• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.383-384
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• 2006

Fe-4Ni-0.5Mo-1Cu powder was selected as raw material, pressed and sinter-hardened at $1135\;^{\circ}C$ for 30 min with rapid cooling. The density varies in the range of $7.24-7.29\;g/cm^3$. Its fatigue properties have been tested in axial loading of alternating tensile/compressive stress at R=-1 with a servo-pulse pump. The fatigue endurance limit was measured to be 260 MPa. The microstructure showed more homogeneous bainite and martensite. Fractography displayed the fatigue cracks initiated from the pore areas near the surface. A non-typical ductile fatigue striation was found. More dimples occurred on fracture surface due to the plastic deformation, which can prohibit cracking propagation and improve its fatigue properties.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.189-190
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• 2006

During cold compaction processes loose powder is pressed under tooling action in order to produce complex shaped engineering components. Here, the analysis of the plastic deformation of granular packings is of fundamental importance to the development of computer simulation models. Powders can be idealized by packing discrete particles, where each particle is a sphere meshed with finite elements. The pressing of a body centered cubic packing was compared with numerical prediction and experimental data. The global response was expressed in force-displacement curve, and the accuracy of the numerical models analyzed for high relative densities up to 0.95.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.309-310
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• 2006

Porous titanium implants can be produced by powder metallurgy in combination with suitable space holder materials. Various mechanical experiments were done to characterize this material regarding the influence of the processing parameters on microstructure and mechanical properties taking into account the properties of the human bone. In this paper, the anistropic behaviour of uniaxially compacted samples was analysed in compression tests and compared to the behaviour of isostatically pressed samples. The failure of the struts of the porous titanium and the crack- initiation and -growth was examined by in-situ SEM analysis.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.611-612
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• 2006

In a manufacturing technique of the sintered filter, pressureless sintering method has good permeability, it is not need the binder and lubricant used on compacting process, so it has little contamination and it is easy to control the pore size and shape but the mechanical strength is low relatively and it is difficult that parts of complicate form are manufactured. In the case of manufacturing the filter by press and sintering method, in order to be satisfactory characteristic of un-pressed filter, in this study sintered metal filter fabricated by using 30-40mesh stainless steel 316L powder and additive agents. Porosity and structure of pores, permeability and mechanical strength of the sintered filter were investigated with the variation sintering conditions. Porosity was nearly constant about $60{\sim}70%$, density, permeability and mechanical strength were changed markedly with quantity of additive materials and sintering conditions.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.138-139
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• 2006

Sintered steels are materials characterized by residual porosity, whose dimension and morphology strongly affect the fatigue crack growth behaviour of the material. Prismatic specimens were pressed at $7.0\;g/cm^3$ from Astaloy CrM powder and sintered varying the sintering temperature and the cooling rate. Optical observations allowed to evaluate the dimensions and the morphology of the porosity and the microstructural characteristics. Fatigue tests were performed to investigate the threshold zone and to calculate the Paris law. Moreover $K_{Ic}$ tests were performed to complete the investigation. Both on fatigue and $K_{Ic}$ samples a fractographic analysis was carried out to investigate the crack path and the fracture surface features. The results show that the Paris law crack growth exponent is around 6.0 for $1120^{\circ}C$ sintered and around 4.7 for $1250^{\circ}C$ sintered materials. The same dependence to process parameters is not found for $K_{Ith}$.

• 한국재료학회지
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• 제8권3호
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• pp.245-251
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• 1998

Bi를 첨가한 n형 PbTe 가압소결체를 기계적 합금화 공정으로 제조하여, 소결 특성과 열전특성을 분석하고 이를 용해/분쇄법으로 제조한 PbTe가압소결체와 비교하였다. 기계적 합금화 공정으로 제조한 PbTe가압소결체에는 용해/분쇄법으로 제조한 시편에 비해 Seebeck계수가 음의 값으로 증가하였으며, 전기비저항이 증가하고 열전도도가 감소하였다. 또한 기계적 합금화 공정으로 제조한 PbTe에서 최대성능지수가 증가하였으며, \ulcorner대성능지수를 나타내는 온도가 저온으로 이동하였다. 0.3wt% Bi를 첨가한 PbTe를 $650^{\circ}C$에서 가압소결시 기계적 합금화 공정으로 제조한 시편은 $200^{\circ}C$에서 $1.33\times10^{-3}/K$의 최대성능지수를 나타내었으며, 용해/분쇄법으로 제조한 시편은 $400^{\circ}C$에서 $1.07\times10^{-3}/K$의 최대성능지수를 나타내었다.

• 한국분말재료학회지
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• 제8권3호
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• pp.157-162
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• 2001

An optimum route to fabricate the ferrous alloy dispersed $Al_2O_3$ nanocomposites such as $Al_2O_3$/Fe-Ni and $Al_2O_3$/Fe-Co with sound microstructure and desired properties was investigated. The composites were fabricated by the sintering of powder mixtures of $Al_2O_3$ and nano-sized ferrous alloy, in which the alloy was prepared by solution-chemistry routes using metal nitrates powders and a subsequent hydorgen reduction process. Microstructural observation of reduced powder mixture revealed that the Fe-Ni or Fe-Co alloy particles of about 20 nm in size homogeneously surrounded $Al_2O_3$, forming nanocomposite powder. The sintered $Al_2O_3$/Fe-Ni composite showed the formation of Fe$Al_2O_4$ phase, while the reaction phases were not observed in $Al_2O_3$/Fe-Co composite. Hot-pressed $Al_2O_3$/Fe-Ni composite showed improved mechanical properties and magnetic response. The properties are discussed in terms of microstructural characteristics such as the distribution and size of alloy particles.

• 한국분말재료학회지
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• 제25권4호
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• pp.327-330
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• 2018

This study is conducted as a preliminary research to verify the feasibility of Ti-based Oxide dispersion strengthened (ODS) alloy. Pure-Ti powder is mixed with $Y_2O_3$ powder and subsequently, mechanically alloyed at $-150^{\circ}C$. The Ti-based ODS powder is hot-isostatically pressed and subsequently hot-rolled for recrystallization. The microstructure consists of elongated grains and Y excess fine particles. The oxide particle size is larger than that of the typical Fe-based ODS steel. Tensile test shows that the tensile ductility is approximately 25%, while the strength is significantly higher than that of pure Ti. The high-temperature hardness of the Ti-ODS alloy is also significantly higher than that of pure Ti at all temperatures, while being lower than that of Ti-6Al-4V. The dimple structure is well developed, and no evidence of cleavage fracture surface is observed in the fracture surface of the tensile specimen.

• 한국세라믹학회지
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• 제36권10호
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• pp.1102-1107
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• 1999

SiC-Si3N4 composites were prepared by mixing $\alpha$-Si3N4 powder to $\alpha$-SiC powder in the range of 10 to 30 vol% with 10vol% interval. 6wg% Al2O3 and 6wt% Y2O3 were respectively added as sintering aids. Hot pressing was performed at 1,80$0^{\circ}C$ for 1 hour with 25 MPa pressure. In the case of adding 20vol% of $\alpha$-Si3N4 powder the relative density to theoretical value and the flexural strength were 99.1% and 34,420 MPa respectively and the worn amount was 2.09$\times$10-3 mm2 which were the highest values in the all range of he composition. Although the composite containig 10 vol% of $\alpha$-Si3N4 powder showed the highest fracture toughness(KIC) of 4.65MN/m3/2 the reduction of the wear resistance in this composite is likely to be affected by the homogeneity and the uniformity of the grain coalescence and growth during the sintering process.

• 한국재료학회지
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• 제11권11호
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• pp.986-990
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• 2001

An optimum route to fabricate the $A1_2O_3/Fe-Ni$ alloy nanocomposites with sound microstructure and enhanced mechanical properties as well as magnetism was investigated. To prepare homogeneous nanocomposite powders of Fe-Ni alloy and $Al_2O_3$, the solution-chemistry routes using $Al_2O_3 \; Ni(NO_3)_2{\cdot}6H_2O$ and $Fe(NO_3)_3{\cdot}9H_2O$ powders were applied. Microstructural observation of the powder mixture revealed that the Fe-Ni alloy particles of about 20 nm in size were homogeneously surrounded $A1_2O_3$, forming nanocomposite powder. The hot-pressed composite showed improved fracture toughness and magnetic response. These results suggest that the synergy materials with an improved mechanical properties and excellent functionality can be fabricated by controlled powder preparation and consolidation processing.