the author with congenital muscular torticollis. Three dimensional computed tomography (3-D CT) scans was obtained upon patient’s admission. Adjustment of skull’s position to Frankfort horizontal plan was done. Cervical vertebral segmentation was done which allowed a 3D module to be separately created for each vertebra to detect any anatomical or positional changes.Results The segmented vertebrae showed an apparent anatomical changes, which were most noticeable at the level of the atlas and axis vertebrae. These changes decreased gradually till reaching the seventh cervical vertebra, which appeared to be normal in all patients. The changes in the atlas vertebra were mostly due to its intimate relation with the skull base, while the changes of the axis were the most significantConclusion Cervical vertebral segmentation is a reliable tool for isolation and studying cervical vertebral pathological changes of each vertebra separately. The accuracy of the procedures in addition to the availability of many software that can be used for segmentation will allow many surgeons to use segmentation of the vertebrae for diagnosis and even for preoperative simulation planning.

Study on DC-Offset Cancellation in a Direct Conversion Receiver

  • Park, Hong-Won
    • The Bulletin of The Korean Astronomical Society
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    • v.37 no.2
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    • pp.157.2-157.2
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    • 2012
  • Direct-conversion receivers often suffer from a DC-offset that is a by-product of the direct conversion process to baseband. In general, a basic approach to reduce the DC-offset is to do simple average of the baseband signal and remove the DC by subtracting the average. However, this gives rise to a residual DC offset which degrades the performance when the receiver adopts the coding schemes with high coding rates such as 8-PSK. Therefore, more advanced methods should be additionally required for better performance. While the training sequences are basically designed to have good auto-correlation properties to facilitate the channel estimation, they may be not good for the simultaneous estimation of the channel response and the DC-offset. Also the DC offset compensation under a bad condition does not give good results due to the estimation error. Correspondingly, the proposed scheme employs the two important points. First, the training sequence codes are divided into two groups by MSE(Mean Squared Errors) for estimating the channel taps and then SNR calculated from each group is compared to predefined threshold to do fine DC-offset estimation. Next, ON/OFF module is applied for preventing performance degradation by large estimation error under severe channel conditions. The simulation results of the proposed scheme shows good performances compared to the existing algorithm. As a result, this scheme is surely applicable to the receiver design in many communications systems.

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Reserve capacity of fatigue damaged internally ring stiffened tubular joints

  • Thandavamoorthy, T.S.
    • Steel and Composite Structures
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    • v.4 no.2
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    • pp.149-167
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    • 2004
  • Offshore platforms have to serve in harsh environments and hence are likely to be damaged due to wave induced fatigue and environmental corrosion. Welded tubular joints in offshore platforms are most vulnerable to fatigue damage. Such damages endanger the integrity of the structure. Therefore it is all the more essential to assess the capacity of damaged structure from the point of view of its safety. Eight internally ring stiffened fatigue damaged tubular joints with nominal chord and brace diameter of 324 mm and 219 mm respectively and thickness 12 mm and 8 mm respectively were tested under axial brace compression loading to evaluate the reserve capacity of the joints. These joints had earlier been tested under fatigue loading under corrosive environments of synthetic sea water and hence they have been cracked. The extent of the damage varied from 35 to 50 per cent. One stiffened joint was also tested under axial brace tension loading. The residual strength of fatigue damaged stiffened joint tested under tension loading was observed to be less than one fourth of that tested under compression loading. It was observed in this experimental investigation that in the damaged condition, the joints possessed an in-built load-transfer mechanism. A bi-linear stress-strain model was developed in this investigation to predict the reserve capacity of the joint. This model considered the strain hardening effect. Close agreement was observed between the experimental and predicted results. The paper presents in detail the experimental investigation and the development of the analytical model to predict the reserve capacity of internally ring stiffened joints.

Dynamic prediction fatigue life of composite wind turbine blade

  • Lecheb, Samir;Nour, Abdelkader;Chellil, Ahmed;Mechakra, Hamza;Ghanem, Hicham;Kebir, Hocine
    • Steel and Composite Structures
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    • v.18 no.3
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    • pp.673-691
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    • 2015
  • In this paper we are particularly focusing on the dynamic crack fatigue life of a 25 m length wind turbine blade. The blade consists of composite materiel (glass/epoxy). This work consisted initially to make a theoretical study, the turbine blade is modeled as a Timoshenko rotating beam and the analytical formulation is obtained. After applying boundary condition and loads, we have studied the stress, strain and displacement in order to determine the critical zone, also show the six first modes shapes to the wind turbine blade. Secondly was addressed to study the crack initiation in critical zone which based to finite element to give the results, then follow the evolution of the displacement, strain, stress and first six naturals frequencies a function as crack growth. In the experimental part the laminate plate specimen with two layers is tested under cyclic load in fully reversible tensile at ratio test (R = 0), the fast fracture occur phenomenon and the fatigue life are presented, the fatigue testing exerted in INSTRON 8801 machine. Finally which allows the knowledge their effect on the fatigue life, this residual change of dynamic behavior parameters can be used to predicted a crack size and diagnostic of blade.