• Journal of Food Hygiene and Safety
• /
• v.14 no.1
• /
• pp.76-83
• /
• 1999

Solid phase microextraction (SPME) was used for the determination of 6 standard solvents (methanol, isopropanol, methyl ethyl ketone, ethyl acetate, cyclohexane, toluene) in food packaging materials. SPME method is a solvent-free sample preparation technique in which a fused silica fiber coated with polymeric organic liquid is introduced into the headspace above the sample. SPME method using fiber coated polydimethylisiloxane (PDMS) was compared with static headspace (SHS) method used as a reference. It was found that the optimal adsorption condition using PDMS-SPME method was 2$0^{\circ}C$ for 15 minutes for the standard solvents. Detection limits, linearity, reproducibility and recovery of both SHS and PDMS-SPME methods have been determined using 6 standard solvents. Both methods were characterized by high reproducibility and good linearity. Using SHS methods, the mean recovery of the 6 standard solvents was ranged from 75.5% to 105.8% with a mean relative standard deviation (RSD) of 0.3% to 4.8%. With PDMS-SPME method, the mean recovery of the 6 standard solvents was ranged from 86.7% to 108.3% with a mean RSD of 0.4% to 2.5%. The detection limits of both methods were the same for toluene, cyclohexane and methyl ethyl ketone; those of PDMS-SPME method were higher than those of SHS method for methanol, isopropanol and ethyl acetate. PDMS-SPME fiber shoed excellent adsorption for non-polar solvents such as toluene, while it showed relatively low adsorption for polar solvents such as methanol.

• Proceedings of the Korean Society of Soil and Groundwater Environment Conference
• /
• 2003.04a
• /
• pp.259-262
• /
• 2003

In the Republic of Korea, Ministry of Construction & Transportation and Korea Water Resources Corporation manage the national groundwater monitoring network at the 169 stations and will organize the supplementary groundwater monitoring network at the 10,000 stations by 2011 year. The method that organizes the monitoring network was developed using the Analytic Hierarchy Process with pairwise comparison. Several estimation factors for the estimating every district were selected to reflect each district conditions. Their weighting value was decided by pairwise comparison and questions to the experts about groundwater The optimal number of groundwater monitoring well was calculated through the developed method. To verify this method, groundwater was monitored in Jeonju city by way showing the example. The study area In Jeonju city needs 7 stations for the supplementary groundwater monitoring network. The results monitored in 7 stations inferred the groundwater level around the study area by Kriging. The mean of residual between inferred groundwater level value from Kriging and actual groundwater level is rather low. Furthermore, the mean and standard deviation of residual between inferred groundwater level change and actual groundwater change is much lower. The Fact that 7 monitoring stations are sufficient for observing the groundwater condition in the study area makes it possible for suggested monitoring number to be proper.

• Journal of Welding and Joining
• /
• v.31 no.5
• /
• pp.7-14
• /
• 2013

The legitimacy of dominating factor in the high accuracy prediction of welding distortion was investigated for butt welding and fillet welding. When out-of-plane distortion was measured by the experiment objecting to butt welding, if tack welding was easily performed, the position of a neutral axis was variously changed by the irregularity. Then, there have been a case that out-of-plane distortion was generated in the unexpected direction. This case should be especially noted. New model for the experiment was proposed so as to solve this problem. As it was elucidated by the case of fillet welding, it was verified that the analysis should be carried out with satisfying the yield condition (especially at high temperature above 700 degree Celsius) and with closely simulating the penetration shape (heat input in weld metal) in order to solve the proposition that is the high accuracy prediction of welding distortion. It was confirmed that residual stress is highly predicted because welding distortion is highly predicted, too.

• Explosives and Blasting
• /
• v.17 no.4
• /
• pp.32-50
• /
• 1999

This study deals with interface charactristics of tube and tubesheet of the nuclear steam generator by the explosive expansion in order to take advantage of optimum expansion ratio, pull-out strength and leakage tightness and improvement of the resisitance on the stress corrosion cracking for low residual stress. The paper also show the relationship between roll, hydraulic and explosive expansion. The results obtain are as follows (1) Because of the explosive bonding is to use the high speed pressure and energy by the explosive, workability is good, bonding region is homogenous (2) Expansion ratio is 2.7%, Pull-out strength 850kg, Leakage strength $500kg/cm^2$. Clearance gap is 10~30mm in case of explosive expansion and interface structure of the tube and tubesheet is optimum condition. (3) As the transition region of the explosive expansion is inactive, the resistance of the stress corrosion cracking is increases 30~40% compare to the roll and hydraulic expansion.

• Proceedings of the KIEE Conference
• /
• 2006.07b
• /
• pp.783-784
• /
• 2006

In case of a difference exist between the experimental value and estimated value of back-emf, there can be a difference of turn number or residual flux density of permanent maget of the motor. In order to presume the turn number, the average length for each coil is used to calculate the resistance. However in producing the motor, doc to the tension of coil, the outer diameter of coil becomes smaller, and then the resistance estimated by average length for each coil is not correct. Therefore in this paper, through the comparison of experiment value and estimated value of inductance, a method of presuming the turn number and PM's residual flux density of an IPM motor is presented. The inductance of IPM motor changes with the rotor position, therefore the rotor part is taken out and then the inductance in open circuit condition is measured. In the analytical calculation, 3D FEM(Finite Element Method) is used, which can consider the leakage flux of end turns in frinzing effect.

• Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
• /
• 2001.05a
• /
• pp.338-343
• /
• 2001

Recently the steel parts used at automobiles are required to be used under high stress more than ever before in need of the weight down. To achieve this requirement of a high strength steel, it must be necessary to decrease inclusion content and surface defect as like decarburization, surface roughness etc., In this study, the surface conditions are measured to know the influence on fatigue properties by two cases of shot peening of two-stage shot peening and single-stage shot peening. And for this study, two kinds of spring steel(SAE 9254, DIN 50CrV4) are made. This study shows the outstanding improvement of fatigue properties at the case of two-stage shot peening in the rotary bending fatigue test and this is assumed to be from (1) on low stress condition, the single stage shot peening is not affected by nonmetallic inclusion under metal. (2) it is possible that the two-stage shot peening increases the fatigue life and the high stress, but, that is affected by nonmetallic inclusion under metal. (3) so far, beeasily 50CrV4 have made high stress. But, results also show fatigue failures originated at inclusion near surface, and this inclusion type is turned out to be a alumina of high hardness.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.31 no.7
• /
• pp.475-480
• /
• 2018

We investigated the tribological properties of amorphous carbon (a-C) films deposited with CrC interlayers of various thicknesses as the adhesive layer. A-C and CrC thin films were deposited using the unbalanced magnetron (UBM) sputtering method with graphite and chromium as the targets. CrC films as the interlayer were fabricated under a-C films, and various structural, surface, and tribological properties of a-C films deposited with various CrC interlayer thicknesses were investigated. With various CrC interlayer thicknesses under a-C films, the tribological properties of CrC/a-C films were improved; the increased film thickness exhibited a maximum high hardness of over 27.5 GPa, high elastic modulus of over 242 GPa, critical load of 31 N, residual stress of 1.85 GPa, and a smooth surface below 0.09 nm at the condition of 30-nm CrC thickness.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.23 no.2
• /
• pp.98-102
• /
• 2010

This paper describes that single crystalline 3C-SiC (cubic silicon carbide) thin films have been deposited on carbonized Si(100) substrates using hexamethyldisilane (HMDS, $Si_2(CH_3){_6}$) as a safe organosilane single precursor and a nonflammable mixture of Ar and $H_2$ gas as the carrier gas by APCVD at $1280^{\circ}C$. The deposition was performed under various conditions to determine the optimized growth condition. The crystallinity of the 3C-SiC thin film was analyzed by XRD (X-ray diffraction). The surface morphology was also observed by AFM (atomic force microscopy) and voids between SiC and Si interfaces were measured by SEM (scanning electron microscopy). Finally, residual strain and hall mobility was investigated by surface profiler and hall measurement, respectively. From these results, the single crystalline 3C-SiC film had a good crystal quality without defects due to viods, a low residual stress, a very low roughness.

• Proceedings of the Korean Vacuum Society Conference
• /
• 2010.02a
• /
• pp.47-47
• /
• 2010

Discharge under the water is very hard and demand considerable high voltage. But specially improved electrode can generate plasma discharge to salty water with relatively low voltage. A round shape ceramic electrode having many pinholes combined with metallic one can generate plasma. 400 volt, 10 kHz and 3 micro second pulse width were applied to repeatedly running synthetic seawater with 10 L/m velocity, containing cultivated E. coli and Bacillus. As a result, 18, 94, 99.97, 100, 100 % disinfection rates to E. coli and 17.1, 17.1, 82.9, 99.4, 99.9 % disinfection rates to Bacillus subtilis were achieved to 1, 2, 3, 4, 5 times repetitive treatment respectively. In the plasma condition, the ions and electrons are separated and new kinds of components are re-synthesized by the intensive movement of the components. Especially chlorine ions are separated and recombined to residual free chlorine like HOCl, $OCl^-$. The residual free chlorine concentrations of discharged water were 0.25, 0.88, 1.39, 1.59, 1.66 mg $Cl_2$/L after 5 times treatment respectively. Another unconfirmed radical and oxidants for example, OH, $H_2O_2$, and $O_3$ can have an effect on microorganism of course.

• Korean Journal of Materials Research
• /
• v.16 no.12
• /
• pp.743-746
• /
• 2006

ZTA tubes were prepared by centrifugal casting and sintered at $1600^{\circ}C$ for 2 hrs. The ZTA tubes were machined into specimens of $3{\times}4{\times}40$ mm. Molten Soda lime glass (SLG) was penetrated into the surface of ZTA at an optimized condition of $1500^{\circ}C$ for the holding time of 5 h and furnace cooled. The extra glass on the surface was removed using a resin bonded diamond wheel. The glass penetrated samples were tested for their flexural strength using four point bend test. Vickers Indentation cracks were made on the glass penetrated surface at different loads of 9.8 N, 49 N, 98 N and 196 N. The residual compression on the surface enhanced the flexural strength and crack arrest behaviour remarkably. This was attributed to the thermoelastic mismatch between the glass and ZTA matrix during cooling.