• Title/Summary/Keyword: post-heating

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The Preferred Orientation and Morphology Characteristics of AlN Thin Films Prepared by RF Power Under Room Temperature Process (저온공정을 이용한 AlN 박막의 우선배향성과 모폴로지에 관한 연구)

  • Oh, Su-Young;Kim, Eung-Kwon;Lee, Tae-Yong;Kang, Hyun-Il;Yu, Hyun-Kyu;Song, Joon-Tae
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.5
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    • pp.458-462
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    • 2008
  • In this paper, we investigated the (002) preferred orientation and morphology characteristics of AlN thin film by using reactive rf sputtering. Additionally, AlN thin films grown in the range from 150 to 300 W were studied under room temperature without substrate heating and post annealing. Sputtered AlN thin films were well grown on Si substrates and the (002) main peak in XRD patterns showed the highest intensity at 300 W with $0.25^{\circ}$ degree of full width at half-maximum (FWHM). As increased RF power, the surface roughness was increased from 1.0 to 3.4 nm. In Fourier transformation infrared spectroscopy (FTIR), $A_1$ (TO) and $E_1$ (TO) mode closed to AlN thin film confirmed the changes with increasing the intensity rate. From these results, we could confirm a chance of the growth of AlN thin film by only low temperature.

Electrical Properties of ITO Thin Film Deposited by Reactive DC Magnetron Sputtering using Various Sn Concentration Target (반응성 DC 마그네트론 스퍼터링법으로 증착한 ITO 박막의 전기적 특성 평가)

  • Kim, Min-Je;Jung, Jae-Heon;Song, Pung-Keun
    • Journal of the Korean institute of surface engineering
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    • v.47 no.6
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    • pp.311-315
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    • 2014
  • Indium tin oxide (ITO) thin films (30 nm) were deposited on PET substrate by reactive DC magnetron sputtering using In/Sn(2, 5 wt.%) metal alloy target without intentionally substrate heating during the deposition under different DC powers of 70 ~ 110 W. The electrical properties were estimated by Hall-effect measurements system. The resistivity of ITO thin film deposited using In/Sn (5 wt.%) metal alloy target at low DC power increased with increasing annealing time. However, they increased with increasing annealing time at high DC power. In the case of ITO (Sn 2 wt%), we can't find clear change in resistivity with increasing annealing time. However, carrier density and mobility showed difference behavior due to change of oxygen vacancy.

Analysis of House Energy for Remodeling Rural House (농촌 노후주택 정비를 위한 건물에너지 분석)

  • Park, Mee-Jeong;Kim, Jeong-gook;Shin, Min-Ji;Oh, Su-Min;Nam, He-Kyeong;Yoo, Ji-Hwang;Kim, Eun-Ja;Lim, Chang-Su
    • Journal of the Korean Institute of Rural Architecture
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    • v.21 no.3
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    • pp.9-16
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    • 2019
  • The increase in housing energy costs due to deteriorated rural house is directly related to the quality of life of rural residents, which is fundamental challenge for the government. In this study, we analyzed the current energy performance and the effect of housing energy efficiency improvement after remodeling of the four rural houses over 20 years old considering the rural housing type. As the result, the heating energy requirements of the unit surface is very high, and the effect was predicted to vary by housing after improved thermal insulation. This means that the cost of housing energy will be utilized as a target selection criterion or post-effect for the rural house remodeling project. In addition, the energy performance was analyze for the compact houses, which are in demand, mainly for young rural immigrants. As the result, the energy performance is very efficient.

An experimental and numerical analysis of concrete walls exposed to fire

  • Baghdadi, Mohamed;Dimia, Mohamed S.;Guenfoud, Mohamed;Bouchair, Abdelhamid
    • Structural Engineering and Mechanics
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    • v.77 no.6
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    • pp.819-830
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    • 2021
  • To evaluate the performance of concrete load bearing walls in a structure under horizontal loads after being exposed to real fire, two steps were followed. In the first step, an experimental study was performed on the thermo-mechanical properties of concrete after heating to temperatures of 200-1000℃ with the purpose of determining the residual mechanical properties after cooling. The temperature was increased in line with natural fire curve in an electric furnace. The peak temperature was maintained for a period of 1.5 hour and then allowed to cool gradually in air at room temperature. All specimens were made from calcareous aggregate to be used for determining the residual properties: compressive strength, static and dynamic elasticity modulus by means of UPV test, including the mass loss. The concrete residual compressive strength and elastic modulus values were compared with those calculated from Eurocode and other analytical models from other studies, and were found to be satisfactory. In the second step, experimental analysis results were then implemented into structural numerical analysis to predict the post-fire load-bearing capacity response of the walls under vertical and horizontal loads. The parameters considered in this analysis were the effective height, the thickness of the wall, various support conditions and the residual strength of concrete. The results indicate that fire damage does not significantly affect the lateral capacity and stiffness of reinforced walls for temperature fires up to 400℃.

1-D Modeling of Heater Surface Temperature Distribution in EHC-based Urea-SCR System (EHC 기반 Urea-SCR 시스템 히터 표면온도 분포의 1-D 모델링)

  • Park, Sunhong;Son, Jihyun;Moon, Seoksu;Oh, Kwangchul;Jang, Sungwook;Park, Sungsuh
    • Journal of ILASS-Korea
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    • v.27 no.1
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    • pp.11-17
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    • 2022
  • In upcoming Post Stage-V and Tier 5 regulations of construction machineries, nitrogen oxide (NOx) emissions are strictly limited in cold start conditions. In response to this, a method of improving NOx conversion efficiency has been applied by installing an electric heating catalyst (EHC) in front of conventional urea-SCR systems so that the evaporation and thermal decomposition of urea-water solution can be promoted in cold start conditions. In this strategy, the evaporation and thermal decomposition of urea-water solution and corresponding NOx conversion efficiency are governed by temperature conditions inside the EHC. Therefore, characterizing the temperature distribution in the EHC under various operating conditions is crucial for the optimized operation and control of the EHC in Urea-SCR systems. In this study, a 1-D modeling analysis was performed to predict the heater surface temperature distribution in EHC under various operating conditions. The reliability of prediction results was verified by comparing them with measurement results obtained using an infrared (IR) camera. Based on 1-D analysis results, the effects of various EHC operation parameters on the heater surface temperature distribution were analyzed and discussed.

Investigation of the effect of internal curing as a novel method for improvement of post-fire properties of high-performance concrete

  • Moein Mousavi;Habib Akbarzadeh Bengar
    • Computers and Concrete
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    • v.33 no.3
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    • pp.309-324
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    • 2024
  • Internal curing, a widely used method for mitigating early-age shrinkage in concrete, also offers notable advantages for concrete durability. This paper explores the potential of internal curing by partial replacement of sand with fine lightweight aggregate for enhancing the behavior of high-performance concrete at elevated temperatures. Such a technique may prove economical and safe for the construction of skyscrapers, where explosive spalling of high-performance concrete in fire is a potential hazard. To reach this aim, the physico-mechanical features of internally cured high-strength concrete specimens, including mass loss, compressive strength, strain at peak stress, modulus of elasticity, stress-strain curve, toughness, and flexural strength, were investigated under different temperature exposures; and to predict some of these mechanical properties, a number of equations were proposed. Based on the experimental results, an advanced stress-strain model was proposed for internally cured high-performance concrete at different temperature levels, the results of which agreed well with the test data. It was observed that the replacement of 10% of sand with pre-wetted fine lightweight expanded clay aggregate (LECA) not only did not reduce the compressive strength at ambient temperature, but also prevented explosive spalling and could retain 20% of its ambient compressive strength after heating up to 800℃. It was then concluded that internal curing is an excellent method to enhance the performance of high-strength concrete at elevated temperatures.

Development of a prototype TL/OSL reader for on-site use in a large-scale radiological accident

  • Hyoungtaek Kim;Chang-Young Park;Sang In Kim;Min Chae Kim;Jungil Lee
    • Nuclear Engineering and Technology
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    • v.56 no.6
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    • pp.2113-2119
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    • 2024
  • This study presents the development and characterization of a prototype TL/OSL reader for the retrospective dose assessment of individuals in radiological emergencies. The reader is portable, semi-automatic, and capable of accurate measurements. The dimension of the reader is 25 × 25 × 37 cm3 and the weight is about 15 kg. The reader consists of a sample moving stage, a heating module, an optical stimulation module, a detection module, a data acquisition (DAQ) unit, a nitrogen gas control module, and a PC with a GUI program. The reader has three measurement modes: TL, CW_OSL, and custom mode. The reader was characterized using commercial thermal luminescence dosimeters (TLD, LiF:Mg,Cu,Si) and optically stimulated dosimeters (OSLD, Al2O3:C), as well as fortuitous materials, such as display glasses and resistors of mobile phone. The results showed that the reader is capable of measuring signals with a detection limit of up to 0.02 mGy using a commercial dosimeter. In the dose recovery test using fortuitous materials, the reconstructed doses obtained three days post-irradiation closely aligned with the initially administered doses. As a result, this study suggests that the developed TL/OSL reader is a promising instrument for emergency dose assessment at accident sites.

Recovery of BTEX-aromatics from Post-consumer Polypropylene Fraction by Pyrolysis Using a Fluidized Bed (유동층(流動層) 급속열분해(急速熱分解)에 의한 폐(廢) Polypropylene fraction으로부터 BTEX-aromatics의 회수(回收))

  • Cho, Min-Hwan;Jeong, Soo-Hwa;Kim, Joo-Sik
    • Resources Recycling
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    • v.17 no.6
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    • pp.50-56
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    • 2008
  • A polypropylene fraction collected from the stream of post-consumer plastics was pyrolyzed. The aim of this study is to observe the dependence of yield of BTEX-aromatics normally used as solvent on the reaction temperature. To reach the goal, three experiments were carried out at different temperature between 650 and $700^{\circ}C$, using a fluidized bed reactor that shows an excellent heat transfer. In the experiments, product gases were used as a fluidizing medium to maximize the amount of BTEX-aromatics at fixed flow rate and feed rate during the pyrolysis. Oil, gas and char were obtained as product fractions. Product gases were analyzed with GCs(TCD, FID) and with a GC-MS system for qualitative analysis. For an accurate analysis of product oil, the product oil was distilled under vacuum, and separated the distillation residues from oil fractions that were actually analyzed with a GC-MS system. As the reaction temperature went higher, the content of BTEX-aromatics increased. The maximal yield of BTEX-aromatics was obtained at $695^{\circ}C$ with a value of about 30%. The main compounds of product gas were $CH_4$, $C_2H_4$, $C_2H_6$, $C_3H_6$, $C_4H_{10}$ and the product gas had an higher heating value about 45MJ/kg. It could be used as a heat source for a pyrolysis plant or for other fuel applications.

Physical Properties of ZnO Thin Films Grown by Sol-Gel Process with Different Preheating Temperatures (예열 온도 변화에 따른 Sol-Gel 법에 의해 제작된 ZnO 박막의 물리적 특성 연구)

  • 김익주;한호철;이충선;송용진;태원필;서수정;김용성
    • Journal of the Korean Ceramic Society
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    • v.41 no.2
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    • pp.136-142
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    • 2004
  • A homogeneous and stable ZnO sol was prepared by dissolving the zinc acetate dihydrate(Zn(CH$_3$COO)$_2$$.$2H$_2$O) in solution of isopropanol((CH$_3$)$_2$$.$CHOH) and monoethanolamine(MEA:H$_2$NCH$_2$CH$_2$OH). ZnO thin films were prepared by sol-gel spin-coating method and investigated for c-axis preferred orientation and physical properties with preheating temperature. The c-axis growth had a difference as increaing preheating temperature. ZnO thin film preheated at 275$^{\circ}C$ and post-heated at 650$^{\circ}C$ was highly oriented along the (002) plane. After preheating at 200∼300$^{\circ}C$ and post-heating at 650$^{\circ}C$, the transmittance of ZnO thin films by UV-vis. measurement was over 85% in visible range and exhibited absorption edges at about 370 nm. The optical band gap energy was obtained about 3.22 eV, The photoluminescence emission characteristics of ZnO thin film preheated at 275$^{\circ}C$ and post-heated at 650$^{\circ}C$ was found to orange emission(620 nm, 2.0 eV) by PL measurement, which revealed the possibility for application of inorganic photoluminescence device.

An Experimental Analysis of Ultrasonic Cavitation Effect on Ondol Pipeline Management (온돌 파이프라인 관리를 위한 초음파 캐비테이션 효과에 대한 실험적 분석)

  • Lee, Ung-Kyun
    • Journal of the Korea Institute of Building Construction
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    • v.24 no.1
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    • pp.67-75
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    • 2024
  • In the context of Korean residential heating systems, Ondol pipelines are a prevalent choice. However, the maintenance of these pipelines becomes a complex task once they are embedded within concrete structures. As time progresses, the accumulation of sludge, corrosive oxides, and microorganisms on the inner surfaces of these pipelines diminishes their heating efficiency. In extreme scenarios, this accumulation can induce corrosion and scale formation, compromising the system's integrity. Consequently, this research introduces an ultrasonic generation system tailored for the upkeep of Ondol pipelines, with the objective of empirically assessing its practicality. This investigation delineates three variants of ultrasonic generating apparatuses: those employing surface vibration, external generation, and internal generation techniques. To emulate the presence of contaminants within the pipelines, substances in powder, slurry, and liquid forms were employed. The efficacy of the cleaning process post-ultrasonic wave application was scrutinized over time, with image analysis methodologies being utilized to evaluate the outcomes. The findings indicate that ultrasonic waves, whether generated externally or internally, exert a beneficial effect on the cleanliness of the pipelines. Given the inherent characteristics of Ondol pipelines, external generation proves impractical, thereby rendering internal generation a more viable solution for pipeline maintenance. It is anticipated that future endeavors will pave the way for innovative maintenance strategies for Ondol pipelines, particularly through the advancement of internal generation technologies for pipeline applications.