• Title/Summary/Keyword: pretreatments

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Effect of scutellariae radix pharmacopuncture on the type 1 hypersensitivity (황금약침(黃芩藥鍼)이 Type 1 Hypersensitivity에 미치는 영향)

  • Kim, Yu-Seung;Song, Choon-Ho
    • Korean Journal of Acupuncture
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    • v.23 no.3
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    • pp.111-122
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    • 2006
  • Objectives : We studied the effects of Scutellariae Radix pharmacopuncture solution (SRHAS) on the type 1 hypersensitivity. Methods : In vivo, we measured compound 48/80-induced active systemic anaphylactic shock using ICR mice and anti-DNP IgE-induced passive cutaneous anaphylaxis (PCA) using Sprague Dawley rats. In vitro, we showed effects on cytotoxicity and ${\beta}-hexosaminidase$ release from RBL-2H3 cells. Results : In vivo, SRHAS pretreatments (100% or 50%) at BL13 inhibited active systemic anaphylactic shock induced by compound 48/80. PCA was only inhibited by pretreatments of SRHAS at optional points. In vitro, $0.1{\sim}2%$ SRHAS treatments did not affect cell viability while ${\beta}$-hexosaminidase release was significantly inhibited. Conclusions : These results suggest that SRHAS may be beneficial in the inhibition of type I hypersensitive inflammatory response.

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Physical Properties and Dyeing Behaviors of Cotton Fabric Treated with Low Temperature Plasma and/or Cellulase (저온플라즈마 및 효소처리한 면의 물성 및 염색성)

  • Yoon, Nam Sik;Lim, Yong Jin
    • Textile Coloration and Finishing
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    • v.8 no.3
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    • pp.59-65
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    • 1996
  • Cotton fabrics were treated by low temperature plasma and/or cellulase, and its physical and dyeing properties were investigated. All the pretreatments of the cotton with low temperature plasma of oxygen, nitrogen and argon slowed down the rate of weight loss of cotton in cellulase solution. Plasma pretreatment did not show any strength retention effect on cotton fiber in the subsequent cellulase treatment. Pretreatment of cotton with low temperature oxygen plasma decreased the rate of dyeing in direct dye bath, while cellulase or plasma/cellulase pretreatment increased the rate. Equilibrium dye uptake of cotton was not changed greatly by the pretreatments except the normal untreated cotton showed more or less high uptake. The pretreatment of cellulase with a water-soluble carbodiimide reduced the enzymatic activity, and did not show any strength retention of cotton in enzymatic weight loss.

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Effects of Pretreatments of PET Substrate on the Adhesion of Copper Films Prepared by a Room Temperature ECR-MOCVD Method (PET 기질의 전처리효과가 상온 ECR 화학증착법에 의해 증착된 구리박막의 계면접착력에 미치는 영향)

  • Hyun Jin;Jeon Bupju;Byun Dongjin;Lee Joongkee
    • Korean Journal of Materials Research
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    • v.14 no.3
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    • pp.203-210
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    • 2004
  • Effects of various pretreatments on the adhesion of copper-coated polymer films were investigated. Copper-coated polymer films were prepared by an electron cyclotron resonance-metal organic chemical vapor deposition (ECR-MOCVD) coupled with a DC bias system at room temperature. PET(polyethylene terephthalate) film was employed as a substrate material and it was pretreated by industrially feasible methods such as chromic acid, sand-blasting, oxygen plasma and ion-implantation treatment. Surface characterization of the copper-coated polymer film was carried out by AFM(Atomic Force Microscopy) and FESEM(Field Emission Scanning Electron Microscopy). Surface energy was calculated by based on the value of the contact angle measured. The adhesion of copper/PET films was determined by a pull-off test according to ASTM D-5179. It was found that suitable pretreatment of the PET substrate was required for obtaining good adhesion property between copper films and the substrate. In this study the highest adhesion was observed in sand-blasting, and then followed by those of acid and oxygen plasma treatment. However, the effect of surface energy was insignificant in our experimental range. This is probably due to compensating the difference in surface energy from various pretreatments by exposing substrate to ECR plasma for 5 min or longer at the early stage of the copper deposition. Therefore, it can be concluded that surface roughness of the polymer substrate plays an important role to determine the adhesion of copper-coated polymer for the deposition of copper by ECR-MOCVD.

Changes in Properties of Tropical Kapok Fibers by the Pretreatments (열대산 케이폭 섬유의 전처리에 따른 특성 변화)

  • Shin, Soo-Jeong;Jung, Woong-Ki;Sung, Yong Joo;Lee, Joon-Woo;Kim, Se-Bin
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.1
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    • pp.52-58
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    • 2013
  • The effets of the pretreatments of tropical kapok fibers were evaluated in this study in terms of water sorption capacity and oil sorption capacity. The alkali treatments with NaOH resulted in the reduction of lignin, oil and hemicellulose, which were detected with FT-IR spectrum. The reduction of the lyphophilic components such as fat on kapok fiber by the ozone treatments were also measured with FT-IR spectrum. The oil sorption capacity of kapok fiber was decreased by the alkali treatments and the ozone treatments, while the water sorption capacity was increased. The liquid sorption capacity were greatly affected by the mechanical cutting of kapok fiber which exposed the big lumen of kapok fiber. The hydrophilic property of kapok fiber could be controlled by the pretreatments, which would increase the applicability of kapok fiber for preparation of various functional paper products.

The Effects of Phenolic Radical Carriers on the Enzymatic. Bleaching of Kraft Pulp (Kraft펄프의 효소표백반응에 미치는 페놀라디칼 전달체의 영향)

  • 류근갑
    • KSBB Journal
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    • v.10 no.2
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    • pp.183-190
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    • 1995
  • The effects of enzymatic pretreatments on the bleaching of kraft pulp were studied. The kappa number of pulp samples which represents the lignin content of pulp decreased by 25.2% by the pretreatments with xylanase(EC 3.2.1.8, Pulpzyme HB) while it decreased by 13.7% without enzyme pretreatments after the extraction of the pretreated pulp samples in 1N NaOH. To enhance the effects of enzymatic pretreatment on the bleaching of kraft pulp, phenols were used as radical carriers with the simultaneous use of peroxidase(EC 1.11.1.7, Novozyme 502), $H_2O_2$, and xylanase. Guaiacol (1mM) was most effective by decreasing the kappa number by 29.6% when a low initial concentration of $H_2O_2$ (0.1mM) was used. The use of either a higher initial concentration of $H_2O_2$ or phenols lacking electron donating substituents such as phenol and p-chloyophenol, however, decreased the efficiency of enzymatic pretreatment indicating that the production rate and the stability of phenolic radicals are important parameters.

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Bond strength of self-adhesive resin cements to composite submitted to different surface pretreatments

  • dos Santos, Victor Hugo;Griza, Sandro;de Moraes, Rafael Ratto;Faria-e-Silva, Andre Luis
    • Restorative Dentistry and Endodontics
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    • v.39 no.1
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    • pp.12-16
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    • 2014
  • Objectives: Extensively destroyed teeth are commonly restored with composite resin before cavity preparation for indirect restorations. The longevity of the restoration can be related to the proper bonding of the resin cement to the composite. This study aimed to evaluate the microshear bond strength of two self-adhesive resin cements to composite resin. Material and Methods: Composite discs were subject to one of six different surface pretreatments: none (control), 35% phosphoric acid etching for 30 seconds (PA), application of silane (silane), PA + silane, PA + adhesive, or PA + silane + adhesive (n = 6). A silicone mold containing a cylindrical orifice ($1mm^2$ diameter) was placed over the composite resin. RelyX Unicem (3M ESPE) or BisCem (Bisco Inc.) self-adhesive resin cement was inserted into the orifices and light-cured. Self-adhesive cement cylinders were submitted to shear loading. Data were analyzed by two-way ANOVA and Tukey's test (p < 0.05). Results: Independent of the cement used, the PA + Silane + Adhesive group showed higher microshear bond strength than those of the PA and PA + Silane groups. There was no difference among the other treatments. Unicem presented higher bond strength than BisCem for all experimental conditions. Conclusions: Pretreatments of the composite resin surface might have an effect on the bond strength of self-adhesive resin cements to this substrate.

Nutrient and ruminal fermentation profiles of Camellia seed residues with fungal pretreatment

  • Yang, Chunlei;Chen, Zhongfa;Wu, Yuelei;Wang, Jiakun
    • Asian-Australasian Journal of Animal Sciences
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    • v.32 no.3
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    • pp.357-365
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    • 2019
  • Objective: The experiment was conducted to evaluate the effects of four fungal pretreatments on the nutritional value of Camellia seed residues, and to evaluate the feeding value of pretreated Camellia seed residues for ruminants. Methods: Camellia seed residues were firstly fermented by four lignin degrading fungi, namely, Phanerochaete chrysosporium (P. chrysosporium)-30942, Trichoderma koningiopsis (T. koningiopsis)-2660, Trichoderma aspellum (T. aspellum)-2527, or T. aspellum-2627, under solid-state fermentation (SSF) conditions at six different incubation times. The nutritional value of each fermented Camellia seed residues was then analyzed. The fermentation profiles, organic matter degradability and metabolizable energy of each pre-treated Camellia seed residue were further evaluated using an in vitro rumen fermentation system. Results: After 5 days of fermentation, P. chrysosporium-30942 had higher degradation of lignin (20.51%), consumed less hemicellulose (4.02%), and the SSF efficiency reached 83.43%. T. koningiopsis-2660 degraded more lignin (21.54%) and consumed less cellulose (20.94%) and hemicellulose (2.51%), the SSF efficiency reached 127.93%. The maximum SSF efficiency was 58.18% for T. aspellum-2527 and 47.61% for T. aspellum-2627, appeared at 30 and 15 days respectively. All the fungal pretreatments significantly improved the crude protein content (p<0.05). The Camellia seed residues pretreated for 5 days were found to possess significantly increased organic matter degradability, volatile fatty acid production and metabolizable energy (p<0.05) after the treatment of either P. chrysosporium-30942, T. koningiopsis-2660 or T. aspellum-2527. The fungal pretreatments did not significantly change the rumen fermentation pattern of Camellia seed residues, with an unchanged ratio of acetate to propionate. Conclusion: The fungi showed excellent potential for the solid-state bioconversion of Camellia seed residues into digestible ruminant energy feed, and their shorter lignin degradation characteristics could reduce loss of the other available carbohydrates during SSF.

Effects of pretreatments and storage temperature on the quality of lotus leaves (연잎의 품질특성에 미치는 전처리 방법과 저장온도의 영향)

  • Choi, Jeong-Sil;Kong, Moon-Hee;Yeo, Soo-Hwan;Choi, Han-Seok;Jeong, Seok-Tae
    • Food Science and Preservation
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    • v.23 no.2
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    • pp.155-161
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    • 2016
  • This study aimed to investigate the effects of pretreatments blanching, roasting, drying, and storage temperatures ($25^{\circ}C$, $4^{\circ}C$ and $-10^{\circ}C$) on their quality of lotus leaves. As a result, the lotus leaves retained a good appearance when stored at $25^{\circ}C$ for 5 days, $4^{\circ}C$ for 30 days, and $-10^{\circ}C$ for 90 days, regardless of the pretreatment used. At the same storage temperatures, pH, soluble solids, total acid content, polyphenols, and microorganisms were significantly different among the pretreatments (p<0.05). Soluble solids, pH, and total acid contents were not significantly different for the same pretreatments at different storage temperatures. However, the polyphenol, oxalic acid, and tartaric acid contents of lotus leaves were significantly different after drying and blanching treatments. In particular, it was shown that polyphenol content of the lotus leaf was affected by both pretreatment and storage temperature. In conclusion, the lotus leaves appeared in good condition until 5 days at $25^{\circ}C$, 30 days at $4^{\circ}C$, and 90 days at $-10^{\circ}C$, regardless of the pretreatment while influenced by storage temperature.

EFFECT OF DENTURE BASE SURFACE PRETREATMENTS ON THE TENSILE BOND STRENGTH BETWEEN A RESILIENT LINER AND A PROCESSED DENTURE BASE RESIN (의치상 레진의 표면 전처리가 연성 이장재와의 인장결합강도에 미치는 영향)

  • Yoon, Min-Chul;Jeong, Chang-Mo;Jeon, Young-Chan
    • The Journal of Korean Academy of Prosthodontics
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    • v.45 no.5
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    • pp.621-632
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    • 2007
  • Statement of problem: The failure of adhesion between the resilient denture liner and the denture base is a serious problem in clinic. Purpose: The purpose of this study was to evaluate the effect of denture base resin surface pretreatments (mechanical and/or chemical) on the tensile bond strength between a resilient liner and processed denture resin. Material and method. Acrylic-based resilient liners (Soft liner; GC co., Japan & Coe-Soft; GC America Inc. USA) and silicone-based resilient liners (Mucosoft, Parkell Inc., USA & Dentusil; Bosworth co., USA) were used. Specimens in each soft lining material were divided two groups with or without mechanical pretreatment. Each denture base specimen received 1 of 4 chemical pretreatments including: (1) no treatment, (2) 30-s acetone treatment, (3) 15-s methylene chloride treatment, (4) 180-s methyl methacrylate treatment. All specimens were thermocycled and placed under tension until failure in a universal testing machine. Results: 1. Silicone-based resilient liners exhibited significantly higher tensile bond strengths than acrylic-based resilient liners (P<.05). 2. Grinding the denture base resin improved tensile bond strengths of silicone-based resilient liners, but reduced tensile bond strengths of acrylic-based resilient liners (P<.05). 3. In acrylic-based resilient liners, treating with acetone significantly increased the bond strength of Soft liner and treating with methyl methacrylate significantly increased the bond strength of Coe-Soft (P<.05). However they were not effective compared to silicone-based resilient liner. 4. In silicone-based resilient liners, treating with all chemical etchants significantly increased the bond strength of Mucosoft to denture base, and treating with methylene chloride and methyl methacrylate increased the bond strength of Dentusil to denture base (P<.05). Conclusion: Although chemical and mechanical pretreatments were not effective on tensile bond strength of acrylic-based resilent liner to denture base, treating the denture base resin surface with appropriate chemical etchants after mechanical pretreatment significantly increased the tensile bond strength of silicone-based resilient liner to denture base.