• Title/Summary/Keyword: powder method

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Characteristic of Tantalum Powder and Effect of Reaction Temperature on the amount of Diluent (희석제량에 따른 탄탈륨 분말 특성 및 반응온도의 영향)

  • 윤재식;박형호;배인성;정성만;김병일
    • Journal of Powder Materials
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    • v.9 no.5
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    • pp.315-321
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    • 2002
  • Pure tantalum powder has been produced by combining Na as a reducing agent, $K_2TaF_{7}$ as feed material, KCl and KF as a diluent in a stainless steel(SUS) bomb, using the method of metallothermic reduction. The present study investigated the effect of the amount of the diluent and reaction temperature on the characteristics of tantalum powder in the production process. The temperature applied in this study $850^{\circ}C$ and the amount of the additional reductant from +5% of the theoretical amount used for the reduction of the entire $K_2TaF_{7}$. The results showed that as the amount of the diluent increased, the reaction temperature became lower because the diluent prevented a temperature rise. Also, according to the mixture ratio of the feed materials and the diluent changed from 1 : 0.25 to 1 : 2, the particle size decreased from $5\mutextrm{m}$ to $1\mutextrm{m}$ and a particle size distribution which is below 325 mesh in fined powder increases from 71% to 83%. The average size of Tantalum powder, $2-4\mutextrm{m}$, was close to that of the commercial powders($2-5\mutextrm{m}$). Also under this condition, impurities contained in the powder were within the range allowed for the commercial Ta powders.

Characteristics of Powder with Amount of Reductant Excess in Production of Tantalum Powder by MR-EMR Combination Process (MR-EMR 복합공정에 의한 탄탈륨분말의 제조시 과잉첨가 환원제 양에 따른 분말의 특성)

  • 배인성;윤재식;박형호;김병일;이현우;김낙찬;설경원
    • Journal of Powder Materials
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    • v.11 no.4
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    • pp.333-340
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    • 2004
  • In this study, tantalum powder has been producted by MR-EMR combination process. MR-EMR combination process is a method that is able to improve demerits of MR(metallothermic reduction) and EMR(electronically mediated reaction) process. This study examined the characteristics of powder with the amount of reductant excess using $K_2$TaF$_{7}$ as feed materials, Na as a reductant and KCl/KF as a diluent. In addition, this study examined acid treatment that affect the high purification of powder. The impurities contained in powder was removed in various conditions of acid treatment. The total charge passed through external circuit and average particle size(FSSS) were increased with increasing amount of sodium excess. The proportion of fine particle(-325mesh) was decreased with increasing amount of sodium excess. The yield was improved from 70% to 76% with increasing amount of sodium excess. Considering the impurities, charge, morphology, particle size and yield, an amount of sodium excess of 10wt% were found to be optimum conditions for MR-EMR combination process.s.

The Quality Properties of Hongsamdasik with Added Red Ginseng Powder (홍삼가루를 첨가한 홍삼다식의 품질 특성)

  • Lee, Mi-Young;Kim, Hyun-Oh
    • The Korean Journal of Food And Nutrition
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    • v.21 no.3
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    • pp.283-287
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    • 2008
  • The principal objective of this study was to assess the quality characteristics of Hongsamdasik prepared with the addition of red ginseng powder(0%, 2%, 4%, 6%, 8%). The moisture content of Hongsamdasik did not significantly differ between the added red ginseng powder group and control group. The following Hunter color values are not part of the sensory evaluation testing in the results obtained with Hongsamdasik, decreased, whereas the a and b values increased with increasing amounts of added red ginseng powder. The bitter taste was evaluated as improving with increased amounts of red ginseng powder. Hongsamdasik with 2% red ginseng powder had the highest acceptability value. On our mechanical evaluation, the hardness recording, which increased from the control value with increased amounts of red ginseng powder, and significantly so(p<0.05). In conclusion, the Hongsamdasik with up to $2{\sim}4%$ added red ginseng powder would be a useful method for the production of Dasik with its traditional high quality.

Magnetic Properties of Fe Powder Core Fabricated by Warm Compaction (온간성형법으로 제조된 Fe 분말 코어의 자성특성)

  • Kim, Se-Hoon;Jo, Tae-Sun;Park, Min-Suh;Kim, Young-Do
    • Journal of Powder Materials
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    • v.14 no.5
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    • pp.298-302
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    • 2007
  • In recent years, a rapid increase in demands for the soft magnetic composite parts has been created and it has been tried to improve their properties by various processing methods, alloying elements and compaction parameters. Warm compaction method has been used for the reduction of residual stress, the improvement of magnetic properties and the higher densities. In this work, the effects of warm compaction and polymer binder on magnetic properties of Fe powder core were investigated. The sintering powder, Fe oxide, was ball-milled for 30n hours. And then ball-milled Fe oxide powder was reduced through hydrogen reduction process. The hydrogen reduced Fe powder and polymer binder were mixed by 3-D turbular mixer. And then the mixed powder was warm-compacted. The magnetic properties such as core loss and permeability were measured by B-H curve analyzer.

Strength Properties of Recycled Concrete Containing Water-redispersible Copolymer Powder (재유화형분말수지를 혼입한 재생콘크리트의 강도 특성)

  • Kim, In-Su;Sung, Chan-Yong
    • Proceedings of the Korean Society of Agricultural Engineers Conference
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    • 2005.10a
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    • pp.128-134
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    • 2005
  • This study was performed to evaluate the strength and durability properties of recycled concrete containing water - redispersible copolymer powder(WRP) and blast furnace slag powder(BSP) [RCWS]. Material used were cemente, recycled coarse aggregare, natural fine aggregate, water-redispersible copolymer powder, blast-furnace slag powder. Especially, Water-redispersible powder was used for blending with Inorganic binders such as cemente, gypsum and hydrated lime etc. First of all, Mixed ratio method of RCWS made Two Type. One was called type-1 which used to BSP content 5% and WRP(Water-redispersible powder) content 0%, 1%, 2%, 3%, 4%, 5%, 6%. respectively. Another was called Type-2 which used to BSP(blast furnace slag powder)content 10% and WRP(Water-redispersible powder) content 0%, 1%, 2%, 3%, 4%, 5%, 6%. respectively. According to the experimental results of (RCWS), Incase Type-2 at curing age 28days, Compressive strength, pulse velocity and dynamic modulous of elasticity were shown higher than Type-1 and The more WRP content increasing($0%{\sim}6%$) was the lower Compressive strength, Pulse velocity and Dynamic modulous of elasticity. Water absorption ratio was in the range of $3.85%\;{\sim}\;3.23%$, it was almost equal to Type-1, 2 but Increasing the WRP content($0%{\sim}6%$), The water absorption ratio is decreased.

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The Development of Aluminium Alloy Piston by Powder Forging Method (분말단조법에 의한 알루미늄 합금 피스톤 개발)

  • Kang, Dae-Yong;Park, Jong-Ok;Kim, Kil-Jun;Kim, Young-Ho;Cho, Jin-Rae;Lee, Jong-Heon
    • Journal of the Korean Society for Precision Engineering
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    • v.17 no.8
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    • pp.87-93
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    • 2000
  • Powder Forging technology is being developed rapidly because of its economic merits and the possibility of lightening parts by replacing steel parts with aluminum ones especially in automotive parts manufacturing. Recently Powder Forging process is widely used for manufacturing primary mechanical parts as a combined technology of P/M and precision hot forging. This paper describes the process conditions for the powder forging of Aluminium alloy piston. For example powder alloy design preform design by FEM simulation cold of compaction of specimens and preform sintering of preform powder forging process. The characteristics of sintered compaction of specimens and preform sintering of preform powder forging process. The characteristics of sintered products and final forged piston ones are investigated with tensile strength hardness ductility and so on. Eventually its results prove the improve mechanical properties of the piston produced by powder forging.

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Effect of drying method on rheological properties of milk powders (건조방법에 따른 분류의 리올로지 특성)

  • Lee, Sang-Cheon;Chang, Kyu-Seob;Park, Young-Deok;Kang, Hyun-Ah
    • Applied Biological Chemistry
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    • v.36 no.6
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    • pp.416-423
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    • 1993
  • Milk powders were made by several drying methods and raw materials, and rheological properties of milk powders were investigated by an Instron Universial Testing Machine. The results obtained are summarised as follows. Bulk density of the drum dried whole milk powder was $0.382\;g/cm^3$ and was higher than that of other milk powders. The Hausner ratio, angle of repose and compressibility of the spray dried skim milk powder were 1.127, $32.5^{\circ}$ and 0.029 respectively. This result indicated that skim milk powder showed free flowing characterristics. The compressibility of the drum dried whole milk powder was decreased by the decrease of moisture content. Compressibility of the milk granule was 0.056 and was lower than that of milk powder. The spray dried milk powder of a grobular shape had higher solidity than the freeze or drum dried milk powder. The drum dried milk powder particles consist of irregular shape.

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Electromagnetic Wave Shielding Effect of Nano-powder Dispersed Epoxy Resin Composite (나노분말이 분산된 에폭시 섬유수지의 전자파차폐 효과)

  • Han, Jun-Young;Lee, Chul-Hee;Choi, Min-Gyu;Hong, Soon-Jik;Park, Joong-Hark;Lee, Dong-Jin
    • Journal of Powder Materials
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    • v.22 no.4
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    • pp.234-239
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    • 2015
  • Electronic products are a major part of evolving industry and human life style; however most of them are known to emit electromagnetic waves that have severe health hazards. Therefore, different materials and fabrication techniques are understudy to control or limit transfer of such waves to human body. In this study, nanocomposite powder is dispersed into epoxy resin and shielding effects such as absorption, reflection, penetration and multiple reflections are investigated. In addition, nano size powder (Ni, $Fe_2O_3$, Fe-85Ni, C-Ni) is fabricated by pulsed wire evaporation method and dispersed manually into epoxy. Characterization techniques such as X-ray diffraction, Scanning electron microscopy and Transmission electron microscopy are used to investigate the phase analysis, size and shape as well as dispersion trend of a nano powder on epoxy matrix. Shielding effect is measured by standard test method to investigate the electromagnetic shielding effectiveness of planar materials, ASTM D4935. At lower frequency, sample consisting nano-powder of Fe-85%Wt Ni shows better electromagnetic shielding effect compared to only epoxy, only Ni, $Fe_2O_3$ and C-Ni samples.

Fabrication and Characterization of Thermal Battery using Porous MgO Separator Infiltrated with Li based Molten Salts

  • Kim, Kyungho;Lee, Sungmin;Im, Chae-Nam;Kang, Seung-Ho;Cheong, Hae-Won;Han, Yoonsoo
    • Journal of Powder Materials
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    • v.24 no.5
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    • pp.364-369
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    • 2017
  • Ceramic powder, such as MgO, is added as a binder to prepare the green compacts of molten salts of an electrolyte for a thermal battery. Despite the addition of a binder, when the thickness of the electrolyte decreases to improve the battery performance, the problem with the unintentional short circuit between the anode and cathode still remains. To improve the current powder molding method, a new type of electrolyte separator with porous MgO preforms is prepared and characteristics of the thermal battery are evaluated. A Spherical PMMA polymer powder is added as a pore-forming agent in the MgO powder, and an organic binder is used to prepare slurry appropriate for tape casting. A porous MgO preform with $300{\mu}m$ thickness is prepared through a binder burnout and sintering process. The particle size of the starting MgO powder has an effect, not on the porosity of the porous MgO preform, but on the battery characteristics. The porosity of the porous MgO preforms is controlled from 60 to 75% using a pore-forming agent. The batteries prepared using various porosities of preforms show a performance equal to or higher than that of the pellet-shaped battery prepared by the conventional powder molding method.

Change in Chemical Components of Green Powder Tea during Storage Period at $-5^{\circ}C$ Storage Temperature (가루녹차의 저온저장($-5^{\circ}C$) 중 품질 변화)

  • Park, Jang-Hyun;Kim, Jong-Keun
    • Food Science and Preservation
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    • v.13 no.6
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    • pp.681-685
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    • 2006
  • The effect of storage methods on green tea powder were investigated by examining quality changes of the tea during storage at $-5^{\circ}C$. aluminium-packing without any treatment showed the green powder tea quality of unchanged for 120 days storage, after which significant decrease in the green powder tea constituents connected quality such as total nitrogen, total amino acid, tannin, caffeine, chlorophyll, vitamin C, and fatty acid were observed. The changes in the green color indexes(a value) of green powder tea at $-5^{\circ}C$ were resulted in the of -16.69, -16.20, and 13.69 for 30, 60, and 120 days with the storage period respectively. A sensuous examination for quality assay of the green powder tea demonstrated 93, 91, 88 and 73 points as a storage period 0, 30, 60 and 120 day, respectively. This study suggested that storage method at $-5^{\circ}C$ was a successful method for storage of green powder tea.