• Title/Summary/Keyword: prisms

Search Result 129, Processing Time 0.024 seconds

Crystal Structure of Nitrogen Adsorption of $Cd^{2+}$ ion Exchanged Zeolite-X (카드늄으로 이온교환된 제올라이트 X의 질소 흡착 결정구조)

  • Lee, Seok-Hee;Jeong, Gyoung-Hwa;Kim, Nam-Seok
    • Journal of the Korean Applied Science and Technology
    • /
    • v.22 no.3
    • /
    • pp.204-211
    • /
    • 2005
  • The structure of nitrogen adsorption complex of fully dehydrated $Cd^{2+}$ ion exchanged zeolite-X, $|Cd_{46}(N)_{18}|[Si_{100}Al_{92}O_{384}]$, was determined in the cubic space group $Fd\overline{3}$ at 21(1) $^{\circ}C$ [a = 24.863(4) ] by single crystal X-ray diffraction analysis. The crystal was prepared by ion exchange in a flowing steam of 0.05 M aqueous solution $Cd(NO_3)_2$ : $Cd(O_2CCH_3)_2$ = 1:1 for five days, followed by dehydration at $500^{\circ}C$ and $2{\times}10^{-6}$ Tor. for two days, and exposured to 100 Tor. zeolitically dry nitrogen gas at 21(1) $^{\circ}C$. The structure was determined in atmosphere, and was refined within $F_0$ > $4{\sigma}(F_0)$ using reflection for which the final error can appear in indices $R_1$ = 0.097 and $wR_2$ = 0.150. In this structure, $Cd^{2+}$ ions occupied four crystallographic sites. Nine $Cd^{2+}$ ions filled the octahedral site I at the centers of hexagonal prisms (Cd-O = 2.452(16) ${\AA}$). Eight $Cd^{2+}$ ions filled site I' (Cd-O = 2.324(19) ${\AA}$). The remaining 29 $Cd^{2+}$ ions are found at two nonequivalent sites II (in the supercages) with occupancy of 11 and 18 ions. Each of these $Cd^{2+}$ ions coordinated to three framework oxygens, either at 2.159(15) or 2.147(14) ${\AA}$, respectively. Eighteen nitrogen molecules were adsorbed per unit cell and three per supercage.

Characteristics of Fluid Force Reduction of a Square Prism With a Small Triangular Prism (작은 삼각주에 의한 정방형주의 유체력 저감특성)

  • Ro, Ki-Deok
    • Journal of Advanced Marine Engineering and Technology
    • /
    • v.39 no.3
    • /
    • pp.243-247
    • /
    • 2015
  • The characteristics of the fluid force reduction of a square prism having a small triangular prism at the upstream side was investigated by measuring of lift and drag on the square prism The experimental parameters were the width ratios (H/B=0.2~0.6) of triangular prisms to the prism width and the gap ratios (G/B=0~3) between the square prism and the triangular prism. The drag reduction rate of the square prism was increased and then decreased with G/B in case of the same H/B, and was increased with H/B in case of the same G/B. The maximum drag reduction rate was represented by 78.5% at H/B=0.6 and G/B=1.5. The lift reduction rate of the square prism was hardly not affected by the width and gaps ratios, the average value was about 52.4%.

Holographic recording system by combined use of rotational, angular, and spatial multiplexing method (회전, 각, 그리고 공간 다중화 방법을 결합사용한 홀로그램 기록 시스템)

  • 신동학;장주석
    • Korean Journal of Optics and Photonics
    • /
    • v.9 no.3
    • /
    • pp.199-204
    • /
    • 1998
  • To increase the storage density in hologram recording, a simple scheme to obtain rotational, angular and spatial multiplexing efficiently at the same time is proposed and experimented. Both rotational multiplexing and angular multiplexing are obtained by controlling the reference beam directly by use of a pair of wedge prisms, while spatial multiplexing is obtained by shifting the recording medium in the recording plane. It is possible to get both an acute-angle geometry, in which the angle between the signal and reference beams is less than 90$^{\circ}$, and a 90$^{\circ}$ geometry, in which the angle is approximately 90$^{\circ}$. In experiment, 180 holograms were multiplexed with an acute-angle geometry where a photopolymer was used for the recording medium, and 147 holograms with 90$^{\circ}$ geometry where a Fe-doped LiNbO$_3$ crystal was used. The proposed scheme makes it easy it easy to realize a practical holographic memory system by simplifying the control of three complex mechanical motions that are necessary for the three multiplexing techniques.

  • PDF

Reinforced fibrous recycled aggregate concrete element subjected to uniaxial tensile loading

  • Hameed, R.;Hasnain, K.;Riaz, M. Rizwan;Khan, Qasim S.;Siddiqi, Zahid A.
    • Advances in concrete construction
    • /
    • v.9 no.2
    • /
    • pp.195-205
    • /
    • 2020
  • In this study, effect of recycled aggregates and polypropylene fibers on the response of conventionally reinforced concrete element subjected to tensile loading in terms of tension stiffening and strain development was experimentally investigated. For this purpose, concrete prisms of 100 × 100 mm cross section and 500 mm length having one central deformed steel re-bar were cast using fibrous and non-fibrous Recycled Aggregate Concrete (RAC) with varying percentages of recycled aggregates (0%, 25%, 50%, 75% and 100%) and tested under uniaxial tensile load. For all fibrous RAC mixes, polypropylene fibers were used at constant dosage of 3.15 kg/㎥. Effect of recycled aggregates and fibers on the compressive strength of concrete was also explored in this study. Through studying tensile load versus global axial deformation of composite and strain development in concrete and steel, it was found that replacement of natural aggregates with recycled aggregates in concrete negatively affected the cracking load, tension stiffening and strain development, and this negative effect was observed to be increased with increasing contents of recycled aggregates in concrete. The results of this study showed that it was possible to minimize the negative effect of recycled aggregates in concrete by the addition of polypropylene fibers. Reinforced concrete element constructed using concrete containing 50% recycled aggregates and polypropylene fibers exhibited cracking behavior, tension stiffening and strain development response almost similar to that of concrete element constructed using natural aggregate concrete without fiber.

A Disposable Grating-Integrated Multi-channel SPR Sensor Chip for Detection of Biomolecule (회절격자가 집적된 일회용 다중채널 SPR 생체분자 검출 칩)

  • Jin, Young-Hyun;Cho, Young-Ho
    • The Transactions of The Korean Institute of Electrical Engineers
    • /
    • v.58 no.1
    • /
    • pp.147-154
    • /
    • 2009
  • This paper presents a grating~integrated SPR (Surface Plasmon Resonance) sensor chip for simple and inexpensive biomolecule detection. The grating-integrated SPR sensor chip has two sensing channels having a nano grating for SPR coupling. An external mirror is used for multi channel SPR sensing. The present sensor chip replaces bulky and expensive optical components, such as fiber-optic switches or special shaped prisms, resulting in a simple and inexpensive wavelength modulated multi-channel SPR sensing system. We fabricate a SPR sensor chip integrated with 835 nm-pitch gratings by a micromolding technique to reduce the fabrication cost. In the experimental characterization, the refractive index sensitivity of each sensing channel is measured as $321.8{\pm}8.1nm$/RI and $514.3{\pm}8.lnm$/RI, respectively. 0.5uM of the target biomolecule (streptavidin) was detected by a $1.13{\pm}0.16nm$ shift of the SPR dip in the 10%-biotinylated sample channel, while the SPR dip in the reference channel for environmental perturbation monitoring remained at the same position. From the experimental results, multi-channel biomolecule detection capability of the present grating-integrated SPR sensor chip has been verified. On the basis of the preliminary experiments, we successfully measured the binding reaction rate for the $2\;nM{\sim}200\;nM$ monoclonal-antibiotin, thus verifying biomolecule concentration detectability of the present SPR sensor chip. The binding reaction rates measured from the present SPR sensor chip agredd well with those from a commercialized SPR sensor.

Chemistry and Cathodoluminescence Properties of the Carbonate Minerals From the Tertiary Marine Sediments, SE Korea (제3기 해성퇴적층에서 산출되는 탄산염광물의 화학적 및 음극선 발광 특성)

  • Son, Byeong-Kook;Kim, Hyun-Tae
    • Journal of the Mineralogical Society of Korea
    • /
    • v.17 no.2
    • /
    • pp.123-133
    • /
    • 2004
  • Carbonate minerals are examined by cathodoluminescence microscopy and chemical analysis to characterize the carbonate materials occurring in the Tertiary marine basin. The microscopic technique with cathodoluminescence gives new informations that are not obtainable by conventional microscopic techniques. The carbonate cements in sandstones appear to be uniform with transmitted light or with crossed prisms. but the inspection with cathololuminescence reveals foraminiferal tests and rhomb crystals in the carbonate cements. The chemical analysis indicates that the intense luminescence depends mainly on the presence of$ Mn^{ 2+}$ and $Fe^{2+}$ as activator ions, but the $Fe^{2+}$ also acts as an important quencher ion when Fe concentration in dolomite is over 10,000 ppm. The dolomites, which are rich in calcium, are formed at the early stage of diagenesis at a temperature of about 60 ~ $70^{\circ}C$.

Development of medium resolution cross-dispersed silicon grisms in the Near Infrared ; Direct Silicon wafer bonding technique

  • Jeong, Hyeon-Ju;Wang, Wei-Song;Gully-Santiago, Michael;Deen, Casey;Pak, Soo-Jong;Jaffe, Daniel T.
    • The Bulletin of The Korean Astronomical Society
    • /
    • v.36 no.2
    • /
    • pp.125.2-125.2
    • /
    • 2011
  • We are developing medium resolution cross-dispersed silicon grisms in the near IR region ($1.45{\sim}5.2{\mu}m$). The grisms will be installed in MIMIR, a multifunction instrument at the Lowel Observatory, USA. The two devices are designed to cover H and K band and L and M band simultaneously. Our goal is to make grism with R=3000 at 1.2 arcsec slit. The Silicon has high refractive index (n=3.4 at $1.5{\mu}m$) which enhances the resolving power by up to 5 times when compared to conventional material such as BK-7 (n=1.5 at 1.5 ${\mu}m$). The bonded grisms will be installed in a filter wheel for the uses switch from spectroscopic mode to imaging mode easily. Our device is compact and light weighted while it provides a decent resolving power. We produce monolithic grisms using e-beam lithography at the NASA JPL and chemically etching the grooves on the silicon prisms. Moreover, the main-disperser and cross-disperser will be contacted together by direct Si-Si bonding technique and eventually turn into one piece. The bonded pair offers more stability in terms of the layout of the spectrum and removes the Fresnel loss at the intersection of two grisms. We report on the proper wafer bonding steps through this research, and inspected the bonding quality thermally, optically and mechanically.

  • PDF

Inverse model for pullout determination of steel fibers

  • Kozar, Ivica;Malic, Neira Toric;Rukavina, Tea
    • Coupled systems mechanics
    • /
    • v.7 no.2
    • /
    • pp.197-209
    • /
    • 2018
  • Fiber-reinforced concrete (FRC) is a material with increasing application in civil engineering. Here it is assumed that the material consists of a great number of rather small fibers embedded into the concrete matrix. It would be advantageous to predict the mechanical properties of FRC using nondestructive testing; unfortunately, many testing methods for concrete are not applicable to FRC. In addition, design methods for FRC are either inaccurate or complicated. In three-point bending tests of FRC prisms, it has been observed that fiber reinforcement does not break but simply pulls out during specimen failure. Following that observation, this work is based on an assumption that the main components of a simple and rather accurate FRC model are mechanical properties of the concrete matrix and fiber pullout force. Properties of the concrete matrix could be determined from measurements on samples taken during concrete production, and fiber pullout force could be measured on samples with individual fibers embedded into concrete. However, there is no clear relationship between measurements on individual samples of concrete matrix with a single fiber and properties of the produced FRC. This work presents an inverse model for FRC that establishes a relation between parameters measured on individual material samples and properties of a structure made of the composite material. However, a deterministic relationship is clearly not possible since only a single beam specimen of 60 cm could easily contain over 100000 fibers. Our inverse model assumes that the probability density function of individual fiber properties is known, and that the global sample load-displacement curve is obtained from the experiment. Thus, each fiber is stochastically characterized and accordingly parameterized. A relationship between fiber parameters and global load-displacement response, the so-called forward model, is established. From the forward model, based on Levenberg-Marquardt procedure, the inverse model is formulated and successfully applied.

Optical System Design for Projection TV using Micro Display (마이크로 디스플레이를 이용한 프로젝션 TV용 광학계 설계)

  • Park, Sung-Chan;Lee, Jung-Yul
    • Korean Journal of Optics and Photonics
    • /
    • v.17 no.3
    • /
    • pp.240-247
    • /
    • 2006
  • This paper discusses the optical system design for projection TV using LCOS type micro display, which provides the high resolution, slim depth, and a large screen of more than 60 inches. We analyzed the relationship between the illumination system, projection lens, color separation & recombination system, and micro display. From this quantitative analysis, the starting data for the optimum light engine was defined, and all optical systems were designed by an optimization process. Three RGB panels were proposed for a high luminence system, and the four prisms symmetrically located make equal optical path lengths for the RGB rays. This color separation & recombination system enables the a compact illumination system. Also, in order to the slim light engine with high resolution, the folded projection lens system was designed by inserting a mirror between projection lenses.

Comparisons of Phoria Test Among Prism Settings of Von Graefe Technique (Von Graefe법의 프리즘 세팅에 따른 사위검사의 비교)

  • Yu, Dong-Sik;Ha, Eun-Mi
    • Journal of Korean Ophthalmic Optics Society
    • /
    • v.20 no.2
    • /
    • pp.211-218
    • /
    • 2015
  • Purpose: The aim of this study was to compare the differences among prism settings of the von Graefe technique for phoria measurement. Methods: Thirty eight healthy subjects (mean age $22.35{\pm}2.72years$) were tested with eye examination by interview, cover test, and refraction. Phorias were measured in a random order using four prism settings for the von Graefe method: base-in (BI) and base-up (BU), BI and base-down (BD), BU and BI, and BD and BI over the right and left eye, respectively. Results: Among the four prism settings in measurements of lateral and vertical phoria, there were not significant differences at distance, whereas there were significant at near. The reliability of near lateral phoria (ICC: 0.95) was good, but that of near vertical phoria was less reliable (ICC: 0.83). In comparisons of the paired t-test, the 95% limits of agreement, and mean difference between prism settings, BU had more useful than other prism settings at near phoria. Conclusions: Results from this study suggest that the von Graefe test with BU or BU including other setting prisms have useful methods, especially for near phoria measurements.