• 제목/요약/키워드: purity test

검색결과 192건 처리시간 0.026초

L형(型) 주물응고(鑄物凝固)에 대한 Computer Simulation (Computer Simulation of Solidification in L-Sections)

  • 한윤희;김명한;김동옥
    • 한국주조공학회지
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    • 제5권2호
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    • pp.125-136
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    • 1985
  • The most desirable method for the solution of solidification problems in castings must be the one which combines accuracy, simplicity, and low computer usage cost. The purpose of the present study is to develop a method which includes all these advantages. The purpose of the present research was approached by the introduction of two methods: (1) A pour-out test, employed with very high purity aluminum, for the purpose of obtaining accurate solidification data in L-sections; and (2) an numerical technique, using the cubic spline function for defining solidification curves.

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저순도 Al지금을 사용한 Al-Zn-In-Mg계 Al합금 유전양극의 특성에 관한 연구 (A study of galvanic characteristics of aluminium alloy anode in the Al-Zn-In-Mg system made of the low purity aluminium ingot)

  • 김원녕;김기준;김영대
    • Journal of Advanced Marine Engineering and Technology
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    • 제9권3호
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    • pp.240-249
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    • 1985
  • This paper presents the results of the galvanic anode's characteristicsin the Al-Zn-In-Mg and Al-Zn-In-Mg system anodes used aluminium ingot of low purity, 99.5% grade. The results of thses performance tests are as follows: 1) Zn, In and Mg are an available elements to improve the performance of Aluminium alloy anodes. 2) When the range of zinc content in the Al-Zn-In-Mg system anode is 2-5% the more zinc content, the more improve the anode performance. 3) Al-Zn-In-Mg system anode requires a long term over 50 days for the performance test. 4) The composition of Al-Zn-In-Mg system anode which shows the most excellent performance is Al-(2-3%) Zn-(0.02%) In-(1.0%) Mg. 5) When the Al-Zn-In-Mg system anode is annealed for an hour in 500 to 550 .deg. C, the anode performance is improved. 6) The lower average potential and the better corrosion pattern in the Al-Zn-Mg, Al-Zn-In and Al-Zn-In-Mg system anodes, the more current efficiency is improved.

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폐 신티그래피용 $^{99m}TC$ 표지 미소구형인 혈청 알부민의 제조에 관한 연구 (Studies on the Preparation of $^{99m}TC$ Labelled Human Albumin Microsphere for Lung Scintigraphy)

  • 박경배;오옥두;김재록
    • 대한핵의학회지
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    • 제23권1호
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    • pp.63-69
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    • 1989
  • In order to develop technetium-99m-labelled human albumin microsphere (HAM) for lung scintigraphy, various experimemts such as preparation and fractionation of HAM, establishment of optimal labelling conditions, determination of radiochemical purity, stability test and biodistribution of $^{99m}Tc-HAM$ were carried out. HAM was prepared from the suspension of 1ml aqueous human serum albumin (25%) in 130 ml of olive oil at $130\sim135^{\circ}$ with vigorous stirring. The resulting HAM was fractionated with microsieve to get the desired particle size $(15\sim50\mu)$ and autoclaved for sterilizaiton. The HAM particles were treated with stannous chloride and the pH of the suspension was adjusted to $3.0\sim3.5$ with phosphate buffer. After freeze-drying the contents of single reaction vial containing 5 mg of HAM and 0.2 mg of $SnCl_2$ it was reacted with $Na^{99m}TcO_4$. The labelling yield was higher than 99.5% and the stability of $^{99m}Tc-HAM$ was high enough to maintain 99.1% of radiochemical purity up to 24 hours. Lung and liver uptake in mice was found to be 94% and 0.9%, respectively. Excellent rabbit and human lung scans were also obtained.

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복합재료 평면 안테나 구조의 제작 및 기계적 특성 평가 (Design of Microstrip Antenna with Composite Laminates and its structural rigidity)

  • 전지훈;유치상;김차겸;황운봉;박현철;박위상
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2002년도 춘계학술발표대회 논문집
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    • pp.195-198
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    • 2002
  • Two types of conformal load-bearing antenna structure (CLAS) were designed with microwave composite laminates and Nomex honeycomb cores, to give both structural rigidity and good electrical performance. One is 4$\times$8 array for Synthetic Aperture Radar(SAR) system and the other is $5\times2$ array for wireless LAN system. Design was based on wide bandwidth, high polarization purity, low loss and good structural rigidity. We studied the design, fabrication and structural/electrical performances of the antenna structures. The flexural behavior was observed under a 3-point bending test, an impact test, and a buckling test. Electrical measurements were in good agreement with simulation results and these complex antenna structures have good flexural characteristics. The design of this antenna structure is extended to give a useful guide for sandwich panel manufacturers as well as antenna designers.

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Varestraint Test법에 의한 Al-Li합금의 용접성 평가 (An Evaluation on the Weldability of Al-Li Alloys by Varestraint Testing Method)

  • 김형태;이창배;신현식;서창제
    • Journal of Welding and Joining
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    • 제14권6호
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    • pp.48-57
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    • 1996
  • The weldability of high purity aluminum-lithium binary alloys has been investigated using the Varestraint test. Autogenous GTAW (gas-tungsten-arc-welds) were run along specimens of different lithium concentration using three sets of welding parameters. Welding voltage was held constant at 10 volts. Welding current (70∼100 amps) and travel speed (23∼33 cm/min) were the parameter varied. Hot-tearing susceptibility varied with lithium content and exhibited a steep peak at 2.6 weight percent lithium. Depth of penetration increased with increasing heat input and lithium concentration. The susceptibility is influenced by the wettability of dendrites by the interdendritic eutectic liquid as well as the time available for back-Siting by eutectic liquid. The welding condition of welding current 70A and travel speed 23 cm/min was showed good resistance to cracking in aluminum-lithium alloys. Suggestions for improving weld cracking resistance are also provided.

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Methanol 자화 방선균으로부터 Aminoglycoside 내성 저해물질의 정제 및 특성 (Purification and Characterization of Aminoglycoside-Resistant inhibitior from methylotrophic Actinomycetes)

  • 김현수;신재욱
    • 한국미생물·생명공학회지
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    • 제27권3호
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    • pp.215-222
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    • 1999
  • Methylotrophic actinomycetes No. 155 produced an aminoglycoside antibiotics(AG)-resistant inhibitor. We have previously reported that the inhibitor shows strong inhibition to sisomicin-resistant strain. In order to understand the functions of inhibitor and sisomicin-resistance, characterizations and purification of inhibitor were investigated. Strain No. 155 was tentatively identified as Nocardiopsis sp. based on morphological and some physiological characteristics. In the antimicrobial activity test, the addition of inhibitor to sisomicin showed a reduction effect of MIC on the test strains such as Gram(+), Gram(-) bacteria and yeasts. The combination of the inhibitor and various antibiotics revealed synergistic against E. coli K-12 and B. subtilis PCI 219. The induced intracellular proteins from sisomicin-resistant strain exhibited the sisomicin inactivation by invitro test. And the induced intracellular proteins were inactivated by addition of the inhibitor. The inhibitor compound was purified by anion exchange chromatography(Dowex-1) and HPLC using Asahipak ES-502C column. The purified inhibitor compound was detected in a single peak(above 98.5% purity) through the HPLC analysis.

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수입목초 및 사료작물 종자의 품질에 관한 조사연구 (A Laboratory Test for Determining the Qulity of Imported pasture Plant and Forage Crop Seeds)

  • 조충섭;김동암
    • 한국초지조사료학회지
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    • 제11권2호
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    • pp.68-75
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    • 1991
  • A series of tests was carried out to determine the purity and germination of pasture plant and forage crop seeds imported in 1986 and 1987 at the grassland and forage laboratory, College of Agriculture, Seoul National University, Suweon. At the same time, the results obtained were compared with the National Livestook Cooperatives Federation(NLCF1's seed standards as a guide for determining seed quality. 1. The germination percentages of Potomac orchardgrass, Fawn tall fescue, Aquila Ky bluegrass and California ladino clover among grasses and legumes tested were lower than those of the N1,CF's standards, but the germination percentages of forage crops were higher than those of the NLCF's standards. 2. The purity of Potomac orchardgrass and Aquila Ky bluegrass were relatively lower than those of the NLCF's standards. 3. The percentages of other crop seeds in Potomac orchardgrass, Fawn tall fescue, Aquila Ky bluegrass and Cayuse oats were lower than those of the NLCF's standards. 4. Percentage of inert matter in the seeds was lower compared with the NLCF's standards except Akela ' forage rape. 5. The seeds of Potomac orchardgrass, NK 367 sorghum hybrid and sorghum x sudangrass hybrids such as NC+855, G83F and TE Haygrazer were contaminated with one or more weed seeds. Rumex spp. was by far the most common weed in the seeds imported. The other weeds occurred at a low level were Rumex acestosella, Senecio jacobaea, Cirsium arvense and Cuscicta spp. 6. There were many variations in 1,000 seed weight among different species. A thousand seed weight of Aquila Ky bluegrass was 0.263g, but that of Tetrone Italian ryegrass, Akela forage rape and Pioneer 3160 sorghum x sudangrass hybrid was 3.875, 3.476 and 242.4578, respectively. 7. According to the fluorescence test of ryegrass seed, Tetrone Italian ryegrass was known as a true annual type, but an unknown cultivar produced in Cheju was contaminated with 6% of perennial ryegrass seed.

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재활용 황산니켈의 국내·외 품질기준현황 및 생산제품의 전해도금 성능 비교 (The Status of Domestic and International Quality Standards for Recycled Nickel Sulfate and Comparison of Electroplating Performance Between Reagent and Recycled Products)

  • 박성철;김용환;신호정;이만승;손성호
    • 자원리싸이클링
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    • 제30권3호
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    • pp.55-62
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    • 2021
  • 국내에서는 1997년 우수 재활용제품(good recycled product, GR) 인증 제도를 도입하여 자원과 에너지 사용효율 개선을 증진하고 있으나 산업계 및 사회 전반적으로 재활용 소재에 대한 인식 부족으로 인해 재활용 제품 사용이 잘되지 않고 있다. 따라서 본 연구에서는 니켈 소재의 국내·외 품질 기준 현황을 조사하였고, 광석으로부터 제조된 황산니켈과 폐리튬이온전지로부터 재소재화 된 황산니켈에 대하여 전해도금 공정에서의 순도 및 전기화학적 특성을 평가하였다. 평가 결과, 전해도금 산업에서 사용 시 재활용 황산니켈과 고순도 황산니켈 시약의 품질은 차이가 없는 것으로 판단된다.

폐 영구자석으로부터 회수한 염화희토류용액에서 PC88A를 이용한 경희토류(Pr, Nd)/중희토류(Tb, Dy) 용매추출 (Solvent Extraction of Light (Pr, Nd) and Medium (Tb, Dy) Rare Earth Elements with PC88A of Rare Earth Chloride Solution from Waste Permanent Magnet)

  • 전수병;손인준;임병철;김정모;김연진;하태규;윤호성;김철주;정경우
    • 자원리싸이클링
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    • 제27권3호
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    • pp.8-15
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    • 2018
  • Nd-Fe-B 폐 영구자석으로부터 회수한 염화희토류용액을 PC88A에 의한 경희토류(Pr, Nd)/중희토류(Tb, Dy) 분리정제에 대한 용매추출 연구를 진행하였다. 회분식 실험 단계에서 추출제(PC88A) 농도 0.5 M, 추출 후 평형 pH는 0.8~1.0(feed의 초기 pH 1.3), 세정액(HCl)의 농도는 0.1 M, 탈거액(HCl)의 농도는 2 M 이상일 때 분리 효율이 좋은 것을 확인하였다. 이 결과값을 혼합침강조에 적용하여 초기 조건에서 운용 조건을 변화시키면서 180시간 운용하여 3N급의 경희토류(Pr, Nd)/중희토류(Tb, Dy)금속 이온으로 분리정제 후 회수하였다.