• Geophysics and Geophysical Exploration
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• v.22 no.2
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• pp.80-87
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• 2019

In this paper, we propose a method to apply the polynomial fitting for regional-residual separation of microgravity data based on the characteristics of gravity anomaly without a prior information. Since the microgravity survey is usually carried out in small regions, it is common to approximate regional anomaly by the first-order polynomial plane. However, if the regional anomaly patterns are difficult to be approximated to a first-order plane, the complete gravity anomaly is divided into small zones enough to approximate first-order plane by means of Parasnis density estimation method. The regional-residual separation is then applied on the splitted zones individually. When the gravity anomalies can be splitted spatially, we showed that the residual anomalies can be more effectively extracted based on the regional geological structures by regional anomaly separation from each of the divided regions, rather than applying the entire data set at one time.

• 한국지구물리탐사학회:학술대회논문집
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• 2006.06a
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• pp.155-160
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• 2006

In this paper, we propose a spatial filtering scheme using factorial kriging, one of geostatistical filtering methodin order to separate regional and residual gravity anomaly. This scheme is based on the assumption that regional anomalies have longer distance relation and residual anomalies have effected on smaller range. We decomposed gravity anomalies intotwo variogram models with long and short effectiveranges by means of factorial kriging. And decomposed variogram models produced the regional and residual anomalies. This algorithm was examined using by a synthetic gravity data, and applied to a real microgravity data to figure out abandoned mineshaft.

• Korean Journal of Food Science and Technology
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• v.42 no.4
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• pp.390-397
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• 2010

Residual solvents in foods are defined as organic volatile chemicals used or produced in manufacturing of extracts or additives, or functional foods. The solvents are not completely eliminated by practical manufacturing techniques and they also may become contaminated by solvents from packing, transportation or storage in warehouses. Because residual solvents have no nutritional value but may be hazardous to human health, there is a need to remove them from the final products or reduce their amounts to below acceptable levels. The purpose of this study was to develop and evaluate an analytical method for the screening of residual solvents in health functional foods. Furthermore, the aim of this study was to constitute a reasonable management system based on the current state of the market and case studies of foreign countries. Eleven volatile solvents such as MeOH, EtOH, trichloroethylene and hexane were separated depending on their column properties, temp. and time using Gas Chromatography (GC). After determining the GC conditions, a sample preparation method using HSS (Head Space Sampling) was developed. From the results, a method for analyzing residual solvents in health functional foods was developed considering matrix effect and interference from the sample obtained from the solution of solvents-free health functional foods spiked with 11 standards solutions. Validation test using the developed GC/HSS/MS (Mass Spectrometry) method was followed by tests for precision, accuracy, recovery, linearity and adequate sensitivity. Finally, examination of 104 samples grouped in suits was performed by the developed HSS/GC/MS for screening the solvents. The 11 solvents were isolated from health functional foods based on vapor pressure difference, and followed by separation within 15 minutes in a single run. The limt of detection (LOD), limit of quantification (LOQ), recovery and coefficient of variation (C.V.) of these compounds determined by the HSS/GC/MS were found to be 0.1 pg/mL, 0.1-125 pg/g, 51.0-104.6%, and less than 15%, respectively. Using the developed HSS/GC/MS method, residual solvent from 16 out of 104 health functional products were detected as a EtOH. This method therefore seems t o be a valuable extension ofanalytical method for the identification of residual solvents in health functional food.

• Geophysics and Geophysical Exploration
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• v.15 no.2
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• pp.51-56
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• 2012

One of the most critical and essential procedures in the interpretation of gravity and magnetic data is to separate the anomaly due to the specific geologic structure from the summation of effects from a broad variety of geologic sources, especially those of different depths. Separation of the residual anomaly from the regional field is the most simple case of the vertical separation. If the anomaly due to a layer of specific depth can be separated or the depth of the separated layer can be quantitatively determined, it may deserve the separation-sounding. We suggest a wavelength filter whose cutoff frequency is determined by log-power spectrum analysis, as a separation-sounding filter. We applied this filter both to synthetic and real gravity data acquired at Heunghae area, and compared the results with those of Jacobsen's upward continuation filter. These showed that the proposed separation-sounding filter could be a useful tool for interpretation of the vertical geologic structure by stripping the gravity effects of geologic sources down to the desired depth.

• Korean Journal of Food Science and Technology
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• v.44 no.3
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• pp.263-268
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• 2012

Novobiocin is a coumarin-containing antibiotic, and has a longer half-life in various animals than other veterinary medicines. A simple and rapid high-performance liquid chromatography assay for the determination of residual novobiocin levels in chicken, beef and milk has been developed and validated. The separation condition for HPLC/UVD was optimized by a MG II $C_{18}$ (4.6 mm $ID{\times}250$ mm, 5 ${\mu}m$) column with 0.1% formic acid in $H_2O$/0.1% formic acid in Acetonitrile (40/60, v/v) as the mobile phase at a flow rate of 1.0 mL/min and the detection wavelength was set at 340 nm. Residues were extracted from tissue by blending with methanol. After liquid-liquid partitioning, lipid materials were removed with n-hexane and purification as Silica (1 g, 6 mL) cartridge with 10 mL acetone/dichloromethane (10/90, v/v). Limit of quantification and linearity performed by the analytical method were 0.02 mg/kg and 0.999 ($r^2$), and the recovery range was $88.8{\pm}5.6-100.3{\pm}4.4$, $88.8{\pm}7.2-97.0{\pm}3.2$ and $88.1{\pm}4.3-92.8{\pm}3.6%$. It is expected that this analytical method with regards to novobiocin in chicken, beef and milk could be applied as an official method to administer food safety on veterinary medicines.