• 한국세라믹학회지
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• 제38권4호
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• pp.307-307
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• 2001

Combustion process with citrate was used to produce the LiMn$_2$O$_4$powder. Precursors are pre-ignited in open air followed by post-heating in the range from $600^{\circ}C$ to 80$0^{\circ}C$ for 4h. With varying the molar ratio (R) of ethylene glycol (EG) to citric acid (CA) from 0 to 4, the effect of EG content on powder characteristics is evaluated. Vacuum drying promote the auto-ignition at room temperature. With small addition of EG metal ion was selectively segregated with organic substances and undesired lithium evaporation occurred during post-heating. LiMn$_2$O$_4$phase which is produced by combustion reaction was decomposed back to Mn$_3$O$_4$because the reaction temperature was higher than 95$0^{\circ}C$. With increasing EG content, the homogeneity of LiMn$_2$O$_4$powder increased and specific surface area increased. And lithium evaporation during vacuum drying and/or ignition also increased.

• Computers and Concrete
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• 제23권4호
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• pp.281-294
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• 2019

The post-fire behavior of structural elements and the cooling process has always been one of the main concerns of the structural engineers. The structures can be cooled at different rates, where they affect the structure's behavior. In the present study, a numerical model has been developed using the Abaqus program to investigate the effect of cooling rate on the post-fire behavior of the CFST column. To verify the model, results of an experimental study performed on CFST columns within a full heating and cooling cycle have been used. In this model, coMParison of the residual strength has been employed in order to examine the behavior of CFST column under different cooling rates. Furthermore, a parametric study was carried out on the strength of steel and concrete, the height of the specimens, the axial load ratio and the cross-sectional shape of the specimen through the proposed model. It was observed that the cooling rate affects the behavior of the column after the fire, and thus the higher the specimen's temperature is, the more effect it has on the behavior. It was also noticed that water cooling had slightly more residual strength than natural cooling. Furthermore, it was recognized from the parametric study, that by increasing the strength of steel and concrete and the load ratio, as well as modifying the cross-sectional shape from circular to square, residual strength of column at the cooling phase was less than that of the heating phase. In addition, with reducing column height, no change was witnessed in the column behavior after the cooling phase.

• 한국표면공학회지
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• 제29권6호
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• pp.766-772
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• 1996

Undoped $SnO_x$ thin films were deposited on Si(100) substrate by using reactive ioassisted deposition technique (R-IAD). In order to investigate the effect of initial oxygen content and heat treatment on the oxidation state and crystalline structure of tin oxide films, $SnO_x$ thin films were post-annealed at 400~$600^{\circ}C$ for 1 hr. in a vacuum ~$5 \times 10^{-3}$ -3/ Torr or were directly deposited on the substrate of $400^{\circ}C$ and the relative arrival ration ($Gamma$) of oxygen ion to Sn metal varied from 0.025 to 0.1, i.e., average impinging energy ($E_a$) form 25 to 100 eV/atom. As $E_a$ increased, the composition ratio of $N_ON{sn}$ changed from 1.25 to 1.93 in post-annealing, treatment and 1.21 to 1.87 in in-situ substrate heating. In case of post-annealing, the oxidation from SnO to $SnO_2$ was closely related to initial oxygen contents and post-annealing temperature, and the perfect oxidation of $SnO_2$ in the film was obtained at higher than $E_a$=75 eV/atom and $600^{\circ}C$. The temperature for perfect oxidation of $SnO_2$ was reduced as low as $400^{\circ}C$ through in-situ substrate heating. The variation of the chemical state of $SnO_x$ thin films with changing $E_a$'s and heating method were also observed by Auger electron spectroscopy.

• 대한기계학회논문집
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• 제11권2호
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• pp.314-321
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• 1987

본 논문에서는 용접열영향부(heat affected zone: HAZ)의 인성에 영향을 미치 는 인자중에서 잔유응력의 영향은 중대한 문제로 주목되고 있으며, 이로 인한 용접재 의 기계적 성질의 저하를 경함하기 위한 방법으로 용접후열처리(post weld heat trea- tment: PWHT)에 의한 제거방법을 이용하고 있다.그러나 이 열처리는 보톤 600.deg. C 이 상의 고온에서 실현되기 때문에 열처리과정에서 템퍼링(tempering)효과로 인한 HAZ의 열화가 때때로 발생하고 있어서 용접 시공상 문제로 되고 있다. 또한 PWHT시에는 가 열중이나 냉각중에도 열처리효과가 진행되고 있다고 볼 수 있으므로, PWHT가열속도는 기계적 성질의 개선이라는 이유외에 경제적 측면에서도 중요시 된다. 특히 용접조직 의 포화는 파괴의 양식에 직접반영되어, 파면형태의 차로 나타나므로, 본 조직의 포화 와 관련시켜 검토하기 위하여 열처리된 HAZ를 대상으로 작용된 응력의 크기와 가열속 도가 HAZ의 파괴인성에 어떠한 영향을 미치는지를 COD파괴인성시험과 미소경도측정, 그리고 주사전자현미경관찰을 통하여 고찰하였다.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2001년도 하계학술대회 논문집
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• pp.709-712
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• 2001

The effects of post annealing temperature by the Rapid Thermal Annealing(RTA) on the electrical properties of Pb(Zr,Ti)O$_3$(PZT) thin film were investigated. Analyses by the RTA treatments reveled that the leakage current of PZT thin films strongly depend on heating temperature and time. It was found that leakage current properties of PZT capacitor were changed by heating temperature during the RTA annealing. On Pt/Ti/Si substrates, PZT films are deposited at 350 $^{\circ}C$ by rf magnetron sputtering. The X-ray diffusion (XRD) was confirmed the formation of PZT thin film. Leakage current characteristics were improved with decreasing the post annealing temperature of PZT thin film. RTA annealed film on the 700$^{\circ}C$ shows ferroelectric and electrical properties with a remanent polarization of 12.4${\mu}$C/$\textrm{cm}^2$ coercive field of 117kV/cm, leakage current J= 6.2${\times}$10$\^$-6/ A/$\textrm{cm}^2$

• Structural Engineering and Mechanics
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• 제57권2호
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• pp.265-280
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• 2016

A NLFE model was proposed to investigate the mechanical behavior of short columns, cast using plain or fibrous lightweight aggregate concrete (LWAC), and subjected to elevated temperatures of up to $700^{\circ}C$. The model was validated, before its predictions were extended to study the effect of other variables, not studied experimentally. The three-dimensional NLFE model was developed using ANSYS software and involved rational simulation of thermal mechanical behavior of plain and fibrous LWAC as well as longitudinal and lateral steel reinforcement. The prediction from the NLFE model of columns' mechanical behavior, as represented by the stress-strain diagram and its characteristics, compared well with the experimental results. The predictions of the proposed models, considering wide range of lateral reinforcement ratios, confirmed the behaviors observed experimentally and stipulated the importance of steel confinement in preserving post-heating mechanical properties of plain and fibrous LWAC columns, being subjected to high temperature.

• 동력기계공학회지
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• 제7권2호
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• pp.56-60
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• 2003

Recently the plastic fuel tube is usually used to reduce production cost and weight in automobiles. These days, material used to plastic fuel tube is the polyamide12. The fuel tube is made of the PA12. Post deformation of the tube has been changed by environmental temperature. So, it is important to prevent post deformation. The experiment is performed to investigate post deformation of the tube produced by each bending process. In this study, the results we obtained are used to bending process system for post deformation as the environmental temperature of the tube. It turned out that the method of steam heating and air cooling was shown less deformation than other methods.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1998년도 춘계학술대회 논문집
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• pp.227-230
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• 1998

The effects of post curing conditions on thermal properties of alumina filled epoxy resin system DGEBA/MDA/SN were investigated. As the post curing time increased at 15$0^{\circ}C$, the glass transition temperature increased from 121 to 124, slightly. As the heating rate increased, high thermal decomposing temperature (T$_{d}$) and most decomposing temperature (T$_{p}$) increased. For the case of post-cured system at 15$0^{\circ}C$ for 4 days showed lower values than virgin system. At the post curing condition the system must have been thermally degraded.ded.

• 전력전자학회:학술대회논문집
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• 전력전자학회 2019년도 전력전자학술대회
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• pp.265-266
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• 2019

This paper proposed a three-channel transformer-type power regulator to control the heater temperature by adjusting the voltage across the heater for pre-heating and the post-heating procedures of the material welding. The experimental results are carried out to verify the performance of three-channel heater temperature control for the heat treatment.

• 태양에너지
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• 제10권1호
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• pp.80-91
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• 1990

1985년도에 체신부에서는 태양열 우체국사를 체신부 산하 각청마다 시범적으로 1개국씩 건립하였는데, 건립된 우체국사 전부 자연형 태양열 시스템을 적용하였다. 이후 '89년까지 전국에 26개 자연형 태양열 우체국사가 건립되어 우리나라에 있어서 자연형 태양열 공공건물의 영역을 확대시키는데 획기적인 계기가 되었다. 따라서 본고에서는 이제까지 건립된 자연형 태양열 우체국사의 문제점을 실태조사 등을 통해 파악하여 이들 문제점을 단계적 해결을 위한 접근 방향을 모색하고, 이와 더불어 보다 열성능이 향상되고, 업무환경이 개선된 자연형 태양열 우체국사의 본격적 건립에 필요한 기초자료를 제공하고자 한다.