• Title/Summary/Keyword: purge

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Coating of $TiO_2$ Thin Films on Glass Substrate using Photo-assisted Atomic Layer Deposition (광원자층증착법에 의한 glass 기판에 $TiO_2$ 박막 코팅)

  • Kim, Hyug-Jong;Kim, Hee-Gyu;Kim, Doe-Hyoung;Kang, In-Gu;Choi, Byung-Ho
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.11a
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    • pp.382-382
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    • 2009
  • 염료감응형 태양전지의 구성체 중 전극으로 연구 되어 지고 있는 $TiO_2$는 기존에 대량 생산이 가능한 spin coating법, screen printing법, spray법의 연구가 이루어져 왔으나 고 효율 태양전지에 쓰이는 전극 시스템에 비해 고 분산성을 지닌 $TiO_2$페이스트를 제조 하는데 어려움이 있다. 그리고 플렉시블 디스플레이 소자의 응용을 위해서는 소자 공정 온도인 $250^{\circ}C$ 이하의 공정 온도가 요구 되어 지므로 고온공정인 CVD법은 이에 적합하지 않다. 이에 본 연구는 진공 증착 방법인 광원자층증착법을 이용하여 $150^{\circ}C$이하의 저온공정온도에서도 적용이 가능한 $TiO_2$ 박막을 185nm의 UV light를 조사하여 glass 기판위에 제조 하고 그에 따른 박막의 물성 분석을 하였다. Mo source로는 titanium tetraisopropoxide(TTIP)와 reactant gas 로는 $H_2O$를 사용하였으며 불활성 기체인 Ar 가스는 purge 가스로 각각 사용하였다. $100^{\circ}C{\sim}250^{\circ}C$ 공정온도를 변수로 $TiO_2$ 박막을 제조 하였으며 제조된 $TiO_2$ 박막의 물성 분석을 위해 FESEM, TEM을 이용하여 표면 및 두께를 분석하였다. 또한 $100^{\circ}C$ 400 cycles에서 약 12nm 막 두께를 관찰 할 수 있었으며 그 결과 박막의 성장률이 $0.3{\AA}$/cycle 임을 확인 할 수 있었다. 그리고 UV-VIS을 이용하여 박막의 좌외선에 대한 흡수도 및 투과도 분석을 하였다. 또한 XPS 성분 분석을 통하여 $100^{\circ}C$의 저온 공정에서 형성된 박막이 $TiO_2$임을 확인 하였다. 이러한 결과에서 185nm의 UV light에 의한 광원자층 증착법으로 $100^{\circ}C$의 저온에서도 $TiO_2$ 박막이 증착 되는 것을 확인 할 수 있었다.

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Formulation of Water-soluble Topical Preparations of Epidermal Growth Factor (상피세포성장인자의 수용성 외용제제화)

  • Lee, Yoo-Cheol;Park, Eun-Seok;Chi, Sang-Cheol
    • Journal of Pharmaceutical Investigation
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    • v.25 no.3
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    • pp.177-184
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    • 1995
  • In order to formulate an aqueous topical preparation of epidermal growth factor(EGF) for the treatment of open wound and bum, the stability of EGF in aqueous vehicles containing various stabilizers was evaluated and the pharmacological activity of gel preparations formulated with poloxamer 407 was determined with wound model. Various additives, which are known as potent stabilizers for proteins and polypeptides so far, were used to increase the stability of EGF in aqueous vehicles. The contents of EGF in the vehicles containing stabilizers were determined with an HPLC method after the storage at $37^{\circ}C$. EGF was more stable in ultrapure water than RO water or saline. All the additives studied resulted in deleterious effects on EGF stability. Therefore, it was speculated that any additives or impurities in the vehicle made EGF unstable. However, nitrogen purge of solution increased the stability of EGF in aqueous vehicles. The aqueous topical preparations of EGF were formulated with poloxamer 407 as a gel base in saline. Gelatin or amastatin was employed as a protease inhibitor. The pharmacological effect of EGF gel was studied with open wound model in mice. EGF preparations, made of oleaginous base or poloxamer gel base, showed significant healing effect compared to the control group(p<0.05). The addition of protease inhibitor in poloxamer 407 gel resulted in significant healing effect compared to the gel without it(p<0.05). Body weights of mice treated with EGF preparation were increased at the first day after the formation of open wound, while those of the control group were decreased. The EGF gel made of poloxamer 407 containing a pretense inhibitor would be a promising aqueous topical preparation for EGF.

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Design of Tritium Handling System(II): Injection System, Regeneration System (삼중수소취급계통의 설계(II): 주입계통, 재생계통)

  • 김광신;김경숙;정은수;손순환;김위수
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2003.11a
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    • pp.117-123
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    • 2003
  • In succession to the previous paper, the tritium injection system and the regeneration system of the tritium handling system are presented. Both systems should be placed inside glove boxes since there can be potential leakage of tritium from these systems. The tritium injection system should be capable of measuring the exact amount of the injected tritium to keep track of the tritium inventory. The tritium injection system is designed to recover the remaining tritium from the system after injection for the minimization of tritum release to the environment as well as for the recovery of precious resource. TRS equipment such as MS, Ni catalyst bed, and metal getter are regenerated with a standalone regeneration system. Unlike other equipments which can be regenerated by heating and purging with appropriate gas, regeneration of the metal getter used to recover tritium is somewhat complicated.

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Economic and Performance Analysis for 2bed and 3bed Oxygen PSA Process (2탑 및 3탑식 Oxygen PSA 장치 운전결과 및 경제성 비교분석)

  • Kim, Kweon-Ill;Kim, Jong-Nam;Cho, Sung-Chul;Cho, Soon-Haeng;Jin, Myung-Jong
    • Applied Chemistry for Engineering
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    • v.7 no.4
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    • pp.653-660
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    • 1996
  • For oxygen PSA process development, adsorbed amount of oxygen and nitrogen on various adsorbents were measured corresponding Langmuir isotherm parameters were measured. A reasonable adsorbent for oxygen process was selected based on the effective adsorbed amount. The PSA process consists of adsorption, desorption, pressurization, purging and pressure equilization steps. Adsorption pressure was about 2 atm and desorption pressure was between 120 torr to 400torr. Cycle time of 2-bed PSA process was 80 seconds and that of 3-bed oxygen PSA process was 180 seconds. In order to compare and analyze operation characteristics and economic feasibilities of 2-bed and 3-bed oxygen PSA processes, productivity, oxygen concentration and recovery were compared and the effect of purge and pressurization steps on the performance of PSA processes were analyzed. For the commercial scale oxygen PSA process, capital and electricity cost were estimated. In the range of $O_2$ production less than $700Nm^3/hr$, the 2-bed process is conformed more feasible in economic view point.

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Influence of Various Catalysts on the Biomass Pyrolysis Reaction (바이오매스 열분해 반응에서 다양한 촉매의 영향)

  • BAK, YOUNG-CHEOL;CHOI, JOO-HONG
    • Transactions of the Korean hydrogen and new energy society
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    • v.28 no.5
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    • pp.536-544
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    • 2017
  • The effects of catalysts addition on the pyrolysis reaction of biomass have been studied in a thermogravimetric analyzer (TGA). The sample biomasses were Bamboo, Pine and Hinoki. The catalysts tested were K, Zn, Cu metal compounds. The pyrolysis reactions were tested in the nonisothermal condition from the room temperature to $550^{\circ}C$ at a heating rate $50^{\circ}C/min$ on the flowing of $N_2$ purge gases. Cellulose contents of Bamboo was higher than that of Pine and Hinoki. As the results, the pyrolysis reaction of volatile matter was finished near the temperature $450^{\circ}C$. The initial decomposition temperatures of the volatile matters ($T_i$) were $165^{\circ}C$ for Bamboo, $190^{\circ}C$ for Pine, and $193^{\circ}C$ for Hinoki. $T_i$ decreased with increasing the catalyst amounts in the sample biomasses. The temperature of maximum reaction rate ($T_{max}$) were $338^{\circ}C$ for Bamboo, $378^{\circ}C$ for Pine, and $377^{\circ}C$ for Hinoki. The effects of catalysts addition on the $T_{max}$ were to decreased it. The reducing effects about $T_{max}$ was the most effective for K metal compounds catalyst. The char amounts remained after pyrolysis at $550^{\circ}C$ were 26.2% for Bamboo, 20.7% for Pine, and 20.9% for Hinoki. The char amounts increased with the catalyst amounts.

Dispersion Polymerization of Acrylamide in the Media of t-Butyl Alcohol/$H_2O$ Mixtures (t-Butyl Alcohol/$H_2O$ 혼합 용매에서 아크릴아미드의 분산중합)

  • 이기창;이성은;송봉근;이동주
    • Polymer(Korea)
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    • v.24 no.5
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    • pp.629-637
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    • 2000
  • Dispersion polymerization of acrylamide in the media of t-butyl alcoho1/$H_2O$ mixtures at 30~5$0^{\circ}C$ in the presence of hydroxypropyl cellulose and ammonium persulfate as steric stabilizer and initiator, respectively, was carried out. It was studied the effects of concentrations of initiator and steric stabilizer, amount of monomer, polymerization temperature, t-butyl alcohol/$H_2O$ ratio, concentration of crosslinker, purification of monomer and nitrogen purge on the particle size of the resulting acrylamide latices and molecular weight of the latex-poly(acrylamide). In this study, poly(acrylamide) latices of 0.1~0.5 ${\mu}{\textrm}{m}$ with 470000~2080000 in (equation omitted) were prepared and the resulting PAM latices were all dissolved in water in stantly.

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Quality Properties of Pork Fed with Glucosamine Derivatives (GD) as Dietary Supplementation (글루코사민 유도체(GD) 급여 돈육의 육질 특성)

  • Park Beom-Young;Cho Soo-Hyun;Hwang In-Ho;Kim Jin-Hyoung;Oh Suk-Jung;Lee Jong-Moon;Yun Sang-Gi
    • Food Science of Animal Resources
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    • v.24 no.3
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    • pp.221-224
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    • 2004
  • The feeding group, composed of weaning pigs fed 3 mL of glucosamine derivatives, was compared for the carcass and quality characteristics with the unfeeding control group for 25∼70 days since they were born. The results were as follows; There were no significant differences in carcass weight and back-fat thickness between the feeding group and the unfeeding group although the feeding group had low ranges of standard error when compared to the control. Feeding group had higher incidence frequencies of A grade (42.7%) than the control (29.2%). The feeding group and unfeeding group had no significant differences in meat color, cooking loss, WBS, pH, WHC and purge loss. Results from this study showed that feeding GD had effect on the decrease the market weight and production of consist carcass weight, however, the feeding GD had no effect on pork quality during rearing times after weaning.

The Analysis of Trihalomethanes in Water Sample by Purge-and-Trap Gas Chromatograph/Mass Spectrometer and Risk Assessment (퍼지-트랩 기체크로마토그래프/질량분석계에 의한 물시료 중 Trihalomethanes의 분석 및 위해성 평가)

  • Kwak Sunyoung;Pyo Heesoo;Park Song-Ja
    • Environmental Analysis Health and Toxicology
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    • v.20 no.1
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    • pp.29-37
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    • 2005
  • Recently, significant contamination problems by residual chemicals have occasionally been occurred from major rivers and drinking water in Korea. Therefore, the management for use of them and risk assessment should be more strictly performed. In this study, we have analyzed trihalomethanes in treated water samples taken from water plants located in the region of four major rivers (i.e. Han river, Geum river, Youngsan river and Nakdong river) in Korea for eight years (1997~2004). From the data, we could assess the excess cancer risk by calculating the chronic daily intakes (CDI) multiplied by individual oral slope factors, Q₁*, for the cancer suspected matters such as trihalomethanes, moreover the hazard index which is calculated by dividing the CDI by the acceptable daily reference dose (R/sub f/D) was determined for the risk assessment. As a result, in the case of 95 percentile excess cancer risk, it was shown that the excess cancer risk for dichlorobromomethane in the Nakdong river region is highest among the tested samples as 8.73 x 10/sup -6/. The 95 percentile total hazard index (the sum of individual hazard indices considering R/sub f/D), in addition, was below 1.0 for all samples, and therefore it was assessed that water samples taken from treatment plants of four major rivers are not harmful.

Power System Development of Unmanned Aerial Vehicle using Proton Exchange Membrane Fuel Cell (고분자 전해질 연료전지를 이용한 무인비행체 동력시스템 설계)

  • Jee, Yeong-Kwang;Sohn, Young-Jun;Park, Gu-Gon;Kim, Chang-Soo;Choi, Yu-Song;Cho, Sung-Baek
    • Transactions of the Korean hydrogen and new energy society
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    • v.23 no.3
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    • pp.250-255
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    • 2012
  • In this paper, the development and performance analysis of a fuel cell-powered unmanned aerial vehicle is described. A fuel cell system featuring 1 kW proton exchange membrane fuel cell combined with a highly pressurized fuel supply system is proposed. For the higher fuel consumption efficiency and simplification of overall system, dead-end type operation is chosen and each individual system such as purge system, fuel supply system, cooling system is developed. Considering that fluctuation of exterior load makes it hard to stabilize fuel cell performance, the power management system is designed using a fuel cell and lithium-ion battery hybrid system. After integration of individual system, the performance of unmanned aerial vehicle is analyzed using data from flight and laboratory test. In the result, overall system was properly operated but for more duration of flight, research on weight lighting and improvement of fuel efficiency is needed to be progressed.

Browser fuzzing and analysis using known vulnerability (소프트웨어 취약점의 종류와 탐색 방법)

  • Kim, Nam-gue;Kim, Hyun Ho;Lee, Hoon-Jae
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2015.10a
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    • pp.753-756
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    • 2015
  • Internet technology is universal, news from the Web browser, shopping, search, etc., various activities have been carried out. Its size becomes large, increasing the scale of information security incidents, as damage to this increases the safety for the use of the Internet is emphasized. IE browser is ASLR, such as Isolated Heap, but has been continually patch a number of vulnerabilities, such as various protection measures, this vulnerability, have come up constantly. And, therefore, in order to prevent security incidents, it is necessary to be removed to find before that is used to exploit this vulnerability. Therefore, in this paper, we introduce the purge is a technique that is used in the discovery of the vulnerability, we describe the automation technology related thereto. And utilizing the known vulnerabilities, and try to show any of the typical procedures for the analysis of the vulnerability.

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