• Title/Summary/Keyword: powder factor

검색결과 511건 처리시간 0.024초

용융염 합성법에 의한 PLZT 세라믹스의 제작과 그 전기적.광학적 특성 (Electrical and Optical Properties of PLZT Ceramics Prepared by Flux Method)

  • 남효덕
    • 한국세라믹학회지
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    • 제23권4호
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    • pp.62-68
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    • 1986
  • $(Pb_{1-x} La_x)(Zr_{0.65} Ti_{0.35})_{1-x/4}O_3$ (PLZT X/65/35) powders were prepared by molten salt synthesis using NaCl-K Cl and conventional calcining of oxides. The effects of molten salt on formation and charactrization of PLZT powder and on dielectric piezolectric and optical properties of PLZT ceramics were studied, The completed PLZT powder formation in the presence of fused salt was attained at 50-10$0^{\circ}C$ lower temperature than that in solid state reaction and the particle size of the powder made by molten salt synthesis was markedly increased with increasing calcining temperature. The substitution of Na and/or K ions in NaCl-KCl for Pb ion in process of molten salt synthesis was increased with increasing La concentration Z. These substituted Na and/or K ions were identified as the origins of decreasing coupl-ing factor and optical transmittance of PLZT ceramics.

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STUDIES ON THE EFFECTS OF GINSENG COMPONENTS ON DIABETES MELLITUS

  • Okuda Hiromichi;Yoshida Ryoichi
    • 고려인삼학회:학술대회논문집
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    • 고려인삼학회 1980년도 학술대회지
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    • pp.53-57
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    • 1980
  • Red ginseng powder was administered at a dose of 2.7 g per day for 3 months to 21 diabetic patients who were under the treatment with insulin. It was found that the ginseng powder was effective to 12 patients and ineffective to 9 patients. Based on these clinical results, experiments were carried out to elucidate factors which concerned with improvement of pathological conditions of diabetes mellitus. In the previous symposium, we reported that red ginseng powder contained an anti-lipolytic peptide, or an insulin-like peptide. In the course of purification of the insulin-like peptide in the ginseng, we found another fraction which possessed anti-lipolytic activity. The anti-lipolytic factor of the fraction was purified by gel filtration on Bio Gel P-2 column and Dowex $50W{\times}4$ column chromatography. The character of the finally purified material was examined by thin-layer chromatography, high-speed liquid chromatography and mass spectrometry. With these examinations, the active principle was indentified to be adenosine. Pharmacological significance of these insulin-like substances, the peptide and adenosine, was discussed.

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액체밀도계에 의한 고로슬래그 미분말 분말도 신속평가에서의 영향인자 분석 (Analysis of Influence Factors in Fineness Rapid Evaluation Blast Furnace Slag Powder by Hydrometer)

  • 문병룡;김민상;이제현;주은희;한민철;한천구
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2017년도 추계 학술논문 발표대회
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    • pp.167-168
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    • 2017
  • In this research, the blast-furnace slag powder using the hydrometer also attempted to analysis the influence factor due to the temperature change of water and sample, and the number of upside down turns at the time of rapid evaluation. As a result, the influence of the number of turn was not large, but was the temperature of the water and sample are greatly affected.

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The Effect of the Sintering Additives on the Fabrication and Thermal Conductivity of Porous Sintered RBSN

  • Park, Young-Jo;Kim, Hai-Doo
    • 한국세라믹학회지
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    • 제44권7호
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    • pp.354-357
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    • 2007
  • The nitriding and post-sintering behavior of silicon powder compact containing sintering additives of 2.3 wt% and 7 wt% were investigated in this study. Regardless of the liquid phase content, elongated large grains of a typical morphology evolved in the post-sintered specimens. Phase analysis revealed a complete phase transformation into ${\beta}-Si_3N_4$ in both porous systems. Oxynitride second phases (mellilite) precipitated in the latter, while those were free in the former containing less amount of liquid phase. The post-sintering condition that yielded a favorable microstructure for a filter application was achieved when the specimens were soaked at $1800^{\circ}C$ for 2 h. It was found that the thermal conductivity of porous $Si_3N_4$ ceramics is dominated by the porosity more than this factor is influenced by the addition of $Al_2O_3$.

PFC용 Boost 컨버터의 금속분말 인덕터에 관한 연구 (A Study on the Metal Powder Inductor of a Boost Converter for PFC)

  • 김윤성;안태영;장평우;정인범;최광보
    • 전력전자학회:학술대회논문집
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    • 전력전자학회 2001년도 전력전자학술대회 논문집
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    • pp.368-371
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    • 2001
  • In this paper, the experiment and simulation results of the Boost converter for PFC(power factor correction) using metal powder inductor are presented. The metal powder inductor used in the experiment was composed of Ni-Fe-Mo, Ni-Fe, Fe-Si-Al compound respectively The performance of the 500w class PFC rectifier with the average current mode control and the 300W class PFC rectifier with the variable frequency control, are evaluated.

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훼로보론과 NaBF4 에 의한 강재의 침 경화처리에 관하여 (Study on the Boriding of Steel in Ferroboron and NaBF4 Powder Mixture)

  • 김문일;여운관
    • 한국표면공학회지
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    • 제8권3호
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    • pp.5-11
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    • 1975
  • The boronizing method using ferroborn and NaBF4 powder mixture was studied for surface hardening of medium carbon steel. This boride layer was compared with a boride layer that was formed in ferroboron and KBF4 powder mixture. The frequency factor and activation energy were discussed in this paper. The main results obtained can be summerized as follow. 1) The optimum range of NaBF4 content is 10 to 15% of weight to obtain a thick and dense boride layer. 2) The depth of the boride layer was approximately expressed by the following equation : {{{{d=100 exp (-18,000/RT) SQRT { t} }} 3) The oxidating resistance of boronized steel proved to be good at 800$^{\circ}C$ but almost unacceptable near at 900 $^{\circ}C$. 4) The NaBF4 effect was the same as that reported for KBF4.

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Analysis of $Si_3N_4$ Ultra Fine Powder Using High-pressure Acid Digestion and Slurry Injection in Inductively Coupled Plasma Atomic Emission Spectrometry

  • 김K.H.;김H.Y.;임H.B.
    • Bulletin of the Korean Chemical Society
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    • 제22권2호
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    • pp.159-163
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    • 2001
  • Si3N4 powder has been analyzed by inductively coupled plasma atomic emission spectrometry (ICP-AES). The sample was dissolved by high-pressure acid digestion with HF, H2SO4 (1+1), and HNO3 mix ture. This technique is well suited for the impurity analysis of Si3N4 because the matrix interference is eliminated. A round-robin samples trace elements, such as Ca, W, Co, Al, Fe, Mg, and Na, were determined. For the direct analysis, slurry nebulization of 0.96 mm Si3N4 powder also has been studied by ICP-AES. Emission intensities of Fe were measured as ICP operational conditions were changed. Significant signal difference between slurry particles and aqueous solution was observed in the present experiment. Analytical results of slurry injection and high-pressure acid digestion were compared. For the use of aqueous standard solution for calibration, k-factor was determined to be 1.71 for further application.

강황분말을 첨가한 Sugar-snap cookies의 품질 특성 (Quality Characteristics of Sugar-snap Cookies by additions of Curcuma Longa L. Powder)

  • 최영심;이명호;지옥화
    • 한국조리학회지
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    • 제17권2호
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    • pp.198-208
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    • 2011
  • 본 연구는 강황분말의 첨가량(0, 3, 6, 9, 12, 15%)을 달리 한 sugar-snap cookies의 품질 특성과 관능특성을 평가한 것으로 강황분말을 첨가한 sugar-snap cookies 반죽의 pH는 6.58~7.32 범위였으며 sugar-snap cookies의 수분함량은 9.09~10.77% 사이의 범위였다. 퍼점성은 유의적으로 낮아지는 경향을 보였으며, 강황분말 첨가량이 증가할수록 쿠키의 명도는 감소하고 a값과 b 값은 유의적으로 증가하는 경향이 나타났다(p<0.05). 경도(hardness)는 강황분말 첨가량이 증가할수록 증가하였으며 관능검사는 맛, 색, 향, 조직감, 전체적인 기호도의 항목에서 강황분말 첨가향이 6%일 때 전반적으로 가장 높게 평가되어, 6%의 강황분말을 첨가한 sugar-snap cookies 제조가 적합하다고 사료된다.

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자외선 처리한 목이버섯 분말 첨가량에 따른 쿠키의 품질 특성 (Analysis of the Quality Characteristics of Cookies based on the Addition Rate of Ear Mushroom (Auricularia auricula-judae Quel.) Powder by Ultraviolet B Treatment)

  • 신소희;최소라;송영은;한현아;이송이
    • 한국식품영양학회지
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    • 제33권6호
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    • pp.672-680
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    • 2020
  • This study was conducted to effectively supplement vitamin D and increase the consumption of ear mushroom based on the investigation of the quality characteristics of cookies containing ear mushroom supplemented with vitamin D. Cookies were made of 0%, 1%, 3%, and 5% ear mushroom powder treated by ultraviolet B. Increased addition of ear mushroom powder led to a decrease in the bulk density of the dough as well as a spread factor, color value, and hardness of the cookies. There was no significant difference in the loss rate, but the water content of the dough and cookies was increased. The total polyphenol content of cookies added with 1~5% ear mushroom powder was higher than that of the 0%. The DPPH free radical scavenging activity of cookies added with 5% ear mushroom powder (23.8%) was 2 times higher than that of the 0% (10.9%). The vitamin D2 content of cookies added with 5% ear mushroom powder (835.5 ㎍/100 g D.W.) was 44 times higher than that of the 0% (19.0 ㎍/100 g D.W.). Consequently, ear mushroom powder is considered to be suitable for the production of functional cookies because of high values of antioxidant activity and vitamin D2 content.

합성 방법에 따른 Li1.3Al0.3Ti1.7(PO4)3 소결체의 미세 구조 및 이온전도 특성 연구 (A Study on the Microstructures and Ionic Conductivity of Li1.3Al0.3Ti1.7(PO4)3 with Different Synthesis Routes)

  • 최슬기;최재원;양민호
    • 한국분말재료학회지
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    • 제30권2호
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    • pp.107-115
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    • 2023
  • Li1.3Al0.3Ti1.7(PO4)3(LATP) is considered a promising material for all-solid-state lithium batteries owing to its high moisture stability, wide potential window (~6 V), and relatively high ion conductivity (10-3-10-4 S/cm). Solid electrolytes based on LATP are manufactured via sintering, using LATP powder as the starting material. The properties of the starting materials depend on the synthesis conditions, which affect the microstructure and ionic conductivity of the solid electrolytes. In this study, we synthesize the LATP powder using sol-gel and co-precipitation methods and characterize the physical properties of powder, such as size, shape, and crystallinity. In addition, we have prepared a disc-shaped LATP solid electrolyte using LATP powder as the starting material. In addition, X-ray diffraction, scanning electron microscopy, and electrochemical impedance spectroscopic measurements are conducted to analyze the grain size, microstructures, and ion conduction properties. These results indicate that the synthesis conditions of the powder are a crucial factor in creating microstructures and affecting the conduction properties of lithium ions in solid electrolytes.