• 제목/요약/키워드: reference material

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공동주택 자재표준화를 위한 조립기준면 설계기준에 관한 연구 (A Study on the Design Guideline based Reference Plane for Standardization in Material of the Multi-family housing)

  • 박근수;임석호;지장훈
    • 한국주거학회:학술대회논문집
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    • 한국주거학회 2008년도 춘계학술발표대회 논문집
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    • pp.241-244
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    • 2008
  • This study focused on the checking of design guideline using concept of reference plane as a promoting tool in order to apply to practical affair in relation to material standardization in housing build. For this purpose, we above all defined the role of reference plane. After establishing structural type can correspond to planning module of building components and coordination condition, we did exemplicated the sub-detail of building components which be to detach according to design method using the concept of reference plane that be complexed with spacial territory and replace cycle of building component or material.

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항공기조종사 자격증명취득 표준교재 제공에 관한 고찰 (A Investigation the Aircraft Pilots Licence Acquisition Standard Reference Material Providing)

  • 박원태
    • 한국항행학회논문지
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    • 제20권6호
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    • pp.580-587
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    • 2016
  • 본 논문에서는 항공기조종사 자격증명 취득을 위한 표준교재 제공의 필요성과 제공 방법에 관한 제안을 목적으로 미국 FAA와 한국 공군 사례 분석과 항공기조종사 자격증명을 취득한 조종사 및 예비조종사 178명의 자료를 실증 분석하였다. 사례분석 결과 국내의 경우 표준교재 제공에 제한을 두고 있는 실정과는 달리 미 FAA와 한국공군의 경우 표준교재를 제공하고 있는 것으로 나타났다. 또한 실증분석결과 항공조종사 자격증명 취득을 위해 표준교재 제공의 필요성을 인식하고 있었으며, 그 중요도 또한 매우 높은 것으로 나타났다. 이와 같은 결과는 역량 있는 항공기조종사 육성을 위해서는 표준교재의 제공이 필요하며, 이는 항공운송산업의 급속한 성장에 의한 항공기조종사 부족상황을 완화시키고, 다양한 항공기 관련 사고를 예방하는데 있어 매우 중요하다는 것을 보여주는 결과이다.

토마토 농약다성분분석 정도관리용 분석표준물질 개발 (Development of Analytical Reference Material for Proficiency Test of Pesticide Multi-residue Analysis in Tomato)

  • 김종환;오영곤;최성길;홍수명;김선배;우인덕;김준영;서종수
    • 한국환경농학회지
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    • 제35권3호
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    • pp.223-233
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    • 2016
  • BACKGROUND: This study was to develop a analytical reference material including twenty pesticides in tomato. To use it for proficiency test, the suitability of homogeneity, storage stability, assigned values and uncertainty for analytical reference material were important.METHODS AND RESULTS: In order to develop a analytical reference material of tomato for multi-residue analysis of pesticides, twenty-pesticides were treated in tomato and the samples were frozen and homogenized. The homogeneity, stability, assigned value and uncertainty were calculated according to the requirements of the KS A ISO Guide 35, KS Q ISO 13528 and EURL-PT protocol. The values of the within-bottle standard variation(swb) and the between-bottle standard variation(sbb) were 0.9~6.5% of assigned value and the uncertainty(u*bb) due to inhomogeneity was also calculated as 0.6~1.9% for all pesticides. This indicated that it was satisfactory to be used as a analytical reference material. The storage stabilities of twenty-pesticides at room temperature and freezing conditions were assessed according to the requirement of the KS Q ISO Guide 35. All pesticides were stable at room temperature (20~30℃) for 8 days and freezing (-20℃) for 23 days.CONCLUSION: The feasibility of analytical reference material for pesticide multi-residue analysis in a tomato matrix was investigated. Homogeneity of within/between-bottle, uncertainty and stabilities at room temperature and freezing condition were satisfactory for a use of proficiency test and quality control. From these results, a analytical reference material would be applicable to monitor the proficiency test of pesticide analysis organizations to improve the reliability and consistency.

인증표준물질(CRM)을 이용한 방사면역측정법의 회수율 평가 (The Evaluation of Recovery Rate of Radioimmunoassay Using Certified Reference Material (CRM))

  • 최성희;신선영;임소희;홍미경;노경운;김진의
    • 핵의학기술
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    • 제18권1호
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    • pp.158-162
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    • 2014
  • 공인된 기구에 의해 발급된 문서를 동반하는 인증표준물질은 특성값과 추정값의 신뢰정도를 나타내는 연계 불확도, 그리고 측정한 결과가 명시된 불확정 정도의 범위 내에서 국가 측정 또는 국제측정표준에 일치되도록 연속적으로 비교하고 교정하는 소급성을 제공하는 표준물질이다. 회수율 검사는 검체를 측정하여 얻은 값이 참값에서 얼마만큼 벗어났는지의 차이를 말하며 키트의 정확도를 반영한다. 이러한 인증표준물질을 가지고 회수율 검사를 하는 것은 체외 방사면역진단키트의 정확성을 보여주며 이러한 평가는 매우 중요하다. 인증표준물질은 NIBSC (National Institute for biological standard and control, United Kingdom)와 IRMM (Institute for Reference Materials and Measurements, Belgium)에서 구입하였고 검사 종목은 T4, Ferritin, PSA, Prolactin, AFP 그리고 TSH으로 총 6종목이다. T4는 IRMM의 표준물질을 사용하였고 나머지 종목은 NIBSC의 표준물질을 사용하였다. C-1 (저농도), C-2 (중농도), C-3 (고농도) 3 level로 제조하여 본원에서 사용하는 키트를 이용하여 4회 측정하였다. WHO 인증표준물질을 이용한 회수율 측정에서 T4 90%, Ferritin 88%, PSA 94%, Prolactin 99%, AFP 94%, TSH 93%였다. 6개 종목의 회수율 측정에서 88-99%로 양호한 결과를 보였다. 핵의학 체외진단키트의 정확성을 높이기 위해서 이 연구가 다른 검사실의 키트로 확장되어 검사가 되어야 하고 검사실간에도 교류가 필요하다. 인증표준물질을 이용한 체외진단키트의 회수율 평가가 앞으로도 지속되어야 하며 결과의 정확성은 환자의 만족의 증가로 이어질 것으로 기대한다.

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Development of a Nutritional Supplement Certified Reference Material for Elemental Analysis

  • Lee, Jong Wha;Heo, Sung Woo;Kim, Hwijin;Lim, Youngran;Lee, Kyoung-Seok;Yim, Yong-Hyeon
    • Mass Spectrometry Letters
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    • 제9권4호
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    • pp.105-109
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    • 2018
  • A certified reference material (CRM) for the analysis of inorganic nutrients in nutritional supplements has been developed. Accurate mass fractions of chromium (Cr), iron (Fe), copper (Cu), and zinc (Zn) were determined by isotope dilution inductively coupled plasma mass spectrometry (ID ICP/MS). The measurement results were used to assign certified values for the CRM, which were metrologically traceable to the definitions of the measurement units in the International System of Units (SI). Production of a candidate reference material (RM) and the certification processes are summarized. Each nutrient in the CRM showed good homogeneity, which was estimated using relative standard deviations of the measurement results of twelve bottles in a batch. This CRM is expected to be an important reference to improve reliability and comparability of nutrient analyses in nutritional supplements and related samples in analytical laboratories.

표준물질의 인증 및 사용 (Certification and Use of Reference Materials)

  • 최성운
    • 대한안전경영과학회:학술대회논문집
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    • 대한안전경영과학회 2007년도 춘계학술대회
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    • pp.323-333
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    • 2007
  • This paper presents contents of certificates, and use for reference materials. This study also introduces general requirements for the competence of reference material producers. Lastly this paper shows general and statistical principles for certification of reference materials.

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Preparation and Characterization of a Surface Renewable Solid State Hg/HgO Reference Electrode Utilizing Gold Amalgam

  • Kim, Won;Park, Jong-Man
    • Bulletin of the Korean Chemical Society
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    • 제28권3호
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    • pp.439-442
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    • 2007
  • A solid state Hg(Au)/HgO reference electrode was prepared utilizing gold amalgam solid particles. Solid fine powder of the gold amalgam was prepared by chemical reduction of Au(III) with NaBH4 followed by reduction of Hg(II) in the presence of gold fine particles. The solid content in the suspension of the gold amalgam particles and fine mercury oxide particles in DMF containing PVC was precipitated by the addition of a large amount of water to give solid Hg(Au)/HgO/PVC mixture. After drying, the mixture was pressure-molded to a physically stable Hg(Au)/HgO composite reference electrode material. The electrochemical characteristics of the electrode as a reference electrode were very similar to an ordinary Hg/HgO reference electrode. The electrode material can be molded and fabricated in any desired shape and size. The surface can be renewed by a simple polishing process whenever contaminated or deactivated. The applicability of the electrode in the electrochemical detection of carbohydrates after anion exchange separation was evaluated.

PARAMETER IDENTIFICATION FOR NONLINEAR VISCOELASTIC ROD USING MINIMAL DATA

  • Kim, Shi-Nuk
    • Journal of applied mathematics & informatics
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    • 제23권1_2호
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    • pp.461-470
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    • 2007
  • Parameter identification is studied in viscoelastic rods by solving an inverse problem numerically. The material properties of the rod, which appear in the constitutive relations, are recovered by optimizing an objective function constructed from reference strain data. The resulting inverse algorithm consists of an optimization algorithm coupled with a corresponding direct algorithm that computes the strain fields given a set of material properties. Numerical results are presented for two model inverse problems; (i)the effect of noise in the reference strain fields (ii) the effect of minimal reference data in space and/or time data.